Skip to main content
Log in

Microstructural properties and compressive strength of lime or/and cement solidified silt: a multi-scale study

  • Original Paper
  • Published:
Bulletin of Engineering Geology and the Environment Aims and scope Submit manuscript

Abstract

Because of its poor engineering properties, silt often needs to be treated to meet the design requirements. Solidification using binder is one of the most common methods to improve the engineering properties of silt. Lime or/and cement are often used to treat silt. However, the mechanical properties of soil are closely related to its microstructure. Although much research has been done on the mechanical properties and stabilization mechanism of lime or/and cement solidified silt, the multi-scale research between the microstructure and macroscopic mechanics properties of solidified silt has received no attention. Therefore, in this paper, unconfined compression, mercury intrusion, and scanning electron microscope (SEM) tests were conducted on lime, cement, and lime and cement mixtures (LC) solidified silt. The microstructure parameters of particle, pore, and contact zone were extracted from SEM images. Meanwhile, the effect of curing time and binder dosage on the microstructure parameters was analyzed. In addition, the relationship between micro-parameters and macro-mechanical strength was established. The results showed that the particle diameter, particle area, contact zone diameter, and contact zone area increased with increasing curing time and binder dosage, while the pore ratio, fractal dimension of particle size distribution (PSD), and fractal dimension of contact zone size distribution (CZSD) decreased with increasing binder dosage. The unconfined compressive strength (UCS) decreased with the increase of particle roundness, pore area, pore diameter, pore ratio, and fractal dimension of PSD, and increased with increasing fractal dimension of pore size distribution (PPSD). In addition, there were no obvious relationships between UCS and pore roundness, contact zone area, and fractal dimension of CZSD.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14
Fig. 15
Fig. 16
Fig. 17
Fig. 18
Fig. 19
Fig. 20
Fig. 21
Fig. 22
Fig. 23

Similar content being viewed by others

Abbreviations

A g :

Particle area

R g :

Particle roundness

A p :

Pore area

R p :

Pore roundness

A c :

Area of contact zone

R c :

Roundness of contact zone

q u :

Unconfined compression strength

PSD:

Particle size distribution

PPSD:

Pore size distribution

n p :

Pore area ratio from SEM images

D g :

Particle diameter

FD g :

Fractal dimension of particle size distribution

D p :

Pore diameter

FD p :

Fractal dimension of pore size distribution

D c :

Diameter of contact zone

FD c :

Fractal dimension of contact zone size distribution

IPP:

Image Pro Plus

CZSD:

Contact zone size distribution

LC:

Lime and cement mixtures

References

  • Anderson AN, Mcbratney AB, Fitzpatrick EA (1996) Soil mass, surface, and spectral fractal dimensions estimated from thin section photographs. Soil Sci Soc America J 60:962–969

    Google Scholar 

  • ASTM (2002) ASTM designation D4404. Standard test method for determination of pore volume and pore volume distribution of soil and rock by mercury intrusion porosimetry. In: Annual book of ASTM standards

  • ASTM (2008) Standard test method for unconfined compressive strength index of chemical-grouted soils. ASTM standard D4219-08. American society for testing and materials, west Conshohocken, Pa

  • ASTM (2012) D698-12, standard test methods for laboratory compaction of soil standard effort. ASTM International, West Conshohocken, ASTM International, West Conshohocken, Pennsylvania

    Google Scholar 

  • ASTMD (2010) Standard test methods for liquid limit, plastic limit and plasticity index of soils, ASTM International, West Conshohocken, Pennsylvania

  • Benavente N, Pina P (2009) Morphological segmentation and classification of marble textures at macroscopical scale. COMPUT GEOSCI-UK 35:1194–1204

    Google Scholar 

  • Bouazza A, Kwan PS, Chapman G (2004) strength properties of cement treated Coode Island silt by the soil mixing method. In: GeoTrans 2004

  • Bushell GC, Yan YD, Woodfield D, Raper J, Amal R (2002) On techniques for the measurement of the mass fractal dimension of aggregates. ELSEVIER, Netherlands, p 1

