Abstract
A project to investigate space environment effects on specific materials with interest to remote sensing was initiated in 2016. The goal of the project is to better characterize changes in the optical properties of polymers found in multi-layered spacecraft insulation (MLI) induced by electron bombardment. Previous analysis shows that chemical bonds break and potentially reform when exposed to high energy electrons like those seen in orbit. These chemical changes have been shown to alter a material’s optical signature, among other material properties. This paper presents the initial experimental results of MLI materials exposed to various fluences of high energy electrons, designed to simulate a portion of the geosynchronous Earth orbit (GEO) space environment. In situ optical reflectivity measurements are presented before, during and after electron dosing. It is shown that the spectral profile of some of the tested materials changes as a function of electron dose. These results provide an experimental benchmark for analysis of aging effects on satellite systems which can be used to improve remote sensing and space situational awareness. They also provide preliminary analysis on those materials that are most likely to comprise the high area-to-mass ratio (HAMR) population of space debris in the geosynchronous orbit environment. Finally, the results presented in this paper serve as a proof of concept for simulated environmental aging of spacecraft polymers that should lead to more experiments using a larger subset of spacecraft materials.
Similar content being viewed by others
References
Bedard, M.D.: Using a physics-based reflection model to study the reddening effect observed in spectrometric measurements of artificial space objects. Paper presented at the advance Maui optical and space surveillance technologies conference, Maui
Aberkromby, K.J., Hamada, K., Guyote, M., Okada, J., Barker, E.: Remote and ground truth spectral measurement comparisons of FORMOSAT III. Paper presented at the advance Maui optical and space surveillance technologies conference, Maui
De Groh KK, Banks BA, Asmar OC, Yi GT, Mitchell GG, Guo A, Sechkar EA. Erosion Results of the MISSE 8 Polymers Experiment After 2 Years of Space Exposure on the International Space Station. NASA Technical Report NASA/TM-2017-219445 (2017);
Pippin HG, Normand E, B. Wolf SL, Kamenetzky R. Analysis of Metallized TeflonTM Thin-Film Materials Performance on Satellites. Journal of Spacecraft and Rockets. 2004 41 (3), 322–5;
Townsend JA, Hansen PA, Dever JA, de Groh KK, Banks BA, Wang L, He C. Hubble Space Telescope metallized Teflon (R) FEP thermal control materials: on-orbit degradation and post-retrieval analysis. High Performance Polymers. 1999, ;11 (1):81–99
Finckenor M. MISSE Thermal Control Materials with Comparison to Previous Flight Experiments. In AIP Conference Proceedings 2009, 1087 (1) 241–248
Engelhart, D.P., Plis, E., Humagain, S., Greenbaum, S., Ferguson, D., Cooper, R., Hoffmann, R.: Chemical and electrical dynamics of polyimide film damaged by Electron radiation. Ieee T Plasma Sci. 45(9), 2573–2577 (2017). https://doi.org/10.1109/tps.2017.2729516
Sun, Y.M., Zhu, Z.Y., Jin, Y.F., Liu, C.L., Wang, Z.G., Liu, J., Hou, M.D., Zhang, Q.X.: The effects of high electronic energy loss on the chemical modification of polyimide. Nucl. Instrum. & Methods Phys. Res. B-Beam Interactions with Materials and Atoms. 193, 214–220 (2002)
