Skip to main content
Log in

Experimental and theoretical investigations about the nonlinear vibrations of rectangular atomic force microscope cantilevers immersed in different liquids

  • Original
  • Published:
Archive of Applied Mechanics Aims and scope Submit manuscript

Abstract

Nonlinear flexural vibrations of rectangular atomic force microscope cantilever have been investigated by both the theoretical model and experimental works. As for the theoretical model, the Timoshenko beam theory which takes the rotatory inertia and shear deformation effects into consideration has been adopted. To increase the accuracy of the theoretical model, all necessary details for cantilever and sample surface have been taken into account. Differential quadrature method as a simple and fast numerical method has been used for solving the differential equations. During the investigation, the softening behavior was observed for all cases. It was also seen that raising the amplitude of vibrations led to a decrease in the nonlinear resonant frequency to linear resonant frequency ratio. The effects of different parameters such as normal and lateral contact stiffness, cantilever thickness, the angle between cantilever and sample surface and tip height in the presence of air as environment on the softening behavior were also examined. It was also demonstrated that increasing the lateral and normal contact stiffness, but decreasing the Timoshenko beam parameter would lead to an increase in the amplitude of vibrations for the first and second modes. The vibrational behavior of cantilever immersed in different liquids including water, methanol, acetone and carbon tetrachloride has been studied. Results show that increasing the liquid density reduces the nonlinear frequency. Furthermore, experimental works were compared with theoretical model for water and air environments. Results show good agreement.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14
Fig. 15
Fig. 16
Fig. 17
Fig. 18
Fig. 19

Similar content being viewed by others

Abbreviations

A :

Area of the cross section

c :

Damping coefficient of the beam material

\(c_{a} \) :

Additional hydrodynamic damping

\(c_{\infty }\) :

Hydrodynamic damping when the cantilever is vibrating in free liquid

\(c_{s}\) :

Hydrodynamic damping when the cantilever is close to the surface

AFM:

Atomic force microscope

\(C_{ij}^{(n)} \) :

The weighting coefficients for the nth order derivative for the cantilever

d :

Distance between the lower edge of the cantilever and the centroid of the cross section

D:

Equilibrium tip–sample separation between the cantilever tip and the sample surface

E :

Young’s modulus

\(E_{\text {t}} \) :

Young’s modulus of the tip

\(E_{\text {s}} \) :

Young’s modulus of the sample

\(f_{\text {t}} ,f_{\text {n}} \) :

Interaction forces in tangential and normal directions of sample surface

\(f_{d} \) :

Hydrodynamic force

G :

Shear modulus

\(G_{\text {t}} \) :

Shear modulus of the tip

\(G_{\text {s}} \) :

Shear modulus of the sample

H :

Distance from the natural axis of the beam to the top of the tip

h(xt):

The transient distance between the cantilever and the surface

I :

Moment of the cross section

k :

Shear coefficient

\(k_{\text {c}}\) :

Cantilever contact stiffness

\(k_{n} ,k_{t} \) :

Linear normal and lateral contact stiffness of the sample surface

\(k_{n1} ,k_{n2} ,k_{t1} ,k_{t2} \) :

Nonlinear normal and lateral contact stiffness of the sample surface

kAG :

shear rigidity

\(m_{\text {tip}} \) :

tip mass

N :

The number of total discrete grid points in the domain

r :

Timoshenko beam parameter to describe the rotatory inertia effect

\(R_{\text {t}} \) :

Tip radius

s :

Parameter to describe the shear deformation effect

t :

Time

w :

Transverse deflection of the cantilever

\({\overline{w}} \) :

Dimensionless transverse deflection of the cantilever

x :

Longitudinal coordinate

y :

General transverse deflection of the cantilever

t :

Time

\({\overline{t}} \) :

Dimensionless time

\(Z_{\text {0}} \) :

Surface offset

\(\xi \) :

Longitudinal coordinate parameter for the cantilever

\(\alpha \) :

