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Crystal structure of [(bis(1,10-phenanthroline-κ2N,N′)-(2-carboxy-4-(3-carboxy-5-carboxylatophenoxy)benzoato-κ2O:O′))nickel(II) monohydrate, (1,10-phenanthroline-κ2N:N′)-(μ2-(5-(3′,4′-dicarboxylphenoxy)-isophthalate-κ2O:O′))nickel(II)], C40H24N4O9Ni ⋅ H2O Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-06-05 Li-Ping Yao
C40H26N4O10Ni, triclinic, P1̄ (no. 2), a = 11.5851(8) Å, b = 11.5875(7) Å, c = 13.3921(8) Å, α = 81.440(5)°, β = 77.913(6)°, γ = 76.014(6)°, V = 1696.65(18) Å3, Z = 2, Rgt(F) = 0.0516, wRref(F2) = 0.1203, T = 293(2) K.
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Crystal structure of aqua-(2,2′-bipyridine-κ2N,N′)(((3-nitrophenyl)sulfonyl)glycine-κ2N,O)copper(II) dihydrate, C18H20CuN4O9S Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-06-05 Xiao-Miao Chen, Zheng-Jun Liu, Rong-Fei Zhao, Jing-Song Cheng, Lan Qin, Zhang-Di Long
C18H20CuN4O9S, monoclinic, P21/c (no. 14), a = 16.4177(5) Å, b = 17.9018(5) Å, c = 7.4580(2) Å, β = 90.490(3)°, V = 2191.87(11) Å3, Z = 4, Rgt(F) = 0.0451, wRref(F2) = 0.0956, T = 153(2) K.
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Crystal structure of 5,6-diphenyldibenzo[c, g]chrysene, C38H24 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-06-02 Zhang Bin, Chen Xin, Chen Songhua
C38H24, monoclinic, C2/c (no. 15), a = 37.6829(14) Å, b = 7.4695(3) Å, c = 17.4881(7) Å, β = 95.269(3)°, V = 4901.6(3) Å3, Z = 8, Rgt(F) = 0.0472, wRref(F2) = 0.1177, T = 123(2) K.
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Preparation and crystal structure of a non-symmetrical vanadium(II) dimer: tri-μ2-bromido-(hydrogen-tris(3-isopropyl-4-bromopyrazol-1-yl)borato-κ3N,N′,N′′)-tris(tetrahydrofuran-κO)divanadium(II) – tetrahydrofuran (1/1), C34H57BBr6N6O4V2 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-06-02 Peter J. Bonitatibus, William H. Armstrong, Guido J. Reiss
C34H57BBr6N6O4V2, orthorhombic, Pna21 (no. 33), a = 17.198(2) Å, b = 12.9497(11) Å, c = 20.496(2) Å, V = 4564.8(9) Å3, Z = 4, Rgt(F) = 0.0441, wRref(F2) = 0.1093, T = 183(2) K.
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Crystal structure of 2-methyl-1H-perimidine, C12H10N2 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-06-01 Xiao-Ming Shi, Li-Na Xiao, Peng Peng
C12H10N2, triclinic, P1̄ (no. 2), a = 9.0431(18) Å, b = 9.9770(19) Å, c = 11.623(2) Å, α = 102.375(3)°, β = 109.641(3)°, γ = 99.834(2)°, V = 930.5(3) Å3, Z = 4, Rgt(F) = 0.0395, wRref(F2) = 0.1105, T = 128.15 K.
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Crystal structure of 2-(3,6-dimethyl-2,3-dihydro-4H-benzo[b][1,4]oxazin-4-yl)-2-oxoethyl acetate, C14H17NO4 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-06-01 Minh-Tu Hoang, Ke-Liang Guo, Fei Ye
C14H17NO4, monoclinic, P21/c (no. 14), a = 9.6719(19) Å, b = 13.529(3) Å, c = 11.094(2) Å, β = 112.31(3)°, V = 1342.9(5) Å3, Z = 4, Rgt(F) = 0.0480, wRref(F2) = 0.1422, T = 293(2) K.
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Structural elucidation of 1-(3-acetyl-2,6-dihydroxy-4-methoxyphenyl)-4,5-dihydroxy-2-methylanthracene-9,10-dione isolated from Bulbine latifolia (L.) Wild, C24H18O8 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-06-01 Buyiswa G. Hlangothi, Lungelwa Mahanjana, Eric C. Hosten, Fanie R. van Heerden, Maryna van de Venter
C24H18O8, monoclinic, P21 (no. 4), a = 7.9654(3) Å, b = 23.6910(8) Å, c = 21.2314(8) Å, β = 96.777(2)°, V = 3978.6(3) Å3, Z = 8, R gt(F) = 0.0499, wR ref(F 2) = 0.1320, T = 200 K.
