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Construction and anion exchange of silver(I) complexes bearing 1,2,3-tris(isonicotinoyloxy)benzene

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Abstract

A new potentially tridentate ligand 1,2,3-tris(isonicotinoyloxy)benzene (L) was prepared, and its coordination chemistry with various silver(I) salts AgX (X− = BF4−, ClO4−, PF6−, and CF3SO3−) was investigated in order to elucidate the effects of counteranion size. Self-assembly of silver(I) salts with L afforded four complexes with 1:1 stoichiometries. The molecular structures with small counteranions (BF4−, ClO4−, and PF6−) showed 2-D networks whereas those with large counteranions (CF3SO3−) showed a 1-D network. These silver(I) compounds were fully characterized by infrared spectroscopy, elemental and thermal analyses, and single crystal X-ray diffraction. The role of the present counteranions in determining the structural motifs is discussed in these pages.

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Acknowledgements

This work was supported by the National Research Foundation of Korea (NRF) Grant funded by the Korean Government (2018R1C1B6002006) and research funds for newly appointed professors of Chonbuk National University in 2017.

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Authors and Affiliations

  1. Department of Chemistry Education and Institute of Fusion Science, Chonbuk National University, Jeonju, 54896, Korea

    Hyun Chul Jeong, Siyeon Min, Hansol Park & Tae Hwan Noh

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  1. Hyun Chul Jeong
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  2. Siyeon Min
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  3. Hansol Park
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  4. Tae Hwan Noh
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Correspondence to Tae Hwan Noh.

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Jeong, H.C., Min, S., Park, H. et al. Construction and anion exchange of silver(I) complexes bearing 1,2,3-tris(isonicotinoyloxy)benzene. Transit Met Chem 44, 763–770 (2019). https://doi.org/10.1007/s11243-019-00346-y

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  • DOI: https://doi.org/10.1007/s11243-019-00346-y

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