Wu, Y., Sun, C., Xiao, J., Li, R., Yang, D., He, S.: A study on the free-radical evolution and its correlation with the optical degradation of 170 keV proton-irradiated polyimide. Polym. Degrad. Stab. 95(7), 1219–1225 (2010). https://doi.org/10.1016/j.polymdegradstab.2010.03.033
Choi, H.S., Lee, J., Cho, K.S., Kwak, Y.S., Cho, I.H., Park, Y.D., Kim, Y.H., Baker, D.N., Reeves, G.D., Lee, D.K.: Analysis of GEO spacecraft anomalies: space weather relationships. Space Weather-the International Journal of Research and Applications. 9, (2011). https://doi.org/10.1029/2010sw000597
Ginet, G., O’Brien, T., Huston, S., Johnston, W., Guild, T., Friedel, R., Lindstrom, C., Roth, C., Whelan, P., Quinn, R.: AE9, AP9 and SPM: new models for specifying the trapped energetic particle and space plasma environment. Space Sci. Rev. 179(1–4), 579–615 (2013)
Mehnert, R.: Materials modification using electron beams. In: Misaelides, P. (ed.) Application of Particle and Laser Beams in Materials Technology, Vol. 283. Nato Advanced Science Institutes Series, Series E, Applied Sciences, pp. 557–580 (1995)
Meng, C., Fang, W., Jing, L., Hai-Bo, Z.: Charging dynamics of a polymer due to electron irradiation: a simultaneous scattering-transport model and preliminary results. Chin. Phys. B. 21(12), 127901 (2012)
Paulmier, T., Dirassen, B., Arnaout, M., Payan, D., Balcon, N.: Electric properties of space used polymers under high energy electron irradiation. In: Solid Dielectrics (ICSD), 2013 IEEE International Conference on 2013, pp. 788–791. IEEE
Engelhart, D.P., Plis, E., Ferguson, D., Cooper, R., Hoffmann, R.: Optical and Chemical Characterization of Polyimide in a GEO-Like Environment. Technical Paper: 2016 Advanced Maui Optical and Space Surveillance Technologies Conference (2016)
Plis, E., Engelhart, D.P., Barton, D., Cooper, R., Ferguson, D., Hoffmann, R.: Degradation of polyimide under exposure to 90keV electrons. Phys. Status Solidi. B-Basic Solid State Phys. 254(7), (2017a). https://doi.org/10.1002/pssb.201600819
Rahnamoun, A; Engelhart, D.P.; Humagain, S; Koerner, H; Plis, E.A.; Kennedy, W.J.; Cooper R; Greenbaum, S.G.; Ryan Hoffmann, R; van Duin, A.T.C. Chemical dynamics characteristics of Kapton polyimide damaged by electron beam irradiation. Polymer. In review.
M. Finckenor, D. Dooling.: Multilayer insulation material guidelines. In: NASA (ed.), vol. TP-1999-209263. vol. TP-1999-209263. TP-1999-209263, (1999)
Rodriguez, H., Aberkromby, M., Mulrooney, K.J., Baker, M.E.: Optical properties of multi-layered insulation. Paper presented at the advanced Maui optical and space surveillance technologies conference, Maui
Schildknecht, T., Musci, R., Ploner, M., Beutler, G., Flury, W., Kuusela, J., de Leon Cruz, J., de Fatima Dominguez Palmero, L.: Optical observations of space debris in GEO and in highly-eccentric orbits. Adv. Space Res. 34(5), 901–911 (2004). https://doi.org/10.1016/j.asr.2003.01.009
Fukugita, M., Ichikawa, T., Gunn, J.E., Doi, M., Shimasaku, K., Schneider, D.P.: The Sloan digital sky survey photometric system. Astron. J. 111(4), 1748–1756 (1996). https://doi.org/10.1086/117915
Ackerman, M., Kiziah, R., Zimmer, P., McGraw, J., Cox, D.: A Systematic Examination of Ground-Based and Space-Based Approaches to Optical Detection and Tracking of Satellites. Paper presented at the 31st Space Symposium, Technical Track, Colorado Springs April 14, 2015
Sheldahl.: The Red 125 Book. (2015). Available: http://www.sheldahl.com/Products/WebPages/RedBook.aspx
Plis, E.A., Engelhart, D.P., Likar, J., Hoffmann, R.C., Cooper, R., Ferguson, D.: Electrical behavior of carbon-loaded Kapton for spacecraft applications. J. Spacecr. Rocket. 55, 1–2 (2017b). https://doi.org/10.2514/1.A33970
