Pyrogenic carbon (charcoal, black carbon, elemental carbon) is one of the most common materials used for radiocarbon dating of terrestrial samples. However, exogenous carbon contamination can compromise the accuracy of radiocarbon ages. This study presents the results of two chemical pretreatments prior to hydrogen pyrolysis (hypy) as improved protocols for the isolation and decontamination of pyrogenic

Potassium (K)-rich feldspars are one of two mineral types typically used for optical dating. Feldspar grains can contain up to ∼14 wt% K that gives rise to an internal dose rate component. This internal component can comprise a significant proportion of the total environmental dose rate to which a mineral grain is exposed. The environmental dose rate term—the denominator in the optical age equation—determines

The Golo River drains a steep catchment (average gradient of 30 m km−1, surface of 1214 km2) in the northeast part of Corsica Island, delivering sediments to the Ligurian Sea. In this study, we review and revise the geologic map and constrain the extent of the Golo coastal alluvial plain formations and their relative and absolute chronology. To update the surface extent of each formation, we performed

The continental accumulation of dust during the Quaternary led to the formation of widespread loess deposits in southern Tajikistan. In this area, the accumulation of loess is commonly associated with the occurrence of dust storms and the widespread distribution of loess provides evidence of dust storms becoming more frequent in arid Central Asia at least since the Early Pleistocene. Southern Tajikistan

Age distributions of speleothem growth frequency are often employed as proxies for past climate variation. However, their interpretation can be influenced by many variables such as the type of probability density estimator used, the number of samples studied, and indeed the nature of the sampling itself. In order to explore the utility of speleothem age distributions in this context, we constructed

To extend the range of materials that can be used to provide chronological constraint in archaeological and palaeontological settings, we explore the use of cave pearls that form in shallow pools. Here, we present U-series dating results of cave pearls found in cave sediments with mammal fossils collected from systematic excavations at the Diaozhongyan Cave (“DZY”), located in Guangxi Zhuang Autonomous

A comparison of two different mechanical separation procedures, a settling process and sieving process, was performed in the samples preparation for radiocarbon dating of archaeological lime mortars from the Tower Keep at Irulegi Castle (Navarre, Spain). The different fractions obtained by the two different mechanical separation procedures were converted to carbon dioxide by sequential dissolution

The freshwater reservoir effect (FRE) was estimated for the northern part of West Siberia for the first time, based on securely dated samples from the late medieval town of Mangazeya existed mainly in AD 1601–1650. Twelve specimens of six species of freshwater fish were selected for 14C dating, and C and N stable isotopes analysis. The FRE varies from ca. 310 to ca. 1970 14C years, and there is no

The identification and correlation of a sequence of Pleistocene beach barriers located within the northern Coorong Coastal Plain, South Australia, is made difficult by long-term subsidence and extensive reworking. Associated shell beds, to all but the last interglacial barrier, are subsurface and not readily accessible. The whole-rock amino acid racemization method was found to be unsuitable for distinguishing

Lacustrine sediments provide an excellent opportunity to study climate change beyond the instrumental period and further to elucidate its intrinsic interactions with ecosystem. However, the radiocarbon (14C)-based chronological framework of such natural archives, on which robust interpretation of geochemical proxies primarily depends, is commonly challenged due to the difficulty in properly correcting

In optical dating, incomplete and heterogeneous resetting (“bleaching”) of the luminescence signal measured from mineral grains since the last episode of transport and deposition is commonly observed for sedimentary samples. As a result, different grains could have different equivalent dose (De) values at the time of deposition. For such samples, statistical treatment of the De distribution is required

To understand the salinity, redox characteristics, and climatology of Dali Lake during the late Holocene, we analysed trace element records from a high-resolution sediment core (DL-1), including Al, Mn, Zn, Mo, Pb, Fe, Sr, and Ba. The core was dated to 2100 cal BP based on accelerator mass spectrometry (AMS) 14C dating combined with the constant rate of supply (CRS) model. We identified five palaeoclimatic

