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Structural-Phase Transformations and Short-Range Order Evolution in the Fe–Cr System during Mechanical Alloying

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Abstract

Using Mössbauer spectroscopy on 57Fe nuclei and X-ray diffraction, the mechanism of mechanical alloying in a planetary ball mill of the Fe–Cr nanocrystalline system in a concentration range from 20 to 48 at % Cr has been studied in detail. It has been established that mechanical alloying occurs in one stage at a concentration of up to 30 at % Cr and in three stages at higher concentrations. The change in the mechanism of mechanical alloying occurs as iron is saturated with chromium and is caused by the inversion of the sign of the mixing energy from negative to positive.

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Funding

This work was carried out within the framework of the state task of the Ministry of Science and Higher Education of the Russian Federation AAAA-A17-117022250038-7 and with financial support from the Presidium of the Ural Branch of the Russian Academy of Sciences (project 18-10-2-21).

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Authors and Affiliations

  1. Udmurt Federal Research Center of the Ural Branch of the Russian Academy of Sciences, Izhevsk, Russia

    V. E. Porsev, A. L. Ulyanov & G. A. Dorofeev

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  1. V. E. Porsev
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  2. A. L. Ulyanov
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  3. G. A. Dorofeev
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Correspondence to V. E. Porsev.

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The authors declare that they have no conflicts of interest.

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Translated by N. Petrov

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Porsev, V.E., Ulyanov, A.L. & Dorofeev, G.A. Structural-Phase Transformations and Short-Range Order Evolution in the Fe–Cr System during Mechanical Alloying. Phys. Solid State 62, 1117–1125 (2020). https://doi.org/10.1134/S1063783420070203

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