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Study of Polyphenol Components in Extracts of Arctic Brown Algae of Fucus vesiculosus Type by Liquid Chromatography and Mass-Spectrometry

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Abstract

The extraction of polyphenol component of arctic brown algae of the Fucus vesiculosus type and the subsequent fractionation of the extract by column chromatography on a Sephadex LH-20 adsorbent are carried out. The obtained fractions are characterized by size-exclusion chromatography, HPLC with UV and mass spectrometric detection (HPLC–UV-MS), and matrix-assisted laser desorption/ionization mass spectrometry (MALDI–MS). Using the MALDI–MS method, the presence of oligomeric compounds containing up to 13 phloroglucin structural units is detected. Using HPLC–UV-MS, oligomeric compounds in the mass range 374–870 Da (trimers–octamers) are detected, and their ratio is estimated.

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ACKNOWLEDGMENTS

This work was performed using instrumentation of the “Arktika” Core Facility Center of the Northern (Arctic) Federal University.

Funding

The work was carried out as part of the State Assignment of the Ministry of Education and Science of the Russian Federation in the field of scientific activity no. 4.3273.2017/PCh. Unique identifier RFMEFI59417X0013.

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Authors and Affiliations

  1. Lomonosov North (Arctic) Federal University, 163002, Arkhangel’sk, Russia

    D. V. Ovchinnikov, K. G. Bogolitsyn, A. S. Druzhinina, P. A. Kaplitsin, A. E. Parshina, I. I. Pikovskoi & O. Yu. Khoroshev

  2. Department of Chemistry, Moscow State University, 119991, Moscow, Russia

    P. N. Turova, A. N. Stavrianidi & O. A. Shpigun

Authors
  1. D. V. Ovchinnikov
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  2. K. G. Bogolitsyn
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  3. A. S. Druzhinina
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  4. P. A. Kaplitsin
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  5. A. E. Parshina
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  6. I. I. Pikovskoi
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  7. O. Yu. Khoroshev
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  8. P. N. Turova
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  9. A. N. Stavrianidi
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  10. O. A. Shpigun
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Corresponding author

Correspondence to D. V. Ovchinnikov.

Additional information

Translated by V. Kudrinskaya

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Ovchinnikov, D.V., Bogolitsyn, K.G., Druzhinina, A.S. et al. Study of Polyphenol Components in Extracts of Arctic Brown Algae of Fucus vesiculosus Type by Liquid Chromatography and Mass-Spectrometry. J Anal Chem 75, 633–639 (2020). https://doi.org/10.1134/S1061934820050147

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  • DOI: https://doi.org/10.1134/S1061934820050147

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