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The Assembly of Integrated Continuous Flow Platform for on-demand Rosiglitazone and Pioglitazone Synthesis React. Chem. Eng. (IF 5.2) Pub Date : 2022-08-12 Mandeep Purwa, Abhilash Rana, Ajay K. Singh
The thiazolidinediones manufacturing in a batch process is often carried out at different locations, where each successive batch collects a certain amount of intermediate followed by its transportation to another location. Thiazolidinediones containing APIs are unstable at ambient temperature. In this regard, manufacturing sites need huge storage capacity with lower temperature (2-8 oC), which eventually
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Catalytic Reduction of In-Flow Aqueous Cr(VI) using a Slurry of Activated Carbon Fibers-Supported Ni Nanoparticles in a Coiled Flow Inverter React. Chem. Eng. (IF 5.2) Pub Date : 2022-08-09 Rakshit Kajala, Shivam Singh Tomar, Nishith Verma, Krishna D P Nigam
This study presents a coiled flow inverter (CFI) for the first time as an alternate technology to the conventional packed bed reactors for carrying out the in-flow aqueous phase catalytic reduction of hexavalent chromium (Cr(VI)). Cr(VI) is reduced to its less-toxic trivalent state, viz. Cr(III), utilizing an environmentally benign reducing agent- formic acid. An aqueous slurry of the micron-sized
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Assessing a Sustainable Manufacturing Route to Lapatinib React. Chem. Eng. (IF 5.2) Pub Date : 2022-08-09 Roderick T Stark, Dominic Pye, Wenyi Chen, Oliver J Newton, Benjamin J Deadman, Philip Miller, Jenny-Lee Panayides, Darren Lyall Riley, Klaus Hellgardt, King Kuok Mimi Hii
A synthetic route to an anti-cancer drug, lapatinib, was devised to support the development of a sustainable manufacturing process in South Africa. Quantitative metrics were employed to evaluate the sustainability of the key steps of the reaction.
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The synergetic effect of Pd, In and Zr on the mechanism of Pd/In2O3-ZrO2 for CO2 hydrogenation to methanol React. Chem. Eng. (IF 5.2) Pub Date : 2022-08-09 Minhua Zhang, Fuchao Li, Maobin Dou, Yingzhe Yu, Yifei Chen
The hydrogenation of CO2 to methanol is of great significance from both the environmental and economic view. The excellent performance of Zr-doped or Pd-supported In2O3 catalysts have been reported in recent years. However, the mechanism of CO2 hydrogenation in the coexistence of Pd, In and Zr is unclear. In this paper, the density functional theory method has been used to explore the synergistic relationship
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Selective Oxidation of Aldehyde by Oxygen over Macroporous Alkaline Resin React. Chem. Eng. (IF 5.2) Pub Date : 2022-08-06 Xiaojing Fu, Yuchan Han, Rui Chen, Qi Han, Rongfan Zhang, Jun Li
OH-type macroporous strong-base resin was evaluated as a heterogeneous catalyst for the oxidation of aldehydes to corresponding carboxylic acids by molecular oxygen. A wide range of aldehydes, such as aromatic, aliphatic and cyclohexyl aldehydes, were found being oxidized to the goal acids with high yields in short time without any metals or hazardous oxidants or cocatalysts were involved. Solvents
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A scalable twin surface dielectric barrier discharge system for pollution remediation at high gas flow rates React. Chem. Eng. (IF 5.2) Pub Date : 2022-08-01 Alexander Böddecker, Arisa Bodnar, Lars Schücke, Jonas Giesekus, Katja Wenselau, Ryan T. Nguyen-Smith, Timothy Oppotsch, Christian Oberste-Beulmann, Martin Muhler, Andrew R. Gibson, Peter Awakowicz
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A Role of Urea in Regulating the Structural Properties of Zr-Sn-based Oxide Catalysts for Direct Synthesis of Dimethyl Carbonate from CO2 and Methanol React. Chem. Eng. (IF 5.2) Pub Date : 2022-08-04 Hongyong Yang, Huapeng Sun, Wei Zeng, Fangfang Dai, Yan Duan, Midong Shi, Zhiqiang Hua, Xiaohui Yang, Bo Zhang
Urea,Catalyst,Dimethyl Carbonate,CO2,Methanol
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A promising Ruddlesden-Popper oxide cathode for both proton-conducting and oxygen ionic-conducting solid oxide fuel cells React. Chem. Eng. (IF 5.2) Pub Date : 2022-08-03 Shujun Peng, Song Lei, Sisi Wen, Xingyao Liu, Jian Xue
Intermediate and low-temperature solid oxide fuel cells (SOFCs) operated below 800 oC have attracted tremendous interest for their low component cost, preferable chemical compatibility of the components and considerable stability. In this paper, a Ruddlesden-Popper oxide with the composition of Nd1.8La0.2Ni0.74Cu0.21Ga0.05O4+δ (NLNCG) is developed as a cathode for intermediate and low-temperature SOFCs
