Skip to main content
Log in

Quantitation of Si, B, Ca, Mg, Ba, and Zr in Complex-Alloyed Nickel Alloys by ICP-MS

  • Published:
Moscow University Chemistry Bulletin Aims and scope

Abstract

The possibility of the use of a collision and reaction cell is shown and the optimum parameters for its adjustment are selected for the determination of Si, B, Ca, Mg, Ba, and Zr in a complex-alloyed nickel alloy via inductively coupled plasma mass spectrometry (ICP-MS). The procedure of sample dissolution and its preparation for the analysis is presented. The correctness of the obtained results is confirmed by the analysis of the certified reference standard of a nickel alloy.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1.
Fig. 2.

Similar content being viewed by others

REFERENCES

  1. Kablov, E.N., Petrushin, N.V., Svetlov, I.L., and Demonis, I.M., Aviats. Mater. Tekhnol., 2012, no. 8, p. 36.

  2. Kablov, E.N., Petrushin, N.V., Svetlov, I.L., and Demonis, I.M., Tekhnol. Legk. Splavov, 2007, no. 2, p. 6.

  3. Shein, E.A., Tr.Vseross. Nauchno-Issled. Inst. Aviats. Mater., 2016, no. 3, art. ID 2. http://www.viam-works.ru. Accessed December 18, 2018. https://doi.org/10.18557/2307-6046-2016-0-3-2-2

  4. Min, P.G., Sidorov, V.V., and Vadeev, V.E., Tr.Vseross. Nauchno-Issled. Inst. Aviats. Mater., 2017, no. 4, art. ID 3. http://www.viam-works.ru. Accessed December 18, 2018. https://doi.org/10.18557/2307-6046-2017-0-4-3-3

  5. Min, P.G., Sidorov, V.V., Kablov, D.E., and Vadeev, V.E., Tr.Vseross. Nauchno-Issled. Inst. Aviats. Mater., 2017, no. 4, art. ID 4. http://www.viam-works.ru. Accessed December 18, 2018. https://doi.org/10.18557/2307-6046-2017-0-4-4-4.

  6. GOST (State Standard) 6689.7-92: Nickel, Nickel and Copper-Nickel Alloys. Methods for the Determination of Silicon, Moscow, 1993.

  7. GOST (State Standard) 51928-2002: Nickel-Based Fire-Resistant Alloys. Methods for the Determination of Boron, Moscow, 2003.

  8. GOST (State Standard) 6689.12-92: Nickel, Nickel and Copper-Nickel Alloys. Methods for the Determination of Magnesium, Moscow, 1993.

  9. GOST (State Standard) 6689.24-92: Nickel, Nickel and Copper-Nickel Alloys. Method for the Determination of Calcium, Moscow, 1993.

  10. Karachevtsev, F.N., Zagvozdkina, T.N., and Dvoretskov, R.M., Tr.Vseross. Nauchno-Issled. Inst. Aviats. Mater., 2015, no. 12, art. ID 7. http://www.viam-works.ru. Accessed December 18, 2018. https://doi.org/10.18557/2307-6046-2015-0-12-7-7

  11. Titov, V.I., Tr.Vseross. Nauchno-Issled. Inst. Aviats. Mater., 2017, no. 9, art. ID 12. http://www.viam-works.ru. Accessed December 18, 2018. https://doi.org/10.18557/2307-6046-2017-0-9-12-12

  12. Letov, A.F., Karachevtsev, F.N., and Zagvozdkina, T.N., Tr.Vseross. Nauchno-Issled. Inst. Aviats. Mater., 2018, no. 8, art. ID 9. http://www.viam-works.ru. Accessed December 18, 2018. https://doi.org/10.18557/2307-6046-2018-0-8-89-97

  13. Hu, J. and Wang, H., Microchim. Acta, 2001, vol. 137, p. 149.

    Article  CAS  Google Scholar 

  14. Leikin, A.Yu., Karandashev, V.K., Lisovskii, S.V., and Volkov, I.A., Inorg. Mater., 2015, vol. 51, no. 5, p. 1389.

    Article  CAS  Google Scholar 

  15. Zhang, P., Fu, L., Ma, J., and Tang, Y., J. Cent. South. Univ. (Engl. Ed.), 2015, no. 22, p. 37.

  16. Pupyshev, A.A. and Epova, E.N., Analitika Kontrol’, 2001, vol. 5, no. 4, p. 335.

    Google Scholar 

Download references

Funding

This work was financially supported by the Federal State Unitary Enterprise “All-Russian Scientific Research Institute of Aviation Materials,” a State Research Centre of the Russian Federation.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to A. V. Alekseev.

Ethics declarations

The authors declare that they have no conflict of interest.

Additional information

Translated by E. Boltukhina

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Alekseev, A.V., Yakimovich, P.V. & Proskurnina, E.V. Quantitation of Si, B, Ca, Mg, Ba, and Zr in Complex-Alloyed Nickel Alloys by ICP-MS. Moscow Univ. Chem. Bull. 75, 22–27 (2020). https://doi.org/10.3103/S0027131420010022

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.3103/S0027131420010022

Keywords:

Navigation