The standardised growth curve (SGC) procedure is a technique that can facilitate rapid De estimation. In this study, we apply a least-squares (LS) normalisation procedure to single grains of quartz from multiple sites across Australia to test its applicability for establishing common SGCs for individual quartz grains from the same continent. Seventy-two samples from 18 sites were divided into two groups:

Luminescence dating is applied to sediments from Mwulu's Cave, whose lithics have been typologically considered Middle Stone Age (MSA) and have been previously assigned to what is called the Pietersburg industry. This industry is, however, poorly defined both chronologically and typologically. Luminescence methods were applied to both quartz and potassium feldspars by two different laboratories. Age

The 210Pb sediment dating is the most widely used method to determine recent (~100–150 years) chronologies and sediment accumulation rates in aquatic environments and has been used effectively for reconstruction of diverse environmental processes associated with global change. Owing to the relative accessibility of the 210Pb methodology, many environmental chronologies have been produced, but not always

A suite of 10 samples collected from an 11 m thick colluvial sequence at Voordrag, KwaZulu-Natal, South Africa, have been used to undertake a comparison of different luminescence methods. Good agreement is found between single grain quartz optically stimulated luminescence (OSL) and single grain K-feldspar post-infrared infrared-stimulated luminescence (post-IR IRSL) ages, with the exception of the

Pre- or post-depositional heating of fossil biominerals will impact resulting amino acid dates, but the study on the effects on their amino acids of dry artificial heating of molluscs has not yet been fully tested. Here we report a study on three mollusc species to show how amino acid content can potentially be used to identify archaeological samples that have been subjected to artificial heating.

Basaltic lavas provide a window into their mantle sources and the associated geodynamic processes associated with them. Obtaining absolute chronology on young basalt flows is often challenging. Some gypsum crusts in pyro-duct (lava tube) caves crystallize during the last “cooling” stages of tube formation probably at relatively low temperatures (i.e., <100 °C). Here we propose uranium-series dating

Bayesian inference has been applied extensively to chronologies in archaeological science since it provides several advantages over the (classic) frequentist approach. One of the most important aspects of applying Bayesian methods is their capacity to consider the stratigraphic relationship between ages. In luminescence dating, a crucial motivation for applying Bayesian modelling is the ability to

We present a new 52 m composite record (COL17c) composed of five sedimentary sequences retrieved from the Colônia basin (Southeastern Brazil). The COL17c record is composed of two main sub-units deposited under different regimes: a peatland above ~14 m and lacustrine sediments below. Sedimentary description and core scanning (MSCL and XRF) are first used to align individual cores in order to produce

Coasts on active subduction zones are recurrently affected by great earthquakes and associated tsunamis. Deposits resulting from both tidal inundation after coseismic subsidence and from tsunamis can be radiocarbon dated to infer patterns of earthquake and tsunami recurrence. Yet, finding suitable plant material for radiocarbon dating is not always easy. Luminescence dating provides a more ubiquitously

A Cedrela odorata tree ring width chronology spanning from 1786 to 2016 was developed in the quasi-equatorial eastern Amazon Basin. Annual calendar dates were assigned using dendrochronological techniques at the Federal University of Lavras, Brazil. Due to its strategic location at the edge of the Equator (approximately 0°57′S), an independent confirmation of the annual periodicity of this century-long

Time-dependent changes in dose rates generally need to be considered in luminescence dating due to the dynamic character of the geosphere. Nevertheless, this aspect is rather marginally treated in the literature. The present paper describes the methodology of including temporal variations of overburden, moisture content and radionuclide activity into the calculation of dating results. Consideration

In situ cosmogenic nuclides are widely employed to quantify topographic and geomorphic landscape evolution. However, few studies are devoted to investigating possibly unsteady denudation. In this work the denudation rates of five surface bedrock and one depth profile are measured using in situ cosmogenic 36Cl in different climate zones in China; cosmogenic 36Cl is a powerful proxy for the surface denudation

Cosmogenic nuclides (CN) are widely used to determine both erosion rates E and exposure ages t of surfaces. However, in situations where both quantities are unknown, measuring a single CN at a surface is typically not sufficient to determine both t and E. We discuss the possibility of determining both t and E by measuring the CN pair, in-situ 10 Be and 14 C in quartz, at a surface. We use a previously

