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Surface Modification of Magnetic Mesoporous Systems with Aminopropyl Groups and Their Properties

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Abstract

Iron oxide silica FexOy-SiO2 composite systems with aminopropyl (AP) groups on the surface have been synthesized via different routes. The surface modified samples have been studied by X-ray diffraction (XRD) analysis and IR spectroscopy. Magnetic phases of iron oxides have been detected after post-synthetic grafting of AP groups onto the surface of these composite systems. Magnetic properties of these samples have been determined. Only insignificant reduction in the material saturation magnetization and remanent magnetization have been registered upon surface grafting procedure. This approach has been considered to be successful as magnetic properties of the substrate were preserved. Amount of aminoalkyl groups grafted onto the silica composite surface has been determined by thermogravimetric analysis. The mass fraction of grafted aminoalkyl groups has been found to be dependent on the textural properties of the composite sample.

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Acknowledgments

This work was carried out using the equipment of The Core Facilities Center “Research of materials and matter” at the PERC UB RAS.

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Authors and Affiliations

  1. Institute of Technical Chemistry, UB RAS, Acad. Korolev St. 3, Perm, Russian Federation, 614013

    Natalia B. Kondrashova, Artem Sh. Shamsutdinov, Viktor A. Valtsifer & Vladimir N. Strelnikov

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  1. Natalia B. Kondrashova
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  2. Artem Sh. Shamsutdinov
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  3. Viktor A. Valtsifer
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  4. Vladimir N. Strelnikov
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Correspondence to Artem Sh. Shamsutdinov.

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Kondrashova, N.B., Shamsutdinov, A.S., Valtsifer, V.A. et al. Surface Modification of Magnetic Mesoporous Systems with Aminopropyl Groups and Their Properties. J Inorg Organomet Polym 31, 1347–1358 (2021). https://doi.org/10.1007/s10904-020-01775-4

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  • DOI: https://doi.org/10.1007/s10904-020-01775-4

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