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Crystal structure of N,N-dimethyl-4-((7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)ethynyl)aniline, C16H12N4O2S Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-06-01 Chen Songhua, Zhang Bin, Chen Xin, Liu Yongqi
C16H12N4O2S, triclinic, P1̄ (no. 2), a = 7.249(2) Å, b = 8.265(3) Å, c = 12.786(4) Å, α = 82.449(11)°, β = 75.210(10)°, γ = 83.977(11)°, V = 732.3(4) Å3, Z = 2, Rgt(F) = 0.0669, wRref(F2) = 0.1726, T = 173.15 K.
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The crystal structure of poly[bis(N,N-dimethylformamide-κ1O)(μ4- 2′,5,5′,5′′-tetracarboxy-[1,1′:4′,1′′-terphenyl]-3,3′′-dicarboxylato-κ4O:O′:O′′:O′′′)manganese(II)] — N,N-dimethylformamide (1/2), C36H40N4O16Mn Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-29 Guoqiang Li, Guo Chen, Yanping Liu, Gao Wang, Liyu Liu
C36H40N4O16Mn, monoclinic, P21/c (no. 14), a = 10.5247(11) Å, b = 19.0823(19) Å, c = 10.5502(11) Å, β = 112.641(2)°, V = 1955.6(3) Å3, Z = 2, Rgt(F) = 0.0619, wRref(F2) = 0.1741, T = 296 K.
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Crystal structure of (4-aminobenzoato-κ2O,O′)-[5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N′′,N′′′]nickel(II) perchlorate monohydrate, C23H44ClN5NiO7 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-27 Guang-Chuan Ou, Qiang Zhou, Qiong Wang
C23H44ClN5NiO7, orthorhombic, P212121 (no. 19), a = 14.4994(16) Å, b = 19.799(2) Å, c = 20.040(2) Å, V = 5752.9(11) Å3, Z = 8, R gt(F) = 0.0409, wR ref(F 2) = 0.1061, T = 173(2) K.
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Crystal structure of bis{2-(((4-(1-(hydroxyl-imino)ethyl)phenyl)imino)methyl)phenolato-κ2N,O}cobalt(II), C30H26CoN4O4 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-22 Yi Jin, Tao Fu, Bo-Yang Ma, Ping Wei, Ji-Xing Zhao, Li Zhao
C30H26CoN4O4, monoclinic, C2/c (no. 15), a = 16.0520(5) Å, b = 19.1890(5) Å, c = 16.7292(4) Å, β = 93.064(1)°, Z = 8, V = 5145.6(2) Å3, Rgt(F) = 0.0400, wRref(F2) = 0.0932, T = 173(2) K.
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Synthesis and crystal structure of 1-{4-[(3-bromo-2-hydroxy-benzylidene)amino]phenyl}ethanone, C15H12BrNO2 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-22 Yi Jin, Tao Fu, Bo-Yang Ma, Ping Wei, Ji-Xing Zhao, Li Zhao
C15H12BrNO2, monoclinic, P21/c (no. 14), a = 11.7848(3) Å, b = 10.0857(3) Å, c = 12.2695(4) Å, β = 111.2020(10)°, Z = 4, V = 1359.61(7) Å3, R gt(F) = 0.0306, wR ref(F 2) = 0.0745, T = 173(2) K.
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Crystal structure of 1-{4-[(4-fluoro-2-hydroxy-benzylidene)amino]phenyl}ethanone, C15H12FNO2 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-22 Yi Jin, Tao Fu, Bo-Yang Ma, Ping Wei, Ji-Xing Zhao, Li Zhao
C15H12FNO2, monoclinic, C2/c (no. 15), a = 17.9898(8) Å, b = 4.6412(2) Å, c = 30.3832(15) Å, β = 93.072(3)°, Z = 8, V = 2533.2(2) Å3, Rgt(F) = 0.0568, wRref(F2) = 0.1399, T = 173(2) K.
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Crystal structure of 3-((3-nitrophenyl)sulfonamido)propanoic acid — 4,4′-bipyridine (1/1), C19H18N4O6S Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-21 Xiao-Miao Chen, Zheng-Jun Liu, Jing-Song Cheng, Rong-Fei Zhao, Lan Qin
C19H18N4O6S, monoclinic, P21/n (no. 14), a = 8.343(4) Å, b = 7.367(3) Å, c = 31.532(14) Å, β = 97.398(8)°, V = 1921.8(14) Å3, Z = 4, Rgt(F) = 0.0420, wRref(F2) = 0.1158, T = 296.15 K.
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Crystal structure of 3-cinnamoyl-4-hydroxybenzoic acid, C16H12O4 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-20 Chun-Mei Guo, Xiu-Ying Song, Mi-Na Wang, Jia Gu, Xu-Liang Nie
[C16H12O4], monoclinic, P21/n (no. 14), a = 13.760(5) Å, b = 4.9003(18) Å, c = 19.125(7) Å, β = 101.331(5)°, V = 1264.5(8) Å3, Z = 4, Rgt(F) = 0.0383, wRref(F2) = 0.1072, T = 296(2) K.