Angle between the cantilever and sample surface

\(\lambda \) :

Non-dimensional resonant frequency parameter

\(\rho \) :

Mass density

\(\rho _{\text {a}} \) :

Additional mass per length

\(\rho A \) :

Mass per unit length

\(\mu \) :

Dimensionless damping parameter

\(\varPhi \) :

Bending angle of the cantilever

\(\omega \) :

Circular resonant frequency

\(\sigma _{\text {n}} \) :

Nonlinear frequency to linear frequency ratio

\(\delta _{0} \) :

Static contact deformation

\(\eta \) :

Density of the liquid

\(\varLambda \) :

Normal contact stiffness relative to the cantilever stiffness

\(\nu \) :

Poisson’s ratio

\(\nu _{\text {t}} \) :

Poisson’s ratio of the tip

\(\nu _{\text {s}} \) :

Poisson’s ratio of the sample

References

  1. Binning, G., Quate, C.F., Gerber, C.: Atomic force microscope. Phys. Rev. Lett. 56(9), 930–933 (1986)

    Article  Google Scholar 

  2. Turner, J.A., Wiehn, J.S.: Sensitivity of flexural and torsional vibration modes of atomic force microscope cantilevers to surface stiffness variations. Nanotechnology 12(3), 322–330 (2001)

    Article  Google Scholar 

  3. Rabe, U., Janser, K., Arnold, W.: Vibration of free and surface-coupled atomic force microscope cantilevers. Rev. Sci. Instrum. 67(9), 3281–3293 (1996)

    Article  Google Scholar 

  4. Dupas, E., Gremaud, G., Kulik, A.: High-frequency mechanical spectroscopy with an atomic force microscope. Rev. Sci. Instrum. 72(10), 3891–3897 (2001)

    Article  Google Scholar 

  5. Chang, W.: Sensitivity of vibration modes of atomic force microscope cantilevers in continuous surface contact. Nanotechnology 13(4), 510–514 (2002)

    Article  Google Scholar 

  6. Lee, H.L., Chang, W.: Coupled lateral bending-torsional vibration sensitivity of atomic force microscope cantilever. Ultramicroscopy 108(8), 707–711 (2008)

    Article  Google Scholar 

  7. Chen, T.Y., Lee, H.L.: Damping vibration of scanning near-field optical microscope probe using the timoshenko beam model. Microelectron. J. 40(1), 53–57 (2009)

    Article  Google Scholar 

  8. Song, Y., Bhushan, B.: Finite-element vibration analysis of tapping-mode atomic force microscopy in liquid. Ultramicroscopy 107(10–11), 1095–1104 (2007)

    Article  Google Scholar 

  9. Payam, A.F.: Sensitivity of flexural vibration mode of the rectangular atomic force microscope micro cantilevers in liquid to the surface stiffness variations. Ultramicroscopy 135, 84–88 (2013)

    Article  Google Scholar 

  10. Kurt, M., Salvkin, I., Eriten, M., McFarlan, D.M., Gendelman, O.V., Bergman, A.L., Vakakis, A.F.: Effect of 1:3 resonances on the steady-state dynamics of a forced strongly nonlinear oscillator with a linear light attachment. Arch. Appl. Mech. 84(8), 1189–1203 (2014)

    Article  Google Scholar 

  11. Sadeghi, A.: A new investigation for double tapered atomic force microscope cantilevers by considering the damping effect. ZAMM J. Appl. Math. Mech. 95(3), 283–296 (2013)

    Article  MathSciNet  Google Scholar 

  12. Leibold, C., Muller, W.H.: Strain maps on statically bend (001) silicon microbeams using AFM-integrated Raman spectroscopy. Arch. Appl. Mech. 85(9–10), 1353–1362 (2015)

    Article  Google Scholar 

  13. Ghaderi, R., Nejat, A.: Nonlinear mathematical modeling of vibrating motion of nanomechanical cantilever active probe. Latin Am. J. Solids Struct. 11(3), 369–385 (2014)