Mateo-Velez, J.C., Sicard-Piet, A., Lazaro, D., Inguimbert, V., Sarrailh, P., Hess, S., Maget, V., Payan, D.: Severe geostationary environments: numerical estimation of spacecraft surface Charging from flight data. J. Spacecr. Rocket. 53(2), 304–316 (2016). https://doi.org/10.2514/1.a33376
Khan, A.R., Jiang, W., Toyoda, K.: Electron and proton irradiation effect on bulk resistivity of polyimide measured in vacuum. JPN Soc. Aeronaut. Space Sci. 57, 6p (2013)
Shi, J., Gong, C., Tian, X., Yang, S., Chu, P.K.: Optical properties and chemical structures of Kapton-H film after proton irradiation by immersion in a hydrogen plasma. Appl. Surf. Sci. 258(8), 3829–3834 (2012)
Yue, L., Wu, Y., Sun, C., Shi, Y., Zhang, Y.: Effects of proton pre-irradiation on radiation induced conductivity of polyimide. Radiat. Phys. Chem. 119, 130–135 (2016)
Cooper, R., Hoffmann, R.: Jumbo space environment simulation and spacecraft CHARGING chamber characterization. Air Force Technical Report AFRL-RV-PS-TP-2015-0012 (2015)
Mosteller, R.D.: Bibliography of MCNP Verification & Validation: 1990-2003. In: Laboratory, L.A.N. (ed.) La-Ur-03–9032 (2003)
O'Brien, T.P., Johnston, W.R., Huston, S.L., Roth, C.J., Guild, T.B., Su, Y.J., Quinn, R.A.: Changes in AE9/AP9-IRENE version 1.5. IEEE Trans. Nucl. Sci. 65(1), 462–466 (2018). https://doi.org/10.1109/tns.2017.2771324
Engelhart D. P., Plis E. A., Cooper R., Humagain S., Koch A., Brunetti M., Greenbaum S., Hoffmann R.. Effect of Electron Bombardment on Polyimide 191 Film, Key Engineering Materials, vol. 759, pp. 48–53 (2018)
Plis E. A., Engelhart D. P., Cooper R., Ferguson D. C., Hoffmann R.. Effect of environment on 193 charge transport properties of polyimide films damaged by high-energy electron 194 radiation. Journal of Vacuum Science and Technology B 36 (5) (2018). https://doi.org/10.1116/1.5044184
Acktar Advanced Coatings. https://www.acktar-store.com/store/spectral-black-coated-foil-adhesive-backed-20x30cm-10sheet/ (2017). Accessed June 2017
Farnsworth, H.E.: Electronic bombardment of metal surfaces. Phys. Rev. 25(1), 41–57 (1925)
Yates, J.T.: Experimental Innovations in Surface Science: a Guide to Practical Laboratory Methods and Instruments. Springer (1997)
Cowardin, H., Seitzer, P., Abercromby, K., Barker, E., Schildknecht, T.: Characterization of orbital debris photometric properties derived from Laboratory-based measurements. Paper presented at the advanced Maui optical and space surveillance technologies conference, Maui
Sloan Digital Sky Survey. http://www.sdss.org/dr12/algorithms/ugrizvegasun/. Accessed June 2017
Humagain, S., Johnson, J., Stallworth, P., Engelhart, D., Plis, E., Ferguson, D., Cooper, R., Hoffmann, R., Greenbaum, S.: Study of damage and recovery of Electron irradiated polyimide using EPR and NMR spectroscopy. Bull. Am. Phys. Soc. 62, (2017)
Acknowledgements
We would like to acknowledge support from the Air Force Office of Scientific Research, Remote Sensing and Imaging Physics Portfolio (Dr. Stacy Williams). Grant 17RVCOR414.
Author information
Authors and Affiliations
Corresponding author
Additional information
Publisher’s Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Engelhart, D.P., Cooper, R., Cowardin, H. et al. Space Weathering Experiments on Spacecraft Materials. J Astronaut Sci 66, 210–223 (2019). https://doi.org/10.1007/s40295-019-00175-2
Published:
Issue Date:
DOI: https://doi.org/10.1007/s40295-019-00175-2