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Magnetic nano-carbon core shell as potent mixed hemimicelle solid phase extraction strategy for determination of acrylamide from potato chips coupled by high-performance liquid chromatography

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Abstract

Magnetic nano-carbon core shell was applied as mixed hemimicelle magnetic solid phase extraction adsorbent to introduce a novel sample preparation method for determination of acrylamide from potato chips. Acrylamide is identified as neurotoxic, a probable human carcinogen (group 2A) compound. Effective extraction parameters such as type and amount of extracting solvent, type and amount of adsorbent, time of extraction and desorption, the effect of pH, time of ionic liquid loading on the adsorbent and stirring rate (rpm) were studied and optimized. Under optimized extraction conditions, a good linearity was observed in the concentration range of 100–1500 ng/g. Limit of detection was observed as 30 ng/g. Application of the proposed method was surveyed by analysis of some potato chips brands available in the local supermarkets. The satisfactory results with the recovery of 95.58% revealed that the proposed method could be applied in food analysis laboratories.

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Abbreviations

MNC:

Magnetic nano-carbon

LLE:

Liquid–liquid extraction

MNPs:

Magnetic nanoparticles

NPs:

Nanoparticles

SPME:

Solid phase micro-extraction

IL:

Ionic liquid

MSPE:

Magnetic solid phase extraction

DLLE:

Dispersive liquid–liquid micro-extraction

EFSA:

European food safety authority

IL-MNC:

Ionic liquid magnetic nano-carbon

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Acknowledgement

The authors sincerely appreciate Biotechnology Research Centre and Faculty of Nutrition and Food Science of Tabriz University of Medical Sciences for supporting the project.

Funding

This research did not receive any specific grant from funding agencies in the public, commercial or not-for-profit sectors. Conflict of interest: All the authors declare that there is no conflict of interest.

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Authors and Affiliations

  1. Biotechnology Research Centre and Student Research Committee, Tabriz University of Medical Science, Tabriz, Iran

    Arezou Taghvimi

  2. Food and Drug Safety Research Centre, Tabriz University of Medical Science, Tabriz, 51664, Iran

    Samin Hamidi

  3. Biotechnology Research Center, Faculty of Pharmacy, Tabriz University of Medical Science, Tabriz, Iran

    Yousef Javadzadeh & Siavoush Dastmalchi

  4. Faculty of Pharmacy, Near East University, P.O. Box 99138, Nicosia, Mersin 10, North Cyprus, Turkey

    Yousef Javadzadeh & Siavoush Dastmalchi

  5. Drug Applied Research Center and Department of Food Science and Technology, Faculty of Nutrition and Food Science, Tabriz University of Medical Science, Tabriz, Iran

    Mahnaz Tabibiazar

Authors
  1. Arezou Taghvimi
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  2. Samin Hamidi
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  3. Yousef Javadzadeh
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  4. Siavoush Dastmalchi
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  5. Mahnaz Tabibiazar
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Correspondence to Mahnaz Tabibiazar.

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Taghvimi, A., Hamidi, S., Javadzadeh, Y. et al. Magnetic nano-carbon core shell as potent mixed hemimicelle solid phase extraction strategy for determination of acrylamide from potato chips coupled by high-performance liquid chromatography. J IRAN CHEM SOC 17, 817–823 (2020). https://doi.org/10.1007/s13738-019-01811-2

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  • DOI: https://doi.org/10.1007/s13738-019-01811-2

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