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The crystal structure of bis{3-(diphenylphosphaneyl)propanoato-κ2O,P}platinum(II) dihydrate, C30H28O6P2Pt Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-12 Pamela Moyo, Leah Matsinha, C.E. Makhubela Banothile
C30H28O6P2Pt, monoclinic, C2/c (no. 15), a = 16.911(3) Å, b = 9.516(2) Å, c = 16.790(3) Å, β = 100.830(4)°, V = 2653.8(9) Å3, Z = 4, Rgt(F) = 0.0126, wRref(F2) = 0.0310, T = 293 K.
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Crystal structure of bis(1,3-phenylenedimethanaminium) bis(triiodide) tetraiodide – water (1/2) , C8H16I5N2O Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-11 Guido J. Reiss
C8H16I5N2O, monoclinic, C2/c (no. 15), a = 34.180(5) Å, b = 7.6817(3) Å, c = 21.421(3) Å, β = 137.93(3)°, Z = 8, V = 3768.7(16) Å3, Rgt(F) = 0.0364, wRref = 0.0737, T = 290(2) K.
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The crystal structure of 1,3-bis(4-(methoxycarbonyl)benzyl)-2-methyl-1H-benzo[d]imidazol-3-ium bromide, C26H25BrN2O4 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-11 Bin Cai, Chun-Yan Fu, Xin-Yu Guo, Ying Wang
C26H25BrN2O4, triclinic, P1̄ (no. 2), a = 9.4202(5) Å, b = 9.7871(5) Å, c = 15.0135(9) Å, α = 106.775(3)°, β = 92.534(3)°, γ = 117.424(3)°, V = 1150.52(11) Å3, Z = 2, Rgt(F) = 0.0316, wRref(F2) = 0.0671, T = 150(2) K.
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Crystal structure of isopimara-7,15-dien-3-one, C20H30O Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-06 Ming-Hong Dong, Jiang-Hai Ye, Chen-Liang Zhao, Lang Zhou, Juan Zou, Jing-Jie Zhang
C20H30O, triclinic, P1̄ (no. 1), a = 6.6084(9) Å, b = 10.8811(16) Å, c = 12.0845(16) Å, α = 85.719(6)°, β = 79.547(5)°, γ = 89.903(5)°, V = 852.1(2) Å3, Z = 2, Rgt(F) = 0.0744, wRref(F2) = 0.1953, T = 173(2) K.
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Dimerization of 2-[(2-((2-aminophenyl)thio)phenyl)amino]-cyclohepta-2,4,6-trien-1-one through hydrogen bonding, C19H16N2OS Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-05 Anna Hanft, Crispin Lichtenberg
C19H16N2OS, triclinic, P1̄ (no. 2), a = 8.1510(3) Å, b = 8.8021(3) Å, c = 11.3953(5) Å, α = 72.546(2)°, β = 84.568(2)°, γ = 80.760(2)°, V = 768.86(5) Å3, Z = 2, Rgt(F) = 0.0491, wRref(F2) = 0.1494, T = 100 K.
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The crystal structure of (dichromato-κ2O,O′)bis(1,10-phenanthroline-κ2N,N′)nickel(II), C12H16N4O7Cr2Ni Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-04 Chen Wu-Hua, Xie Gui-Xiang, Chen Qin, Ruan Yan-Ming
C12H16N4O7Cr2Ni, orthorhombic, Pbcn (no. 60), a = 13.7804(5) Å, b = 10.3110(5) Å, c = 16.4118(6) Å, V = 2331.96(17) Å3, Z = 4, Rgt(F) = 0.0438, wRref(F2) = 0.1111, T = 293(2) K.
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Crystal structure of rac-trans-N,N′-bis(3-bromo-5-chlorosalicylidene)-1,2-cyclohexanediamine, C20H18Br2Cl2N2O2 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-04 Fang Jiang, Yan Xu, Xun Ma, Jiayi Li, Qiong Wu
C20H18Br2Cl2N2O2, monoclinic, P21/c (no. 14), a = 10.6105(8) Å, b = 17.1664(9) Å, c = 11.9848(9) Å, β = 97.682(3)°, V = 2163.4(3) Å3, Z = 4, Rgt(F) = 0.0330, wRref(F2) = 0.0823, T = 100(2) K.
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Crystal structure of bis((3-chlorosalicylidene)-ethylenediaminato-κ4N,N′,O,O′)nickel (II), C16H12Cl2NiN2O2 Z. Kris. New Cryst. Struct. (IF 0.29) Pub Date : 2020-05-01 Jianchang Xiao, Cun Zhou, Hui Tan, Meifen Huang, Qiong Wu
C16H12Cl2NiN2O2, orthorhombic, Pbca (no. 61), a = 12.5166(12) Å, b = 12.5881(14) Å, c = 19.0086(19) Å, V = 2995.0(5) Å3, Z = 8, Rgt(F) = 0.0435, wR2 = 0.0826, T = 296.15.