Overestimation in dose recovery results was observed at high doses (>1000 Gy) when a single-aliquot regenerative-dose (SAR) procedure is applied to the multiple-elevated-temperature post-IR IRSL (MET-pIRIR) signals from potassium-rich feldspar (K-feldspar) grains from the Nihewan Basin. Such overestimation results from the non-bleachable (residual) signals that were not appropriately corrected for

In optical dating, equivalent dose (De) values for a sample are commonly obtained from measurement of the luminescence signals of individual mineral grains or aliquots and projection of the natural signals onto the corresponding regenerative-dose response curves. A final De estimate is calculated by using a statistical model to combine the individual De values. This method can be problematic for samples

Alluvial and colluvial “cut and fill” deposits preserved in valleys of the Karoo, South Africa, reflect basin-scale adjustments in fluvial process-regime. Such deposits in the Wilgerbosch catchment have previously proven difficult to date using radiocarbon (14C) and optically stimulated luminescence (OSL) methods. In this paper, we test the suitability of K-feldspar post-IR infrared (pIRIR) methods

In luminescence dating of feldspar, laboratory induced luminescence necessary to assess the naturally acquired dose in the environment suffers from a poorly understood instability over time, known as anomalous fading (AF). AF is the source of commonly observed age underestimation in optical dating of feldspar. Approaches to circumvent AF include correction methods as well as attempts to measure directly

The standardised growth curve (SGC) method has been applied to potassium-rich feldspar (K-feldspar) from samples at the Nihewan Basin, northern China. It was observed that the shapes of SGCs obtained from multiple-aliquot regenerative-dose (MAR) and single-aliquot regenerative-dose (SAR) procedures are different at high doses (>900 Gy) for the multiple-elevated-temperature post-IR IRSL (MET-pIRIR)

New K-Ar ages obtained on juvenile pumice glass shards indicate that the Chalupas ignimbrite, one of the main Pleistocene tephra markers of the Ecuadorian arc, was emplaced at 216 ± 5 ka. Morphology and major and trace element contents of the glass shards are similar to those of ash layers from deep-sea cores and allow correlation between continental deposits and marine tephra layers. Based on biostratigraphy

The timing and extent of the last glaciation in the Altai Mountains are key to understanding climate change in this critical region. However, robust glacial chronologies are sparse across the Altai Mountains, especially in the Chinese Altai, impeding the correlation of glacial events and examination of the possible climate forcing mechanisms. Here, we report twenty new 10Be exposure-ages obtained from

Optically stimulated luminescence (OSL) dating of single grains is often required to determine an accurate age for partially-bleached sediment by identifying those grains with OSL signals that were well bleached prior to burial. However, single-grain De distributions are typically characterised by greater amounts of scatter in comparison to multiple grains. Here we investigate the scatter in single-grain

The Saksunarvatn Ash, first found in the Faroe Islands, is a tephra produced by the Grímsvötn volcanic system in Iceland. Since its discovery in the Faroe Islands, dark tephra with a similar stratigraphic position has been described at numerous locations around the North-Atlantic region; including 46 sites in Iceland (soil and lake sediments), 37 marine sediment cores from the North-Atlantic, 23 terrestrial

In the absence of reliable charcoal, wood or plant macrofossils, organic matter in loess-paleosols is often used for 14C dating. However, organic matter can be contaminated by a variety of carbon sources within the sediments, and this may affect the radiocarbon dating results. Specific chemical pretreatments can be applied to minimize such effects, and comparisons with optically stimulated luminescence

In this study we compared De results obtained from single-aliquot (SA) and single-grain (SG) measurements on potassium rich feldspars (K-feldspars) from the Nihewan Basin, north China, based on the multiple-elevated-temperature post-infrared infrared (MET-pIRIR) stimulated luminescence. Discrepancy was observed between the SA and SG De results. Potential reasons for such discrepancy, including residual