    Google Scholar 

  • Cai G, Tao Z, Liu S, Li J, Jie D (2014) Stabilization mechanism and effect evaluation of stabilized silt with lignin based on laboratory data. Mar Georesour Geotechnol 34:1390578475

    Google Scholar 

  • Cotecchia F, Guglielmi S, Cafaro F, Gens A (2019) Characterisation of the multi-scale fabric features of high plasticity clays. pp 361-368

  • Dal Ferro N, Sartori L, Simonetti G, Berti A, Morari F (2014) Soil macro- and microstructure as affected by different tillage systems and their effects on maize root growth. Soil Tillage Res 140:55–65

    Google Scholar 

  • Dathe A, Eins S, Niemeyer J, Gerold G (2001) The surface fractal dimension of the soil–pore interface as measured by image analysis. Geoderma 103:229

    Google Scholar 

  • Deneele D, Le Runigo B, Cui Y, Cuisinier O, Ferber V (2016) Experimental assessment regarding leaching of lime-treated silt. Constr Build Mater 112:1032–1040

    Google Scholar 

  • Dougan LT, Addison PS (2001) Estimating the cut-off in the fractal scaling of fractured concrete. PERGAMON PRESS, Great Britain, p 1043

    Google Scholar 

  • Dudoignon P, Gélard D, Sammartino S (2004) Cam-clay and hydraulic conductivity diagram relations in consolidated and sheared clay-matrices. Clay Miner 39:267–279

    Google Scholar 

  • Ferber V, Auriol JC, Magnan JP, Cui YJ, De Laure E, Gerente C (2006) A microstructural model for the volume changes of unsaturated clayey soils due to wetting. Reston, Va.; [Great Britain]:; American Society of Civil Engineers. P 861

  • Fernández-Martínez M, Sánchez-Granero MA (2016) A new fractal dimension for curves based on fractal structures. Topol Appl 203:108–124

    Google Scholar 

  • Gantzer CJ, Anderson SH (2002) Computed tomographic measurement of macroporosity in chisel-disk and no-tillage seedbeds. Soil Tillage Res 64:101–111

    Google Scholar 

  • Ghalehjough BK, Akbulut S, Celik S (2017) Experimental and numerical investigation on bearing capacity of granular soil affected by particle roundness. Indian J Mar Sci 46:2137–2145

    Google Scholar 

  • Giménez D, Allmaras RR, Nater EA, Huggins DR (1997) Fractal dimensions for volume and surface of interaggregate pores—scale effects. Geoderma 77:19–38

    Google Scholar 

  • H WZ, H X (2003) Direct estimation of the fractal dimensions of a fracture surface of rock. Surface Review and Letters (SRL):751

  • Hu R, Yeung M, Lee C, Wang S (2001) Mechanical behavior and microstructural variation of loess under dynamic compaction. Eng Geol 59:203–217

    Google Scholar 

  • Ikhlef NS, Ghembaza MSN, Dadouch M (2015) Effect of treatment with cement on the mechanical characteristics of silt from Telagh region of Sidi Belabes, Algeria. Geotech Geol Eng 33:1067–1079

    Google Scholar 

  • Jiao K, Yao S, Liu C, Gao Y, Wu H, Li M, Tang Z (2014) The characterization and quantitative analysis of nanopores in unconventional gas reservoirs utilizing FESEM–FIB and image processing: an example from the lower Silurian Longmaxi shale, upper Yangtze region, China. Int J Coal Geol 128-129:1–11

    Google Scholar 

  • Juang CH, Holtz RD (1986) A probabilistic permeability model and the pore size density function. Int J Numer Anal Methods Geomech 10:543–553

    Google Scholar 

  • Kikkawa N, Orense RP, Pender MJ (2013) Observations on microstructure of pumice particles using computed tomography. Can Geotech J 50:1109–1117

    Google Scholar 

  • Kim HM, Anderson SH, Motavalli PP, Gantzer CJ (2010) Compaction effects on soil macropore geometry and related parameters for an arable field. Geoderma 160:251