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Production of γ-valerolactone over mesoporous CuO catalysts using formic acid as the hydrogen source React. Chem. Eng. (IF 5.2) Pub Date : 2022-08-02 Neda Ayashi, Alireza Najafi Chermahini, Nasim Amiri Ramsheh, Rafael Luque
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Autonomous model-based experimental design for rapid reaction development React. Chem. Eng. (IF 5.2) Pub Date : 2022-08-02 Sebastian Knoll, Clemens E. Jusner, Peter Sagmeister, Jason D. Williams, Christopher A. Hone, Martin Horn, C. Oliver Kappe
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A low-cost and high-performance 3D micromixer over a wide working range and its application for high-sensitivity biomarker detection React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-27 Bo Liu, Bin Ran, Chaozhan Chen, Liuyong Shi, Ya Liu, Huaying Chen, Yonggang Zhu
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Probabilistic framework for optimal experimental campaigns in the presence of operational constraints React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-22 Kennedy Putra Kusumo, Kamal Kuriyan, Shankarraman Vaidyaraman, Salvador García Muñoz, Nilay Shah, Benoît Chachuat
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A novel observation platform for determining the micro-dispersion performance in practical reaction systems React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-21 Jing Song, Chencan Du, Junjie Wang, Yongjin Cui, Yujun Wang, Jian Deng, Guangsheng Luo
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The effect of MgO and preparation techniques of the FeMnOδ/MgO–Al2O3 catalyst used for the vapor phase oxidation of cyclohexane React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-16 Vijendra Kumar Yadav, Taraknath Das
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The Al(III)-based polydentate chelate complex catalyzed cycloaddition of carbon dioxide and epoxides: synthetic optimization and mechanistic study React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-14 Hong-Qing Fu, Haifang Mao, Chaoyang Wang, Kun Yin, Miaomiao Jin, Zhenbiao Dong, Yun Zhao, Jibo Liu
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A practical guide to automating fluorine-18 PET radiochemistry using commercially available cassette-based platforms React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-13 Chris Barnes, Manoj Nair, Eric O. Aboagye, Stephen J. Archibald, Louis Allott
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Probing the methanol-assisted autocatalytic formation of methanol over Cu/ZnO/Al2O3 by high-pressure methanol and methyl formate pulses React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-13 Philipp Schwiderowski, Sascha Stürmer, Martin Muhler
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Biocatalytic fumarate synthesis from pyruvate and CO2 as a feedstock React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-13 Mika Takeuchi, Yutaka Amao
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An integrated resource-efficient microfluidic device for parallelised studies of immobilised chiral catalysts in continuous flow via miniaturized LC/MS-analysis React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-07 Hannes Westphal, Rico Warias, Chris Weise, Daniele Ragno, Holger Becker, Matthias Spanka, Alessandro Massi, Roger Gläser, Christoph Schneider, Detlev Belder
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Defluoridation using hydroxyapatite implanted lanthanum organic framework-based bio-hybrid beads React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-12 Antonysamy Jeyaseelan, Ilango Aswin Kumar, Mu. Naushad, Natrayasamy Viswanathan
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Pore flow-through catalytic membrane reactor for steam methane reforming: characterization and performance React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-12 M. Angulo, I. Agirre, A. Arratibel, M. A. Llosa Tanco, D. A. Pacheco Tanaka, V. L. Barrio
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Effect of steam on heat storage and attrition performance of limestone under fluidization during CaO/CaCO3 heat storage cycles React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-11 Yi Fang, Yingjie Li, Yehui Dou, Zirui He, Jianli Zhao
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Correction: Synthesis of sub-nanometric Cu2O catalysts for Pd-free C–C coupling reactions React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-07 Ankit Agrawal, Reena Goyal, B. Moses Abraham, Omvir Singh, Shailendra Tripathi, Mukesh K. Poddar, Rajaram Bal, Bipul Sarkar
Correction for ‘Synthesis of sub-nanometric Cu2O catalysts for Pd-free C–C coupling reactions’ by Ankit Agrawal et al., React. Chem. Eng., 2021, 6, 929–936, https://doi.org/10.1039/D1RE00054C.
