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Identification of Intercalates and Grafted Organic Derivatives of H2La2Ti3O10 by Multinuclear NMR

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Abstract

Using 1H, 13C, and 15N NMR method, it was established that the formation of organic-inorganic hybrids of H2La2Ti3O10 with methylamine and butylamine produces intercalated alkylamino cations, while the introduction of methanol into the interlayer space of H2La2Ti3O10 is accompanied by the formation of covalent bonds.

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ACKNOWLEDGMENTS

This study was performed using the facilities of the Magnetic Resonance Research Center, Center for X-ray Diffraction Studies, Center for Thermogravimetric and Calorimetric Research, and Interdisciplinary Resource Center for Nanotechnology of the St. Petersburg State University.

Funding

This study was performed under financial support by the Russian Science Foundation (project no. 19-13-00 184).

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Authors and Affiliations

  1. St. Petersburg State University, 199034, St. Petersburg, Russia

    M. G. Shelyapina, I. P. Lushpinskaya, S. A. Kurnosenko, O. I. Silyukov & I. A. Zvereva

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  1. M. G. Shelyapina
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  2. I. P. Lushpinskaya
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  3. S. A. Kurnosenko
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  4. O. I. Silyukov
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  5. I. A. Zvereva
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Corresponding author

Correspondence to M. G. Shelyapina.

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No conflict of interest was declared by the authors.

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Shelyapina, M.G., Lushpinskaya, I.P., Kurnosenko, S.A. et al. Identification of Intercalates and Grafted Organic Derivatives of H2La2Ti3O10 by Multinuclear NMR. Russ J Gen Chem 90, 760–761 (2020). https://doi.org/10.1134/S1070363220040337

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  • DOI: https://doi.org/10.1134/S1070363220040337

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