    Google Scholar 

  • Koerner RM (1970) Effect of particle characteristics on soil strength: R.M. Koerner. J. Soil Mech. Fndns. Div., Proc. ASCE96, SM 4, 1221–1234 (July 1970)

  • Kong X, Song S, Wang M, Zhao Q (2019) Experimental research of low liquid limit silt stabilized by lignin in the flooding area of Yellow River. Geotech Geol Eng 37:5211

    Google Scholar 

  • Krohn C, Thompson A (1986) Fractal sandstone pores: automated measurements using scanning-electron-microscope images. Phys Rev B 33:6366–6374

    Google Scholar 

  • Kumar R, Bhattacharjee B (2003) Porosity, pore size distribution and in situ strength of concrete. Cem Concr Res 33:155–164

    Google Scholar 

  • Leroueil S, Vaughan PR (1990) The general and congruent effects of structure in natural soils and weak rocks. Géotechnique 40(3):467–488

    Google Scholar 

  • Liang SH, Lu YD, Pan WS, Zhang XZ (2020) Study on microstructure of red clay in southern Guizhou province based on SEM. Water Resour Power 38(2) in Chinese

  • Liu ZB, Shi B, Inyang HI, Cai Y (2005) Magnification effects on the interpretation of SEM images of expansive soils. Eng Geol 78:89–94

    Google Scholar 

  • Liu C, Shi B, Zhou J, Tang C (2011a) Quantification and characterization of microporosity by image processing, geometric measurement and statistical methods: application on SEM images of clay materials. Appl Clay Sci 54:106

    Google Scholar 

  • Liu C, Shi B, Zhou J, Tang C (2011b) Quantification and characterization of microporosity by image processing, geometric measurement and statistical methods: application on SEM images of clay materials. 54:106

  • Matsushima T, Uesugi TKA, Nakano T (2004) Detection of 3-D irregular grain shape of Toyoura sand at SPring-8. In X-ray CT for Geomaterials. Soils, Concrete, Rocks:121–126

  • MCPRC (2009) Ministry of Communications of the People’s Republic of China. Test methods materials stabilized with inorganic binder materials for highway engineering. China communication press, Beijing

    Google Scholar 

  • Nez-Nistal AM, Veniale F, Setti M, Cotecchia F (1999) A scanning electron microscopy image processing method for quantifying fabric orientation of clay geomaterials

  • Pan LS, Zhou RC (2013) Microscopic features of mudstone based on SEM images. Durnten-Zurich; Trans Tech publications Ltd p 1130

  • Pan J, Niu Q, Wang K, Shi X, Li M (2016) The closed pores of tectonically deformed coal studied by small-angle X-ray scattering and liquid nitrogen adsorption. Microporous Mesoporous Mater 224:245–252

    Google Scholar 

  • Peng Z, Jing S (2017) Correlation relationship analysis of physical mechanics properties and pores microstructures

  • Penumadu D (1996) Evaluating clay microfabric using scanning electron microscopy and digital information processing. NATIONAL ACADEMY OF SCIENCES: United States. p 112

  • Peyton RL, Gantzer CJ, Anderson SH, Haeffner BA, Pfeifer P (1994) Fractal dimension to describe soil macropore structure using X ray computed tomography. Water Resour Res 30:691–700

    Google Scholar 

  • Pradhan B, Nagesh M, Bhattacharjee B (2005) Prediction of the hydraulic diffusivity from pore size distribution of concrete. Cem Concr Res 35:1724–1733

    Google Scholar 

  • Prakongkep N, Suddhiprakarn A, Kheoruenromne I, Gilkes RJ (2010) SEM image analysis for characterization of sand grains in Thai paddy soils. GEODERMA 156:20–31

    Google Scholar 

  • Pu SY, Zhu Z, Song W, Wang H, Wei R (2019a) Deformation properties of silt solidified with a new SEU-2 binder. pp 267-277