The sedimentary system of the Algiers Bay has been impacted in the last decades by the exponential increases in population, urbanism and industrial activities of the city of Algiers, and by episodic floods, mudflows, earthquakes and tsunamis. Activity concentrations of environmental gamma-emitters, namely 210Pb, 226Ra, 40K, 228Ra, 228Th and 137Cs, were measured in a sediment core sampled in 2015 at

Based on the vertical distribution of 210Pb activity concentrations in bottom sediment, linear accumulation rates (LAR) and mass accumulation rates (MAR) were determined for 31 locations in the southern Baltic Sea region by applying models: Constant Flux Constant Sedimentation Rate (CF:CS) and Constant Rate of Supply (CRS). The dating of sediment layers in selected locations was also carried out. The

A 601 m long sedimentary sequence was drilled in Lake Acigöl, located in the lakes region of SW Anatolia, near the Denizli travertine from which the oldest hominin of Turkey was unearthed. Among all dating methods applied to the sedimentary sequence, paleomagnetism, through the recognition of geomagnetic chrons, was the most successful and led to a quasi linear age model, with the 601 m long sedimentary

Permafrost is widely present throughout the Northern Hemisphere high latitudes, and stores large amounts of carbon in the form of frozen soil organic matter. The response of permafrost regions to anthropogenic climate change remains uncertain, in part because of a lack of information on their response to past changes in global climate. Here we test the use of stalagmites from two caves in Siberia as

The 30-km-long Middle Kedrovaya (MK) fault, on the northwestern flank of Lake Baikal, is one of the most impressive late Quaternary seismogenic structures in the Baikal rift. In places, surface fault scarps expose striated bedrock fault planes and offer some opportunities to examine the faulting history. Using cosmogenic 10Be exposure dating, we measured the exposure ages of one of the MK scarps (54

Determining the ages of young volcanic rocks is important for understanding the tectono-magmatic development of geologic terranes. Usually, if rocks are old enough the 40Ar/39Ar or K–Ar techniques can provide reliable ages. However, when rocks are younger, they often lack enough daughter product to resolve an age. Cosmogenic 3He methods provide an alternative for determining the eruption age of relatively

When mollusc shells are analysed conventionally for amino acid geochronology, the entire population of amino acids is included, both inter- and intra-crystalline. This study investigates the utility of removing the amino acids that are most susceptible to environmental effects by isolating the fraction of amino acids encapsulated within mineral crystals of mollusc shells (intra-crystalline fraction)

Kyra is an important tephra unit for Nisyros pre-caldera stage due to a number of subunits with various compositions (basaltic andesite to dacite) and distal dispersion on surrounding Greek islands (Tilos and Chalki) and Datça peninsula (Turkey). As for the most Nisyros tephra units, the available radiometric ages of Kyra tephra are not compatible with the relatively well-established Nisyros tephrostratigraphy

Loess-paleosol sequences in the arid central Asia (ACA) provide valuable material for evaluating the evolution of paleoclimate and dust circulation in the Northern Hemisphere. However, determination of loess chronology has yet remained a main obstacle for paleoclimate interpretation. In this study, analyses of relative paleomagnetic intensity (RPI) were conducted in a loess section on the northern

Lead-210 from natural atmospheric fallout is widely used in multidisciplinary studies for dating recent sediments. In anthropogenically-impacted and/or high energy systems the 210Pb flux onto the sediments may show non-random temporal variability, leading to the failure of classical dating models. The problem of how identifying and dating such cases remained unsolved, and it is the goal of the present

We study seven out of the thirteen lava flows associated to El Metate shield volcano using paleomagnetic, absolute intensity and rock-magnetic experiments. Characteristic paleomagnetic directions were successfully determined from most of the flows. A combined mean direction of D = 346.4° and I = 32.1° (N = 34, R = 33.73, k = 121.74, α95 = 2.2) was obtained for the early flows (Flow 1 − Flow 3). Flow

