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Photoacoustic Spectroscopy for Curing Time Determination of an Acrylic Nanocomposite

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Abstract

Photoacoustic spectroscopy (PAS) has been widely used as a nondestructive and sensitive analytical technique used to determine the thermal diffusivity, effusivity and heat capacity of different materials. In this work, the open cell photoacoustic technique (OPC) technique was used for the kinematic study of heat transfer processes as a function of time for curing nanoresin composites. An exponential growth of the signal during the process of curing was observed. The nanoresin was based on silver nanoparticles (AgNPs) that were synthesized using a green method from an aqueous extract of Capsicum annuum var annuum as an Ag reducer and an acrylic resin. It was cured using a violet laser beam with a wavelength of 405 nm with an average power of 120 mW. The characteristic curing time was measured as a function AgNPs concentration of 0.0, 5.16, 7.27, 11.85, 14.50, 16.86 and 20.96 × 10−4 vol%. The results showed an increase in the curing time of composite resin containing the AgNPs compared to the pure resin. This study has applications in printing parts using laser stereolithography.

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Acknowledgements

We would like to thank CONACYT, COFAA and CGPI-IPN, México for their partial financial support and to ENCB: Microscopy Instrumentation Center, UPIITA: MATEA Group, and CINVESTAV: Physics Department, for their support in instrumental analysis. Also thanks to the Red Nanofotónica, for their partial financial support.

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Authors and Affiliations

  1. Unidad Profesional Interdisciplinaria en Ingeniería y Tecnología Avanzada-Instituto Politécnico Nacional, Av. Instituto Politécnico Nacional No. 2580, Col. Barrio la Laguna Ticomán, Del. Gustavo A. Madero, CP 07340, México, DF, Mexico

    J. L. Luna-Sánchez, J. L. Jiménez-Pérez & A. A. Castañeda-Galván

  2. CONACYT-Centro de Desarrollo de Productos Bióticos, Instituto Politécnico Nacional, Carretera Yautepec-Jojutla, Km. 6, calle CEPROBI No. 8, Col. San Isidro, Apartado Postal 24, C.P. 62731, Yautepec, Morelos, Mexico

    Z. N. Correa-Pacheco

  3. Departamento de Física, Centro de Investigación y de Estudios Avanzados, Instituto Politécnico Nacional, Av. Instituto Politécnico Nacional 2508 Col. San Pedro Zacatenco, CP 07360, Mexico, DF, Mexico

    M. Macías-Mier & A. Cruz-Orea

  4. Tecnológico Nacional de México, Instituto Tecnológico de Ciudad Cuauhtémoc, Av. Tecnológico # 137, C.P. 31500, Ciudad Cuauhtémoc, Chihuahua, Mexico

    R. Gutiérrez-Fuentes

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  1. J. L. Luna-Sánchez
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  2. J. L. Jiménez-Pérez
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  3. Z. N. Correa-Pacheco
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  4. M. Macías-Mier
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  5. A. Cruz-Orea
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Correspondence to J. L. Jiménez-Pérez.

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Luna-Sánchez, J.L., Jiménez-Pérez, J.L., Correa-Pacheco, Z.N. et al. Photoacoustic Spectroscopy for Curing Time Determination of an Acrylic Nanocomposite. Int J Thermophys 41, 99 (2020). https://doi.org/10.1007/s10765-020-02683-y

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  • DOI: https://doi.org/10.1007/s10765-020-02683-y

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