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Effect of Ultrasonication on the Phase Composition of Hyrdoxyapatite Synthesized using a Hydrothermal Method

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Refractories and Industrial Ceramics Aims and scope

The effect of ultrasonication time after hydrothermal synthesis of hydroxyapatite (HA) using the precursor system Ca(NO3)2–(NH4)2HPO4–NH4OH on the phase composition and degree of crystallinity was examined. HA samples were studied using x-ray diffraction and FT-IR spectroscopy. The studies showed that ultrasonication regardless of the duration had no effect on the phase composition and degree of crystallinity of the synthesized HA samples. HA phase Ca10(PO4)6(OH)2 with 0.97 degree of crystallinity was present in all studied samples.

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Acknowledgement

The work was financially supported by the Ministry of Science and Higher Education of the Russian Federation (Project No. RFMEFI57517X0168).

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Authors and Affiliations

  1. National University of Science and Technology MISiS, Moscow, Russia

    A. G. Yudin, D. V. Lysov, K. O. Chuprunov, D. V. Leibo, E. A. Kolesnikov, D. V. Kuznetsov & I. A. Il’inykh

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  1. A. G. Yudin
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  2. D. V. Lysov
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  3. K. O. Chuprunov
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Correspondence to A. G. Yudin.

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Translated from Novye Ogneupory, No. 10, pp. 48 – 53, September, 2019.

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Yudin, A.G., Lysov, D.V., Chuprunov, K.O. et al. Effect of Ultrasonication on the Phase Composition of Hyrdoxyapatite Synthesized using a Hydrothermal Method. Refract Ind Ceram 60, 516–520 (2020). https://doi.org/10.1007/s11148-020-00396-1

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  • DOI: https://doi.org/10.1007/s11148-020-00396-1

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