Production of 5-hydroxymethylfurfural (HMF) from rice-straw biomass using a HSO3–ZSM-5 zeolite catalyst under assistance of sonication

Phan Huy Hoang; Nguyen Minh Dat; Thai Dinh Cuong; Duong Thanh Tung

doi:10.1039/D0RA02037K

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Production of 5-hydroxymethylfurfural (HMF) from rice-straw biomass using a HSO₃–ZSM-5 zeolite catalyst under assistance of sonication†

Phan Huy Hoang,

*^a Nguyen Minh Dat,^a Thai Dinh Cuong^a and Duong Thanh Tung^a

Author affiliations

* Corresponding authors

^a Hanoi University of Science & Technology, No.1 Dai Co Viet Street, Hanoi, Vietnam
E-mail: hoang.phanhuy@hust.edu.vn

Abstract

This work studied the application of sulfonated ZSM-5 zeolite, a bi-functional catalyst for conversion of biomass-derived glucose to HMF. Glucose hydrolysate was obtained by enzymatic hydrolysis of rice straw, that was pretreated by sodium hydroxide. Glucose hydrolysate was then subjected to a transformation reaction to achieve HMF using HSO₃–ZSM-5 zeolite under the assistance of sonication. The reaction conditions including solvent, temperature, catalyst dosage and reaction time were studied. Suitable conditions, which gave the highest yield of HMF of 54.1% have been found. The HSO₃–ZSM-5 zeolite presented a high catalytic efficiency for conversion of glucose to HMF, an important and useful intermediate in the chemical industry.

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Article information

DOI: https://doi.org/10.1039/D0RA02037K
Article type: Paper
Submitted: 03 Mar 2020
Accepted: 26 Mar 2020
First published: 02 Apr 2020
This article is Open Access

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RSC Adv., 2020,10, 13489-13495

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Production of 5-hydroxymethylfurfural (HMF) from rice-straw biomass using a HSO₃–ZSM-5 zeolite catalyst under assistance of sonication

P. H. Hoang, N. M. Dat, T. D. Cuong and D. T. Tung, RSC Adv., 2020, 10, 13489 DOI: 10.1039/D0RA02037K

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