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Magnetic Fe–Cr–Ni oxide alloy nano-belts prepared from the chemical decomposition of a stainless steel screw (a top-down approach): an efficient and cheap catalyst for multicomponent reactions

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Abstract

A new, cheap, and accessible method has been used for the preparation of nano-belts from the chemical decomposition (top-down approach) of a cheap stainless steel screw and found as an efficient magnetically recyclable nanocatalyst for the preparation of quinolines and 1,8-dioxo-octahydroxanthenes under mild reaction conditions. The nano-belts, Fe–Cr–Ni oxide alloy, was prepared in a two-step synthesis and characterized with various instrumental methods. Due to magnetic property of the screw (a ferritic-alloy), the resultant nano-belts is magnetic. Magnetic Fe–Cr–Ni alloy nano-belts were applied toward efficient preparation of quinolines and 1,8-dioxo-octahydroxanthenes under mild conditions. The catalyst could be readily recovered and recycled for several consecutive runs, while it suffers from a very low metal leaching and subsequently efficiency drop.

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Acknowledgements

The authors are grateful to the University of Birjand for financial support.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Sciences, University of Birjand, Birjand, 97175-615, Iran

    Milad Kazemnejadi, Atefeh Zeinali & Mohammad Ali Nasseri

  2. Razi Herbal Medicines Research Center, Lorestan University of Medical Sciences, Khorramabad, Iran

    Zeinab Sharafi

  3. Research Center, Sulaimani Polytechnic University, Sulaimani, 46001, Kurdistan Region, Iraq

    Boshra Mahmoudi

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  1. Milad Kazemnejadi
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  2. Zeinab Sharafi
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  3. Boshra Mahmoudi
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  4. Atefeh Zeinali
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  5. Mohammad Ali Nasseri
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Correspondence to Milad Kazemnejadi.

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Kazemnejadi, M., Sharafi, Z., Mahmoudi, B. et al. Magnetic Fe–Cr–Ni oxide alloy nano-belts prepared from the chemical decomposition of a stainless steel screw (a top-down approach): an efficient and cheap catalyst for multicomponent reactions. J IRAN CHEM SOC 17, 777–787 (2020). https://doi.org/10.1007/s13738-019-01814-z

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