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Licensed Unlicensed Requires Authentication Published by De Gruyter June 10, 2020

Microstructure of spray freezing dried powders affected by the presence of inert particles

  • Fan Zhang , Linsong Wang , Xiaoyu Ma , Qing Xu , Wei Tian and Zhanyong Li EMAIL logo

Abstract

Spray freeze-drying is a process to directly produce high quality powders with short drying time. The difference of microstructures has a great influence on the physical properties of powders. However, during the spray freeze-drying process, the freezing degree of droplets in the drying chamber will change the product structure and affect the powder quality. In this study, the surface structure and morphology of dry powders were observed using scanning electron microscopy. The formation mechanism of droplet morphology during spray freeze-drying was analyzed. The results show that the rapid freezing process can produce finer microstructures.


Corresponding author: Zhanyong Li, Tianjin Key Laboratory of Integrated Design and On-line Monitoring for Light Industry & Food Machinery and Equipment, College of Mechanical Engineering, Tianjin University of Science and Technology, Tianjin, 300222, China; Tianjin International Joint Research and Development Center of Low-Carbon Green Process Equipment, Tianjin, 300222, China, E-mail:

Award Identifier / Grant number: 31571906

  1. Author contribution: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.

  2. Research funding: The authors acknowledge the financial support of this project by the National Natural Science Foundation of China (Grant No. 31571906).

  3. Employment or leadership: None declared.

  4. Honorarium: None declared.

  5. Conflict of interest statement: The authors declare no conflicts of interest regarding this article.

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Received: 2019-11-08
Revised: 2020-04-01
Accepted: 2020-05-01
Published Online: 2020-06-10

© 2020 Walter de Gruyter GmbH, Berlin/Boston

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