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Studying Thermally Reduced Graphene Oxide by X-Ray Photoelectron Spectroscopy

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The article is based on the materials of the Third Russian Conference “Graphene: molecule and 2D crystal”, 5–9 August 2019, Novosibirsk

Abstract

Samples of thermally reduced graphene oxide are studied using differential cross sections for photoelectron inelastic energy losses. We compare different procedures for recovering cross sections from the photoelectron energy spectra resulting from multiple inelastic scattering. It is shown that the cross section for inelastic energy losses (which uniquely characterizes allotropes of carbon) in the sample containing the minimal amount of carbon oxides corresponds the best to pyrolytic graphite.

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References

  1. S. Stankovich, D. A. Dikin, R. D. Piner, K. A. Kohlhaas, A. Kleinhammes, Y. Jia, Y. Wu, S. T. Nguyen, and R. S. Ruoff. Carbon, 2007, 45, 1558–1565.

    Article  CAS  Google Scholar 

  2. H. Yamaguchi, G. Eda, C. Mattevi, H. Kim, and M. Chhowalla. ACS Nano, 2010, 4, 524–528.

    Article  CAS  PubMed  Google Scholar 

  3. D. Li, M. B. Müller, S. Gilje, R. B. Kaner, and G. G. Wallace. Nat. Nanotechnol., 2008, 3, 101–105.

    Article  CAS  PubMed  Google Scholar 

  4. H. Chen, M. B. Müller, K. J. Gilmore, G. G. Wallaceet, and D. Li. Adv. Mater., 2008, 20, 3557–3561.

    Article  CAS  Google Scholar 

  5. I. K. Moon, J. Lee, R. S. Ruoff, and H. Lee. Nat. Commun., 2010, 1, 1–6.

    Google Scholar 

  6. O. C. Compton, D. A. Dikin, K. W. Putz, L. C. Brinson, and S. T. Nguyen. Adv. Mater., 2010, 22, 892–896.

    CAS  Google Scholar 

  7. O. Okhay, G. Gonçalves, A. Tkach, C. Dias, J. Ventura, M. F. R. Silva, L. M. V. Gonçalves, and E. Titus. J. Appl. Phys., 2016, 120, 051706.

    Article  Google Scholar 

  8. K. Yin, H. Li, Y. Xia, H. Bi, J. Sun, Z. Liu, and L. Sun. Nano-Micro Lett., 2011, 3(1), 51–55.

    Article  CAS  Google Scholar 

  9. N. D. K. Tu, J. Choi, C. R. Park, and H. Kim. Chem. Mater., 2015, 27(21), 7362–7369.

    Article  Google Scholar 

  10. S. Eigler, C. Dotzer, A. Hirsch, M. Enzelberger, and P. Müller. Chem. Mater., 2012, 24, 1276–1282.

    Article  CAS  Google Scholar 

  11. P. Cui, J. Lee, E. Hwang, and H. Lee. Chem. Commun., 2011, 47, 12370–12372.

    Article  CAS  Google Scholar 

  12. M. J. McAllister, J. Li, D. H. Adamson, H. C. Schniepp, A. A. Abdala, J. Liu, M. Herrera-Alonso, D. L. Milius, R. Car, R. K. Prud’homme, and I. A. Aksay. Chem. Mater., 2007, 19, 4396–4404.

    Article  CAS  Google Scholar 

  13. S. H. Huh. In: Physics and Applications of Graphene — Experiments. 2011. DOI: https://doi.org/10.5772/14156.

  14. P. V. Kumar, N. M. Bardhan, S. Tongay, J. Wu, A. M. Belcher, and J. C. Grossman. Nat. Chem., 2014, 6, 151–158.

    Article  CAS  PubMed  Google Scholar 

  15. G. S. Bocharov, A. V. Eletskii, and V. P. Mel’nikov. Nanosyst.: Phys., Chem., Math., 2018, 9(1), 98–101.

    CAS  Google Scholar 

  16. G. S. Bocharov and A. V. Eletskii. J. Struct. Chem., 2018, 59, 806–814.

    Article  CAS  Google Scholar 

  17. S. Eigler, C. Dotzer, A. Hirsch, M. Enzelberger, and P. Müller. Chem. Mater., 2012, 24, 1276–1282.

    Article  CAS  Google Scholar 

  18. V. P. Afanas’ev, G. S. Bocharov, A. S. Gryazev, A. V. Eletskii, P. S. Kaplya, and O. Y. Ridzel. J. Phys.: Conf. Ser., 2018, 1121, 012001.

    Google Scholar 

  19. V. P. Afanas’ev, G. S. Bocharov, A. V. Eletskii, O. Yu. Ridzel, and P. S. Kaplya, M. Koeppen. J. Vac. Sci. Technol., B: Nanotechnol. Microelectron.: Mater., Process., Meas., Phenom., 2017, 35(4), 041804.

    Google Scholar 

  20. S. Tougaard. J. Vac. Sci. Tech. A., 1996, 14, 1415.

    Article  CAS  Google Scholar 

  21. W. S. Hummers and R. E. Offeman. J. Am. Chem. Soc., 1958, 80, 1339.

    Article  CAS  Google Scholar 

  22. V. P. Afanas’ev, O. Yu. Golovina, A. S. Gryazev, D. S. Efremenko, and P. S. Kaplya. J. Vac. Sci. Technol., B: Nanotechnol. Microelectron.: Mater., Process., Meas., Phenom., 2015, 33, 03D101.

    Google Scholar 

  23. S. Tougaard and J. Kraaer. Phys. Rev. B, 1991, 43(2), 1651.

    Article  CAS  Google Scholar 

  24. S. Doniach and M. Sunjic. J. Phys. C: Solid State Phys., 1970, 3(2), 285.

    Article  CAS  Google Scholar 

  25. V. P. Afanas’ev, D. S. Efremenko, and A. V. Lubenchenko. J. Surf. Invest.: X-Ray, Synchrotron Neutron Tech., 2011, 5(2), 375–382.

    Article  Google Scholar 

  26. J. F. Moulder, W. F. Stickle, P. E. Sobol, and K. D. Bomben. Handbook of X-Ray Photoelectron Spectroscopy. Physical Electronics: Eden Prairie, MN, 1995.

    Google Scholar 

  27. V. P. Afanas’ev, A. S. Gryazev, D. S. Efremenko, P. S. Kaplya, and N. V. Lyapunov. J. Surf. Invest.: X-Ray, Synchrotron Neutron Tech., 2016, 10(5), 906–911.

    Article  Google Scholar 

  28. N. Pauli, M. Novak, and S. Tougaard. Surf. Interface Anal., 2013, 45, 811.

    Article  Google Scholar 

  29. T. Eberlein, U. Bangert, R. R. Nair, R. Jones, M. Gass, and A. L. Bleloch. Phys. Rev. B, 2008, 77, 233406.

    Article  Google Scholar 

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Funding

This work was performed as part of the State Contract No. 3.1414.2017/4.6.

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Correspondence to G. S. Bocharov.

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The authors declare that they have no conflict of interests.

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Russian Text © The Author(s), 2020, published in Zhurnal Strukturnoi Khimii, 2020, Vol. 61, No. 5, pp. 845–852.

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Afanas’ev, V.P., Gryazev, A.S., Bocharov, G.S. et al. Studying Thermally Reduced Graphene Oxide by X-Ray Photoelectron Spectroscopy. J Struct Chem 61, 803–810 (2020). https://doi.org/10.1134/S0022476620050170

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  • DOI: https://doi.org/10.1134/S0022476620050170

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