Skip to main content

Advertisement

Log in

Mechanical Behavior Characterization of a Stainless Steel Dissimilar Metal Weld Interface : In-situ Micro-Tensile Testing on Carburized Martensite and Austenite

  • Research paper
  • Published:
Experimental Mechanics Aims and scope Submit manuscript

Abstract

Background

Stainless Steel Dissimilar Metal Welds (SS DMW) between low-alloy steel 18MND5 and austenitic 316L stainless steel are critical junctions in the currently operating reactors because of their heterogeneous microstructure and mechanical properties. The presence of a narrow hard layer of carburized martensite and austenite in the ferritic-austenitic interface creates an important hardness gradient which affects the crack behavior of the SS DMW.

Objective

In order to evaluate the plastic properties of this hard layer, a micro tensile testing method was developed.

Methods

Tensile specimens of 15 x 80 x 6 μm were extracted from the martensitic and carburized austenitic layers by focused ion beam (FIB) micro-processing and tested using an in-situ tensile testing device. A platinum FIB deposition was used to measure local strain in the specimen during the test through digital image correlation (DIC). Isotropic elasto-plastic constitutive laws for the martensite and carburized austenite were obtained from the true strain-stress curves calculated from the micro-tensile tests.

Results

It was found that the corresponding plastic properties were in a good agreement with nanoindentation measurements and with values obtained from macroscopic tensile tests on crossweld specimens machined perpendicularly to the ferritic-austenitic interface and characterized using laser beam local diameter measurements.

Conclusions

In-situ tensile testing is a promising technique for plastic behavior characterization of small scale materials and local hard layers in dissimilar metal welds.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14
Fig. 15
Fig. 16
Fig. 17
Fig. 18

Similar content being viewed by others

References

  1. Mas F (2014) Solidification and phase transformations in a dissimilar steel weld 18MND5/309L/308L : evolution of microstructure and mechanical properties. PhD. Grenoble University

  2. Mas F, Martin G, Lh́uissier P., Bréchet Y, Tassin C, Roch F, Todeschini P, Simare A (2016) Heterogeneities in local plastic flow behavior in a dissimilar weld between low-alloy steel and stainless steel. Mater Sci Eng A 667:156–170

    Article  Google Scholar 

  3. Mas F, Tassin C, Valle N, Robaut F, Charlot F, Yescas M, Roch F, Todeschini P, Bréchet Y (2016) Metallurgical characterization of coupled carbon diffusion and precipitation in dissimilar metal welds. J Mater Sci 51(10):4864–4879

    Article  Google Scholar 

  4. Gilles P, Robin V, Fontaine M (2009) Welding residual stress effect on dissimilar metal weld junction fracture. Conference: ICPVT

  5. Blouin A, Chapuliot S, Marie S, Niclaeys C, Bergheau J-M (2014) Brittle fracture analysis of dissimilar metal welds. Eng Fract Mech 131:58–73

    Article  Google Scholar 

  6. Faidy C (2004) Structural Integrity of dissimilar welds : ADIMEW project overview. In: Proceedings of PVP 2004 asme pressure vessel and piping conference, 2004, USA

  7. Gilles PH, Devaux J, Faidy C (2004) ADIMEW Project: Prediction of the ductile tearing of a cracked 16 dissimilar welded junction. In: Proceedings of PVP2004 ASME pressure vessel and piping conference, 2004, USA

  8. Klueh RL, King JF (1982) Austenitic stainless steel - ferritic steel weld joint failures. Weld J 61:302–311

    Google Scholar 

  9. Sun Z, Moisio T (1994) Weld metal/ferritic steel interface in laser welded austenitic/ferritic dissimilar steel joints. J Mater Sci Lett 13:802–805

    Article  Google Scholar 

  10. Gittos MF, Gooch TG (1992) The interface below stainless steel and nickel-alloy claddings. Welding Research Supplement, 461s–472s

  11. Duppont JN, Kusko CS (2007) Technical Note: Martensite formation in austenitic/ferritic dissimilar alloy welds. Welding Journal, 51s-54s

  12. Ornath F, Soudry J, Weiss BZ (1981) Weld pool segregation during the welding of low alloy steels with austenitic electrodes. Weld J 60:227–230

    Google Scholar 

  13. Ikawa H, Shin S, Inui M, Takeda Y, Nakano A (1972) On the martensitic-like structure at weld bond and the macroscopic segregation in weld metal in the welded dissimilar metals of α-steels and γ-steels. IIW Database, 1–33

  14. Kravtsov TG, Ikonnikov VI, Solyanik NK (1989) Structure of the metal in the fusion zone in depositing austenitic steel on pearlitic steel. Weld Int 3:200–202

    Article  Google Scholar 

  15. Pan C, Wang R, Gui J (1990) Direct TEM observation of microstructures of the austenitic/carbon steels welded joint. J Mater Sci 25:3281–3285

    Article  Google Scholar 

  16. Gauzzi F, Missori S (1988) Microstructural transformations in austenitic-ferritic transition joints. J Mater Sci 23:782– 789

    Article  Google Scholar 

  17. Murugan N, Parmar RS (1997) Effect of welding conditions on microstructure and properties of type 316L stainless steel submerged arc cladding. Welding Research Supplement, 210s–217s

