Skip to main content
Log in

Laboratory Study on Evolution Mechanism of Nonmetallic Inclusions in Al-deoxidized Spring Steel

  • Original Article
  • Published:
Transactions of the Indian Institute of Metals Aims and scope Submit manuscript

Abstract

To explore the effect of refractory on the evolution of inclusions, laboratory experiments were conducted with MgO refractory utilizing electron probe X-ray microanalysis. Based on primary inclusions components, six types of inclusions were observed in the steel with MgO refractory: Al2O3, Al2O3–MgO, Al2O3–CaO, Al2O3–MgO–CaO, Al2O3–SiO2–CaO, and MgO inclusions. Al2O3 and Al2O3–MgO inclusions were the primary inclusions and mainly attributed to deoxidization products, with liquidus temperature exceeding 1600 °C. Al2O3–MgO–CaO inclusions resulted from coalescence between MgO and Al2O3–CaO inclusions as well as reduction of Al2O3–CaO by dissolved Mg. Dual-phase Al2O3–MgO–CaO inclusions were characterized by pure MgO cores surrounded by liquidus Al2O3–CaO layer, which was related to the substitution of dissolved Ca and Al in molten steel for MgO in inclusions.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3

(adapted from [29])

Fig. 4
Fig. 5
Fig. 6

(adapted from [28]): a T0; b M1; c M2; d M3; e M4

Fig. 7
Fig. 8

Similar content being viewed by others

References

  1. Suito H and Inoue R, ISIJ Int, 36(1996) 528

    Article  CAS  Google Scholar 

  2. Nishi T and Shinme K, Tetsu-to-Hagané, 84(1998) 837

    Article  Google Scholar 

  3. Itoh H, Hino M, and Ban-Ya S, Metall Mater Trans B, 28(1997) 953

    Article  Google Scholar 

  4. Suito H, Inoue H, and Inoue R, ISIJ Int 31(1991) 1381

    Article  CAS  Google Scholar 

  5. Tozawa H, Kato Y, Sorimachi K, Nakanishi T, ISIJ Int, 39(1999) 426

    Article  CAS  Google Scholar 

  6. Wasai K, Mukai K, and Miyanaga A, ISIJ Int, 42(2002) 459

    Article  CAS  Google Scholar 

  7. Park J H, Jung I H, and Lee H G, ISIJ Int, 46(2006) 1626

    Article  CAS  Google Scholar 

  8. Lowe J and Mitchell A, Clean Steel. Institute of Materials, London (1995)

    Google Scholar 

  9. Connolly Jr, H C and Burnett D, Geochimica et Cosmochimica Acta, 67(2003) 4429

    Article  CAS  Google Scholar 

  10. Holappa L, Hämäläinen M, Liukkonen M, Lind M, Ironmak Steelmak, 30(2003) 111

    Article  CAS  Google Scholar 

  11. Higuchi Y, Numata M, Fukagawa S, Shinme K, ISIJ Int, 36(1996) S151

    Article  Google Scholar 

  12. Brabie V, ISIJ Int, 36(1996) S109

    Article  Google Scholar 

  13. Brabie V, Steel Res Int, 68(1997) 54

    Article  CAS  Google Scholar 

  14. Jansson S, Brabie V, and Jönsson P, Ironmaking & Steelmaking, 33(2006) 389

    Article  CAS  Google Scholar 

  15. Deng Z and Zhu M, ISIJ Int, 53(2013) 450

    Article  CAS  Google Scholar 

  16. Beskow K and Sichen D, Ironmaking & Steelmaking, 31(2004) 393

    Article  CAS  Google Scholar 

  17. Pierard J, Sichen D, Jönsson P, Seetharaman S, Landin T Ironmak Steelmak, 25(1998) 5

    Google Scholar 

  18. Lee J W and Duh J G, J Mater Sci, 38(2003) 713

    Article  CAS  Google Scholar 

  19. Kong L, Deng Z, and Zhu M, Metall Mater Trans B, 49(2018) 1444

    Article  CAS  Google Scholar 

  20. Liu C, Huang F, and Wang X, Metall Mater Trans B, 47(2016) 999

    Article  CAS  Google Scholar 

  21. Okuyama G, Yamaguchi K, Takeuchi S, Sorimachi K I, ISIJ Int, 40(2000) 121

    Article  CAS  Google Scholar 

  22. Deng Z, Zhu M, and Sichen D, Metall Mater Trans B, 47(2016) 3158

    Article  CAS  Google Scholar 

  23. Liu C, Huang F, Suo J, Wang X, Metall Mater Trans B, 47(2016) 989

    Article  CAS  Google Scholar 

  24. Chi YG, ZY Deng, and MY Zhu, Steel Res Int, 88(2017) 1600470.

    Article  Google Scholar 

  25. Lyu S, Ma X, Huang Z, Yao Z, Lee HG, Jiang Z, Wang G, Zou J, Zhao B, Metall Mater Trans B, 50(2019) 2205

    Article  CAS  Google Scholar 

  26. Lyu S, Ma X, Huang Z, Yao Z, Lee HG, Jiang Z, Wang G, Zou J, Zhao B, Metall Mater Trans B, 50 (2019) 732

    Article  CAS  Google Scholar 

  27. Li J Z, Jiang M, He X F, Sun W, Wang X H, Metall Mater Trans B, 47(2016) 2386

    Article  CAS  Google Scholar 

  28. Kimura S, Nakajima K, and Mizoguchi S, Metall Mater Trans B, 32(2001) 79

    Article  Google Scholar 

  29. Sun Y H, Zeng Y N, Xu R, Cai K K, Int J Minerals Metall Mater, 21(2014) 1068

    Article  CAS  Google Scholar 

  30. Luo H, Scand J Metall, 30(2001) 212

    Article  CAS  Google Scholar 

  31. Park, J H and Todoroki H, ISIJ Int, 50(2010) 1333

    Article  CAS  Google Scholar 

  32. Song M, Nzotta M, and Sichen D, Steel Res Int, 80(2009) 753

    CAS  Google Scholar 

  33. Wang D, Li X, Wang H, Mi Y, Jiang M, Zhang Y, J Non-Crystalline Solids, 358(2012) 1196

    Article  CAS  Google Scholar 

  34. Chi Y, Deng Z, and Zhu M, Metall Mater Trans B, 49(2018) 440

    Article  CAS  Google Scholar 

  35. He S, Chen G, Guo Y, Shen B, Wang Q, Metall Mater Trans B, 46(2015) 585

    Article  CAS  Google Scholar 

  36. Jing G, Shu-Sen C, and Zi-Jian C, ISIJ Int, 53(2013) 2142

    Article  Google Scholar 

  37. Ye G, Jönsson P, and Lund T, ISIJ Int, 36(1996) S105

    Article  Google Scholar 

  38. Ito Y I, Suda M, Kato Y, Nakato H, Sorimachi K I, ISIJ Int, 36(1996) S148

    Article  Google Scholar 

  39. Yang W, Zhang L, Wang X, Ren Y, Liu X, Shan Q, ISIJ Int, 53(2013) 1401

    Article  CAS  Google Scholar 

  40. Jiang M, Wang X, Chen B, Wang W, ISIJ Int, 50(2010) 95

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Sha Lyu.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Wu, S., Guo, X., Wang, Y. et al. Laboratory Study on Evolution Mechanism of Nonmetallic Inclusions in Al-deoxidized Spring Steel. Trans Indian Inst Met 73, 2807–2816 (2020). https://doi.org/10.1007/s12666-020-02067-8

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s12666-020-02067-8

Keywords

Navigation