    Article  Google Scholar 

  14. Ansari, R., Pourashraf, R., Gholami, R., Sahmani, S., Ashrafi, M.A.: Size-dependent resonant frequency and flexural sensitivity of atomic force microscope microcantilevers based on the modified strain gradient theory. Int. J. Optomech. 9(2), 111–130 (2015)

    Article  Google Scholar 

  15. Ahmadi, M., Ansari, R., Darvizeh, M., Rouhi, H.: Effects of fluid environment properties on the nonlinear vibrations of afm piezoelectric microcantilevers. Effects Fluid Environ. Properties Nonlinear Vib. AFM Piezoelectric Microcantilevers 50(2), 117–123 (2017)

    Google Scholar 

  16. Schmid M.: adapted from the IAP/TU Wien STM Gallery. from https://en.wikipedia.org/wiki/Scanning_tunneling_microscope, (2005)

  17. Zeng, C., Sullivan, V.C., Ma, X.: In situ atomic force microscopy studies on nucleation and self-assembly of biogenic and bio-inspired materials. J. Miner. 7(9), 158–176 (2017)

    Google Scholar 

  18. Timoshenko, S.P., Goodier, J.N.: Theory of Elasticity. McGraw- Hill, New York (1951)

    MATH  Google Scholar 

  19. Chen, G.Y., Warmack, R.J., Huang, A., Thundat, T.: Harmonic response of near-contact scanning force microscopy. J. Appl. Phys. 78(3), 1465 (1995)

    Article  Google Scholar 

  20. Hosaka, K., Itao, Kuroda, S.: Damping characteristics of beam-shaped micro-oscillators. Sens. Actuators A Phys. 49(1–2), 87–95 (1995)

    Article  Google Scholar 

  21. Song, Y., Bhushan, B.: Simulation of dynamic modes of atomic force microscopy using a 3D finite element model. Ultramicroscopy 106(8–9), 847–73 (2006)

    Article  Google Scholar 

  22. Derjaguin, B.V., Muller, V.M., Toporov, Y.P.: Adhesion of spheres: effect of contact deformations on the adhesion of particles. J. Colloid Interface Sci. 53(2), 314–326 (1975)

    Article  Google Scholar 

  23. Turner, J.A.: Non-linear vibrations of a beam with cantilever- Hertzian contact boundary conditions. J. Sound Vib. 275(1–2), 177–191 (2004)

    Article  Google Scholar 

  24. Korayem, M.H., Sharahi, H.J., Korayem, A.H.: Comparison of frequency response of atomic force microscopy cantilevers under tip-sample interaction in air and liquids. J. Sci. Iranica 19(1), 106–112 (2012)

    Article  Google Scholar 

  25. Sadeghian, H., Rezazadeh, G.: Comparison of generalized differential quadrature and galerkin methods for the analysis of micro-electro-mechanical coupled systems

  26. Zhong, H., GUO, Q.: Non-linear vibration analysis of timoshenko beam using the differential quadrature method. J. Non-linear Dyn. 32(3), 223–234 (2003)

    Article  Google Scholar 

  27. Shu, C.: Differential Quadrature and its Application in Engineering. Springer, Singapore (1999)

    Google Scholar 

  28. Yuta, P.A., Hurley, D.C., Turner, J.A.: Relationship between Q-factor and sample damping for contact resonance atomic force microscope measurement of viscoelastic properties. J. Appl. Phys. 109(9), 113528 (2011)

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Ali Sadeghi.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Pasha, A.H.G., Sadeghi, A. Experimental and theoretical investigations about the nonlinear vibrations of rectangular atomic force microscope cantilevers immersed in different liquids. Arch Appl Mech 90, 1893–1917 (2020). https://doi.org/10.1007/s00419-020-01703-5

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s00419-020-01703-5

Keywords

Navigation