  • Pu SY, Zhu Z, Wang H, Song W, Wei R (2019b) Mechanical characteristics and water stability of silt solidified by incorporating lime, lime and cement mixture, and SEU-2 binder. Constr Build Mater

  • Pu SY, Zhu Z, Song W, Wan Y, Wang H, Xu X (2020a) Comparative study of compressibility and deformation properties of silt stabilized with lime, lime, and cement, and SEU-2 binder. Arab J Sci Eng:1

  • Pu SY, Zhu ZD ,Song WL, Wan Y,Wang HR, Song SG, Zhang J (2020b) Mechanical and microscopic properties of cement stabilized silt,KSCE Journal of Civil Engineering

  • Pusch R, Weston R (2003) Microstructural stability controls the hydraulic conductivity of smectitic buffer clay. Appl Clay Sci 23:35–41

    Google Scholar 

  • Qinghui L, Jiajia Y, Jian Z, Zhigang C (2016) Microstructure study on intact clay behavior subjected to cyclic principal stress rotation. Procedia Engineering 143:991–998

    Google Scholar 

  • Shen Y, Yang H, Xi J, Yang Y, Wang Y, Wei X (2020) A novel shearing fracture morphology method to assess the influence of freeze–thaw actions on concrete–granite interface

  • Shi B, Murakami Y, Wu Z (1998) Orientation of aggregates of fine-grained soil: quantification and application. Eng Geol 50:59–70

    Google Scholar 

  • Shi X, Pan J, Hou Q, Jin Y, Wang Z, Niu Q, Li M (2018) Micrometer-scale fractures in coal related to coal rank based on micro-CT scanning and fractal theory. FUEL 212:162–172

    Google Scholar 

  • Sivakumar V, Doran IG, Graham J (2002) Particle orientation and its influence on the mechanical behaviour of isotropically consolidated reconstituted clay

  • Tang YQ, Jie Z, Hong J, Ping Y, Wang JX (2012) Quantitative analysis of the microstructure of Shanghai muddy clay before and after freezing. Bull Eng Geol Environ 71:309–316

    Google Scholar 

  • Tao, Zhang, Songyu, Liu, Guojun, Cai, Anand, J., Puppala (2015) Experimental investigation of thermal and mechanical properties of lignin treated silt. Eng Geol

  • Tovey NK, Krinsley DH (1992) Mapping of the orientation of fine-grained minerals in soils and sediments. Bull Eng Geol Environ 46:93–101

    Google Scholar 

  • Yilmaz E, Belem T, Bussière B, Benzaazoua M (2011) Relationships between microstructural properties and compressive strength of consolidated and unconsolidated cemented paste backfills. Cem Concr Compos 33:702–715

    Google Scholar 

  • You Z, Lai Y, Zhang M, Liu E (2017) Quantitative analysis for the effect of microstructure on the mechanical strength of frozen silty clay with different contents of sodium sulfate. Environ Earth Sci 76:141–143

    Google Scholar 

  • Zhang ZL, Cui Z (2017) Analysis of microscopic pore structures of the silty clay before and after freezing–thawing under the subway vibration loading. Environ Earth Sci 76:528

    Google Scholar 

  • Zhang T, Cai G, Liu S, Puppala AJ (2016) Engineering properties and microstructural characteristics of foundation silt stabilized by lignin-based industrial by-product. KSCE J Civ Eng 20:2725–2736

    Google Scholar 

  • Zhou H, Wu JH (2017) Study of soil pore fractal features in the process of soil consolidation and its impact on permeability. Industrial Building 08:95–99

    Google Scholar 

  • Zhu ZD, Liu S (2008) Utilization of a new soil stabilizer for silt subgrade. Eng Geol 97:192–198

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding authors

Correspondence to Shaoyun Pu or Zhiduo Zhu.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Pu, S., Zhu, Z., Zhao, L. et al. Microstructural properties and compressive strength of lime or/and cement solidified silt: a multi-scale study. Bull Eng Geol Environ 79, 5141–5159 (2020). https://doi.org/10.1007/s10064-020-01910-y

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10064-020-01910-y

Keywords

Navigation