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The Synthesis of Maghemite Nanoparticles by Thermal Decomposition of Cryochemically Modified Iron(III) Acetylacetonate

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Moscow University Chemistry Bulletin Aims and scope

Abstract

Maghemite nanoparticles of 40 to 150 nm are obtained by the thermal decomposition of preliminarily cryochemically modified iron acetylacetonate. The composition and structure of the obtained particles and cryomodified precursor salt are determined by the X-ray diffraction (XRD) analysis, thermoanalytical methods (thermogravimetry, differential scanning calorimetry), infrared spectroscopy, and transmission electron microscopy.

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REFERENCES

  1. Hwang, S., Umar, A., Dar, G., Kim, S.H., and Badran, R., Sensor Appl.Sensor Lett., 2014, vol. 5, p. 97.

    Article  Google Scholar 

  2. Long, N.V., Teranishi, T., Yang, Y., Thi, C., Cao, Y., and Nogami, M., Int. J. Metall. Mater. Eng., 2015, vol. 1, p. 119.

    Article  Google Scholar 

  3. Vallabani, N.V.S. and Singh, S., Biotech, 2018, vol. 8, p. 279.

    Google Scholar 

  4. Fu, C. and Ravindra, N., Bioinspired,Biomimetic Nanobiomater., 2012, vol. 1, no. 4, p. 229.

    Article  CAS  Google Scholar 

  5. Leong, S.S., Yeap, S.P., and Lim, J.K., Interface Focus, 2016, vol. 6, no. 6, 20160048.

    Article  Google Scholar 

  6. Sumpter, B.G., Dave, P.N., and Chopda, L.V., J. Nanotech., 2014, 398569. https://www.hindawi.com/journals/ jnt/2014/398569.

  7. Arias, L.S., Pessan, J.P., Vieira, A.P.M., Lima, T.M.T., Delbem, A.C.B., and Monteiro, D.R., Antibiotics (Basel, Switz.), 2018, vol. 7, no. 2, p. 46

  8. Ansari, S.A.M.K., Ficiara, E., Ruffinatti, F.A., Stura, I., Argenziano, M., Abollino, O., Cavalli, R., Guiot, C., and D’Agata, F., Materials (Basel, Switz.), 2019, vol. 12, no. 3, p. 465.

  9. Rostovshchikova, T.N., Smirnov, V.V., Tsodikov, M.V., Bukhtenko, O.V., and Maksimov, Yu.V., Kiseleva, O.I., Pankratov, D.A, Russ. Chem. Bull., 2005, vol. 54, p. 1418.

    Article  CAS  Google Scholar 

  10. Rostovshchikova, T., Smirnov, V., Kiseleva, O., Yushcenko, V., Tzodikov, M., Maksimov, Y., Suzdalev, I., Kustov, L., and Tkachenko, O., Catal. Today, 2010, vol. 152, nos. 1–4, p. 48.

    Article  CAS  Google Scholar 

  11. Moodley, P., Scheijen, F.J.E., Niemantsverdriet, J.W., and Thune, P.C., Catal. Today, 2010, vol. 154, nos. 1–2, p. 142.

    Article  CAS  Google Scholar 

  12. Hugounenq, P., Levy, M., Alloyeau, D., Lartigue, L., Dubois, E., Cabuil, V., Ricolleau, C., Roux, S., Wilhelm, C., Gazeau, F., and Bazzi, R., J. Phys. Chem. C, 2012, vol. 116, p. 15702.

    Article  CAS  Google Scholar 

  13. Kurland, H.-D., Grabow, J., Staupendahl, G., Müller, F.A., Müller, E., Dutz, S., and Bellemann, M.E., J. Magn. Magn. Mater., 2009, vol. 321, p. 1381.

    Article  CAS  Google Scholar 

  14. Kurland, H.-D., Grabow, J., Dutz, S., Müller, E., Sierka, M., and Müller, F.A., Cryst. Growth Des., 2013, vol. 13, p. 4868.

    Article  Google Scholar 

  15. Timko, M., Molcan, M., Hashim, A., Skumiel, A., Müller, M., Gojzewski, H., Jozefczak, A., Kovac, J., Rajnak, M., Makowski, M., and Kopčanský, P., IEEE Trans. Magn., 2013, vol. 49, p. 250.

    Article  Google Scholar 

  16. McBain, S., Yiu, H., and Dobson, J., Int. J. Nanomed., 2008, vol. 3, p. 169.

    CAS  Google Scholar 

  17. Shabatina, T.I., Vernaya, O.I., Nuzhdina, A.V., Zvukova, N.D., Semenov, A.M., Shabatin, V.P., Lozinskii, V.I., and Mel’nikov, M.Ya., Nanotechnol. Russ., 2018, vol. 13, p. 182.

    Article  CAS  Google Scholar 

  18. Shabatina, T.I., Vernaya, O.I. Karlova, D.L., Nuzhdina, A.V., Shabatin, V.P., Semenov, A.M., Lozinskii, V.I., and Mel’nikov, M.Ya., Nanotechnol. Russ., 2018, vol. 13, p. 546.

    Article  CAS  Google Scholar 

  19. Vernaya, O.I., Shabatin, V.P., Semenov, A.M., Shabatina, T.I., and Mel’nikov, M.Ya., Moscow Univ. Chem. Bull. (Engl. Transl.), 2020, vol. 75, no. 4, p. 258.

  20. Shabatina, T.I., Vernaya, O.I., Shabatin, V.P., Melnikov, M.Y., Semenov, A.M., and Lozinsky, V.I., Appl. Sci., 2020, vol. 10, no. 1, 170.

    Article  CAS  Google Scholar 

  21. Diaz-Acosta, D., Baker, J., Cordes, W., and Pulay, P., J. Phys. Chem. A, 2001, vol. 105, p. 238.

    Article  CAS  Google Scholar 

  22. Cornell, R.M. and Schwertmann, U., The Iron Oxides: Structure, Properties, Reactions, Occurrences and Uses, New York: Wiley, 2003, p. 147.

    Book  Google Scholar 

  23. Kolida, Yu.Ya., Antonova, A.S., Kropacheva, T.N., and Kornev, V.I., Vestn. Udmurt. Univ., 2014, no. 4, p. 52.

  24. Kim, W., Suh, C.-Y., Cho, S.-W., Roh, K.-M., Kwon, H., Song, K., and Shon, I.-J., Talanta, 2012, vol. 94, p. 348.

    Article  CAS  Google Scholar 

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Funding

This work was supported by the Russian Science Foundation (project no. 16-13-10365-П).

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Authors and Affiliations

  1. Department of Chemistry, Moscow State University, 119991, Moscow, Russia

    O. I. Vernaya, A. S. Shumilkin, V. P. Shabatin, T. I. Shabatina & M. Ya. Melnikov

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  1. O. I. Vernaya
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  2. A. S. Shumilkin
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  3. V. P. Shabatin
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  4. T. I. Shabatina
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  5. M. Ya. Melnikov
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Correspondence to O. I. Vernaya.

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Translated by E. Boltukhina

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Vernaya, O.I., Shumilkin, A.S., Shabatin, V.P. et al. The Synthesis of Maghemite Nanoparticles by Thermal Decomposition of Cryochemically Modified Iron(III) Acetylacetonate. Moscow Univ. Chem. Bull. 75, 265–268 (2020). https://doi.org/10.3103/S0027131420050089

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  • DOI: https://doi.org/10.3103/S0027131420050089

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