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Synthesis of Titanium Oxide Doped with Neodymium Oxide in a Confined Impinging-Jets Reactor

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Abstract

Technologically advanced and easily scalable method for the synthesis of titanium dioxide doped with neodymium oxide via the hydrolysis of titanium tetraisopropylate in the presence of neodymium nitrate in isopropyl alcohol in a confined impinging-jets reactor has been developed. 30 min heating of the amorphous product at 350°С has been sufficient for the formation of the anatase phase. The proposed method can significantly reduce the duration of the synthesis, is energy-efficient, and does not require numerous time-consuming operations.

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Funding

This study was financially supported by the Ministry of Science and Higher Education of Russian Federation in the scope of the state task (no. 0097-2019-0017) and performed using the equipment of the Engineering Center of St. Petersburg State Institute of Technology (Technical University).

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Authors and Affiliations

  1. I.V. Grebenshchikov Institute of Silicate Chemistry of Russian Academy of Sciences, 199034, St. Petersburg, Russia

    A. V. Zdravkov, Yu. S. Kudryashova & R. Sh. Abiev

  2. St. Petersburg State Institute of Technology (Technical University), 190013, St. Petersburg, Russia

    R. Sh. Abiev

Authors
  1. A. V. Zdravkov
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  2. Yu. S. Kudryashova
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  3. R. Sh. Abiev
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Correspondence to A. V. Zdravkov.

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Zdravkov, A.V., Kudryashova, Y.S. & Abiev, R.S. Synthesis of Titanium Oxide Doped with Neodymium Oxide in a Confined Impinging-Jets Reactor. Russ J Gen Chem 90, 1677–1680 (2020). https://doi.org/10.1134/S1070363220090145

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  • DOI: https://doi.org/10.1134/S1070363220090145

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