  18. Swindeman RW, Boiling E (1989) Relaxation response of A533B Steel from 25 to 600°c. Metals and ceramics division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831

  19. Kiener D, Grosinger W, Dehm G, Pippan R (2008) A further step towards an understanding of size-dependent crystal plasticity: In-situ tension experiments of miniaturized single-crystal copper samples. Acta Mater 56:580–92

    Article  Google Scholar 

  20. Bhattacharyya D, Wheeler RW, Harrison RP, Edwards L (2014) The observation of slip phenomena in single crystal fe samples during in-situ Micro-Mechanical testing through orientation imaging. Microsc Microanal 20:1060–9

    Article  Google Scholar 

  21. Reichardt A, Ionescu M, Davis J, Edwards L, Harrison RP, Hosemann P, Bhattacharyya D (2015) In situ micro tensile testing of He+ 2 ion irradiated and implanted single crystal nickel film. Acta Mater 100:147–154

    Article  Google Scholar 

  22. Vo HT, Reichardt A, Frazer D, Bailey N, Chou P, Hosemann P (2017) In situ micro-tensile testing on proton beam-irradiated stainless steel. J Nucl Mater 493:336–342

    Article  Google Scholar 

  23. Katsuhiko F, Fukuya K (2011) Development of micro tensile method in an FIB system for evaluating grain boundary strength. Mater Trans 52:20–24

    Article  Google Scholar 

  24. Ancelet O, Matheron P (2010) Development of a new measurement system for tensile testing. PVP2010-25667, Bellevue; 2010

  25. Ben Salem G (2019) Brittle fracture of stainless steel dissimilar metal welds in the brittle-to-ductile transition range. PhD. Paris Saclay University

  26. Giannuzzi LA, Michael JR (2012) Ion channelling vs. electron channelling image contrast. Microsc Microanal 18:694–695

    Article  Google Scholar 

  27. Prasath Babu R, Irukuvarghula S, Harte A, Preuss M (2016) Nature of gallium focused ion beam induced phase transformation in 316L austenitic stainless steel. Acta Mater 120:391–402

    Article  Google Scholar 

  28. Basa A, Thaulow C, Barnoush A (2013) Chemically induced phase transformation in austenite by focused ion beam. Metall Mater Trans A 45(3):1189–1198

    Article  Google Scholar 

  29. Knipling KE, Rowenhorst DJ, Fonda RW, Spanos G (2010) Effects of focused ion beam milling on austenite stability in ferrous alloys. Mater Charact 61(1):1–6

    Article  Google Scholar 

  30. Bourcier M, Bornert M, Dimanov A, Héripré E, Raphanel JL (2013) Multiscale experimental investigation of crystal plasticity and grain boundary sliding in synthetic halite using digital image correlation. J Geophys Res Sol Earth 118(2):511–526

    Article  Google Scholar 

  31. Allais L, Bornert M, Bretheau T, Caldemaison D (1994) Experimental characterization of the local strain field in a heterogenous elastoplastic material. Acta metall mater 42(11):3865– 3880

    Article  Google Scholar 

  32. www.cast3m.cea.fr

  33. Bucaille JL, Stauss S, Felder E, Michler J (2003) Determination of plastic properties of metals by instrumented indentation using different sharp indenters. Acta Mater 51:1663–1676

    Article  Google Scholar 

  34. Hosemann P, Kiener D, Wang Y, Maloy SA (2012) Issues to consider using nanoindentation on shallow ion beam irradiated materials. J Nucl Mater 425:136–9

    Article  Google Scholar 

  35. Kasada R, Takayama Y, Yabuuchi K, Kimura A (2011) A new approach to evaluate irradiation hardening of ion-irradiated ferritic alloys by nano-indentation techniques. Fusion Eng Des 86:2658–61

    Article  Google Scholar 

  36. Weaver JS, Pathak S, Reichardt A, Vo HT, Maloy SA, Hosemann P, Mara NA (2017) Spherical nanoindentation of proton irradiated 304 stainless steel: a comparison of small scale mechanical test techniques for measuring irradiation hardening. J Nucl Mater 493:368–379

    Article  Google Scholar 

Download references

Acknowledgments

This work was carried out within the MATMECA consortium and supported by the ANR under contract number ANR-10-EQPX-37.

The presented study was sponsored by Framatome with the participation of the MSSMat and CEA/LISN laboratories. The authors wish to express their gratitude to all the partners who contributed in this work, especially Olivier Ancelet and Gregory Perez (CEA/LISN) for their help and contribution in the experimental program on the DMW mock-up, Éric Perrin and Frédéric Douit (MSSMat) for their great participation in the in-situ tensile testing machine development and all the Material research team of MSSMat for their helpful advices.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to G. Ben Salem.

Ethics declarations

Conflict of interests

The authors declare that they have no conflict of interest.

Additional information

Publisher’s Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Ben Salem, G., Héripré, E., Bompard, P. et al. Mechanical Behavior Characterization of a Stainless Steel Dissimilar Metal Weld Interface : In-situ Micro-Tensile Testing on Carburized Martensite and Austenite. Exp Mech 60, 1037–1053 (2020). https://doi.org/10.1007/s11340-020-00633-1

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11340-020-00633-1

Keywords

Navigation