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Reduced graphene oxide–zinc sulfide (RGO–ZnS) nanocomposite: a new photocatalyst for oxidative cyclization of benzylamines to benzazoles under visible-light irradiation React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-05 Mona Hosseini-Sarvari, Hossein Sheikh
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Synthesis of boron-doped carbon nanotubes by thermocatalytic decomposition of ethanol using a floating catalyst chemical vapor deposition method: kinetic study React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-04 Shrilekha V. Sawant, Kinshuk Dasgupta, Jyeshtharaj B. Joshi, Ashwin W. Patwardhan
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Effect of acid distribution and pore structure of ZSM-5 on catalytic performance React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-04 Runze Jin, Ke Ma, Shutao Xu, Yingxu Wei, Lijuan Song, Zhijun Li, Penghui Zhang, Yufeng Wang, Jiaofei Wang, Zhuangzhuang Zhang, Xiaoxun Ma, Haobin Hu, Chengyi Dai, Xinwen Guo
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Synthesis of acrylic acid and acrylic esters via oxidation and oxidative alkoxylation of acrolein under mild conditions with selenium-modified microgel catalysts React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-04 Tetiana Kharandiuk, Kok H. Tan, Iryna Kubitska, Miriam Aischa Al Enezy-Ulbrich, Volodymyr Ivasiv, Roman Nebesnyi, Igor I. Potemkin, Andrij Pich
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Highly conductive CNT aerogel synthesized via an inert FC-CVD technique: a step towards a greener approach React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-04 Manoj Sehrawat, Mamta Rani, Pallvi Dariyal, Sony Bharadwaj, S. R. Dhakate, Bhanu Pratap Singh
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Structural control in the nanoassembly of the tungsten and molybdenum dithiolene complex analog React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-04 Jagannath Bhuyan, Bholanath Pakhira, Ameerunisha Begum, Sabyasachi Sarkar, Kumud Malika Tripathi
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Influence of pH on the kinetics of hydrolysis reactions: the case of epichlorohydrin and glycidol React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-04 Flavio Tollini, Alice Occhetta, Francesca Broglia, Vincenzo Calemma, Stefano Carminati, Giuseppe Storti, Mattia Sponchioni, Davide Moscatelli
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Surface hydroxyl groups: the key to a CrOx/TiO2 catalyst for efficient catalytic oxidation of 2,2′-hydrazine diisobutyronitrile React. Chem. Eng. (IF 5.2) Pub Date : 2022-07-02 Hu Zhang, Xingli Zou, Xueguang Wang, Haijiao Xie, Zheng Jiao, Xionggang Lu
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Outstanding Reviewers for Reaction Chemistry & Engineering in 2021 React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-30
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Catalytic co-pyrolysis of LDPE and PET with HZSM-5, H-beta, and HY: experiments and kinetic modelling React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-30 Sean Timothy Okonsky, J. V. Jayarama Krishna, Hilal Ezgi Toraman
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Copper supported silica-based nanocatalysts for CuAAC and cross-coupling reactions React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-23 Pitchaimani Veerakumar, Nithya Velusamy, Pounraj Thanasekaran, King-Chuen Lin, Seenivasan Rajagopal
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Design of millidevices to expedite apparent solubility measurements React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-17 Maria del Carme Pons Royo, Jean-Luc Beulay, Eric Valery, Alois Jungbauer, Peter Satzer
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Device for automated screening of irradiation wavelength and intensity – investigation of the wavelength dependence of photoreactions with an arylazo sulfone in continuous flow React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-14 Thomas Roider, Norbert Frommknecht, Alexandra Höltzel, Ulrich Tallarek
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Sustainable synthesis of acetals from glycerol as potential additives for biofuels under solvent-free conditions React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-16 Gabriel Abranches Dias Castro, Ana Luíza Quintão Santos, Ángel Gabriel Sathicq, Valeria Palermo, Gustavo Pablo Romanelli, Sergio Antonio Fernandes
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Production of pentyl valerate from γ-valerolactone, pentanol and H2 using Pd and Rh-based bifunctional catalysts React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-15 Karla G. Martínez Figueredo, Emanuel M. Virgilio, Darío J. Segobia, Nicolás M. Bertero
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Facile synthesis of a nano titanium catalyst and its performance in selective oxidation of aromatic and pyridinic alcohols under visible light React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-15 Peng Zheng, Jianguo Liu, Xinghua Zhang, Lungang Chen, Longlong Ma, Qi Zhang
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Catalyst and reactor design considerations for selective production of acids by oxidative cleavage of alkenes and unsaturated fatty acids with H2O2 React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-10 Danim Yun, Zhongyao Zhang, David W. Flaherty
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Combining Cu-SSZ-13 with TiO2: promotion of urea decomposition and influence on SCR React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-09 Yue Ma, Zhimin Shao, Xiaodong Wu, Yang Gao, Baofang Jin, Rui Ran, Zhichun Si, Zhenguo Li, Duan Weng