The Yuanmou H. erectus site is generally considered to be one of the oldest hominin sites in southern China. The chronology of this site has been repeatedly investigated using magnetostratigraphy since its first discovery in the 1960s. However, there are multiple interpretations of the magnetostratigraphy due to the complexity of the sedimentary environment, resulting in a one million year age discrepancy

The Quaternary paleoenvironmental history of the Arctic Ocean remains uncertain, mainly due to the limited chronological constraints, especially beyond the 14C dating limits of accelerator mass spectrometry (AMS). The difficulty in establishing reliable chronostratigraphies is mainly attributed to low sedimentation rates and diagenetic sediment changes, resulting in very poor preservation of microfossils

The Pleistocene deposits capping fluvial terraces in the Bistrita valley (Eastern Carpathians, Romania) host a high density of Upper Palaeolithic (UP) settlements, rendering this area a type-region for Late Pleistocene cultural evolution in eastern Romania and beyond. Despite its archaeological significance, site formation, palaeoenvironmental contextualisation and chronostratigraphy are still insufficiently

The SP lava flow is a quartz-, olivine- and pyroxene-bearing basalt with an 40Ar/39Ar age of 72 ± 4 ka (2σ). The flow is preserved in the desert climate of northern Arizona, USA. Its unweathered appearance and the lack of soil development indicate it has undergone negligible erosion and/or burial, making it an ideal site for direct calibration of cosmogenic nuclide production rates. Cross-calibrated

The inter- and intra-crystalline fractions of Littorina littorea periwinkles recovered from archaeological sites in Northern Spain (covering the Azilian, Magdalenian and Solutrean periods) were examined for amino acid composition and racemisation over time. These fractions were found to be composed of similar proteins, as the amino acids and Asx D/L values were comparable and varied in the same way

The accuracy of ages produced by the U-Pb speleothem chronometer is influenced by initial disequilibrium effects resulting from weathering and transit of water through the epikarst. If some residual disequilibrium remains at the time of measurement, corrections can be made. However, once the system reaches equilibrium, the initial state has to be estimated thus propagating significant uncertainty into

Constraining past variations in rates of erosion remains a key challenge in geomorphology, as estimates of erosion rate on different timescales must be bridged. The Late Pleistocene to Holocene represents a key timescale for studying landscape transience, as climatic change, increasing anthropogenic activity, and/or tectonic activity changed the rate of surface processes in many landscapes. Few chronometers

We present a multidisciplinary dating approach - including radiocarbon, Uranium/Thorium series (U/Th), paleomagnetism, single-grain optically stimulated luminescence (OSL), polymineral fine-grain infrared stimulated luminescence (IRSL) and tephrochronology - used for the development of an age model for the Cañizar de Villarquemado sequence (VIL) for the last ca. 135 ka. We describe the protocols used

Glacial settings are considered to be the most challenging context for the application of luminescence dating. The optically stimulated luminescence (OSL) signal of quartz is often preferred for luminescence dating in partially-bleached settings as it resets (or bleaches) more rapidly in response to sunlight than the post-IR IRSL (pIRIR) signal of K-feldspar, and can therefore better characterise the

The luminescence characteristics and age estimates of nine samples of aeolian quartz are reported from the Southwood B section in the Arve Valley of southern Tasmania, Australia. New OSL and TT-OSL ages obtained from the deepest Tasmanian aeolian section found so far, the Southwood B section (>6 m deep), range from 20 ka (MIS 2) to 180 ka (MIS 6). Here we test two previously published TT-OSL protocols

Single Aliquot Regeneration (SAR) protocol has been routinely used to estimate palaeodose for sediment samples. However, it was observed that significant changes in the optically stimulated luminescence (OSL) sensitivity occur during read out of the natural OSL and that the current SAR protocol does not take into account these changes (Singhvi et al., 2011). It was suggested that if not corrected,

Oxygen isotope (δ18O) records of cave speleothem have played an important role in the past two decades in characterizing the Asian Monsoon (AM) variability and correlating the monsoonal events with other global climate events on millennial timescales. Of a series of millennial events occurred during the last glacial period, the Chinese Stadial-20 (CS-20, corresponding to the Greenland Stadial-20, GS-20)