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Convenient and accurate insight into solution-phase equilibria from FlowNMR titrations React. Chem. Eng. (IF 5.2) Pub Date : 2022-06-09 Daniel B. G. Berry, Ian Clegg, Anna Codina, Catherine L. Lyall, John P. Lowe, Ulrich Hintermair
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PhSe(O)OH/Al(NO3)3-Catalyzed selectivity controllable oxidation of sulphide owing to the synergistic effect of Se, Al3+ and nitrate React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-30 Xu Zhang, Rui Zhou, Zhengyuan Qi, Liping Chen, Lei Yu
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CO2 adsorption on PEHA-functionalized geothermal silica waste: a kinetic study and quantum chemistry approach React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-27 Jonatan Estévez-Jácome, Carlos Argáez, Rosa-María Ramírez-Zamora, Brenda Alcántar-Vázquez
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Synthesis of modified amphiphilic quaternary ammonium silicotungstate and its application in heterogeneous catalytic oxidative desulfurization React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-27 Yanwen Guo, Xingjian Liu, Bing Hu
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Liquid-phase catalytic hydrodechlorination of chlorinated organic compounds in a continuous flow micro-packed bed reactor over a Pd/AC catalyst React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-26 Zipin Peng, Xuepeng Wang, Zheng Li, Xingkun Chen, Yunjie Ding, Jisong Zhang
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Combining multivariate curve resolution and lumped kinetic modelling for the analysis of lignin degradation by copper-catalyzed Fenton-like systems React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-19 Andrea M. Berkovic, Mariana R. Costante, Fernando S. García Einschlag
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Microwave-promoted continuous flow synthesis of thermoplastic polyurethane–silver nanocomposites and their antimicrobial performance React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-19 Qandeel Saleem, Milad Torabfam, Hasan Kurt, Meral Yüce, Mustafa Kemal Bayazit
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N-Doped natural albite mineral as green solid catalyst for efficient isomerization of glucose into fructose in water React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-12 Jiabing Ren, Xin Ye, Xiaoyu Shi, Huixing Xu, Lanxin Wu, Tianfu Wang
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ZnO nanoflakes self-assembled from the water splitting process using a hydroelectric cell React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-17 Jyoti Shah, Abha Shukla, Manoranjan Kar, Govind Gupta, Shipra Jain, R. K. Kotnala
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Construction of an α-chiral pyrrolidine library with a rapid and scalable continuous flow protocol React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-16 Chao Shan, Liming Cao, Jiasheng Yang, Ruihua Cheng, Xiantong Yao, Chaoming Liang, Maolin Sun, Jinxing Ye
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Mechanistic insight into the photocatalytic degradation of organic pollutants and electrochemical behavior of modified MWCNTs/Cu–Co3O4 nanocomposites React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-16 M. F. Sanakousar, Vidyasagar C. C, Víctor M. Jiménez-Pérez, Mounesh, A. H. Shridhar
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Highly efficient Ni–NiO/carbon nanotubes catalysts for the selective transfer hydrogenation of 5-hydroxymethylfurfural to 2,5-bis(hydroxymethyl)furan React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-16 Zixuan Liu, Zexing Huang, Wenguang Zhao, Xianxiang Liu
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Room-temperature conversion of CO2 into quinazoline-2,4(1H,3H)-dione using deep eutectic solvents at atmospheric pressure with high efficiency React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-16 Yu Chen, Chong Liu, Yaoting Duan, Dongkun Yu, Zhenghui Liu, Yuting Li, Ruifen Shi, Yuting Guo, Tiancheng Mu
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Homogeneous catalyst modifier for alkyne semi-hydrogenation: systematic screening in an automated flow reactor and computational study on mechanisms React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-16 Shusaku Asano, Samuel J. Adams, Yuta Tsuji, Kazunari Yoshizawa, Atsushi Tahara, Jun-ichiro Hayashi, Nikolay Cherkasov
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An assessment of a multipoint dosing approach for exothermic nitration in CSTRs in series React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-06 G. M. Mule, S. Kulkarni, A. A. Kulkarni
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A compact, practical photoreactor for multi-reaction arrays React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-06 Gregory D. Brown, Daniel Batalla, Cullen L. Cavallaro, Heidi L. Perez, Stephen T. Wrobleski, Trevor C. Sherwood
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CO2 fixation into cyclic carbonates catalyzed by single-site aprotic organocatalysts React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-04 Ala'a F. Eftaiha, Abdussalam K. Qaroush, Areej K. Hasan, Wissam Helal, Feda'a M. Al-Qaisi
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Analysis of n-hexane, 1-hexene, cyclohexane and cyclohexene catalytic cracking over HZSM-5 zeolites: effects of molecular structure React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-04 Zhenzhou Ma, Xu Hou, Bochong Chen, Liu Zhao, Enxian Yuan, Tingting Cui
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Microwave-assisted depolymerization of lignin with synergic alkali catalysts and a transition metal catalyst in the aqueous system React. Chem. Eng. (IF 5.2) Pub Date : 2022-05-03 Heyu Li, Yingfang Huang, Xiuhua Lin, Yifan Liu, Yuancai Lv, Minghua Liu, Yuming Zhang