Article Frontmatter was published on July 1, 2021 in the journal Holzforschung (volume 75, issue 7).

Identifying two anatomically similar species of Cupressaceae, Chamaecyparis obtusa and Thujopsis spp., is important to better understand the culture of wood use in Japan. However, the conventional method, which involves observing their cross-field pitting, cannot identify them in many cases. This study solves the above problem by introducing an anatomical criterion based on the micro fibril angle (MFA)

Plasma treatment is becoming a mature technique for modification of surfaces of various materials, including wood. A better insight in the treatment process and the impact of the plasma on properties of wood bulk are still needed. The study was performed on Norway spruce and common beech wood, as well as their thermally modified variations. The formations of the airborne discharge, as well as mass

Natural bamboo is rapidly replacing wood, but it is highly hygroscopic and has poor dimensional stability. Herein, Moso bamboo was subjected to hygrothermal treatment at different temperatures. The hydrophobicity and dimensional stability of bamboo increased, as indicated by the 16.5% decrease in volumetric swelling and three-fold increase in the contact angle at 220 °C. The fibers and parenchyma cells

As a natural graded material, bamboo has gradually increasing elastic modulus along the radial direction from the inner to the outer skin. Accurate measurement of the modulus distribution plays an important role in bamboo-based structural design. However, it is difficult to characterise this modulus distribution by using conventional testing approaches on bamboo slices. A more effective method was

Erosion bacteria are the main degraders of archaeological wood excavated from waterlogged environments. Light microscopy and analytical pyrolysis coupled with gas chromatography/mass spectrometry (Py-GC/MS) were exploited to study waterlogged archaeological wood ( Pinus sylvestris L.) at different stages of bacterial decay. The research explored the biochemical changes related to erosion bacteria degradation

In this study, an artificial neural network (ANN) model was designed to predict color change based on visual assessment of coated cross laminated timber (CLT) exposed outdoors. Coatings and stains were investigated based on ASTM protocols to assess wood surface visual rating, against checking, flaking, erosion, and mildew growth in the State of Mississippi (USA) during one year (2019–2020). It was

The goal of the study was to analyze fracture properties of adhesive bond using a three-point end-notched flexure test and the compliance-based beam method. Critical strain energy release rates ( G IIc ) and cohesive laws were obtained for adhesive bonds made of European beech ( Fagus sylvatica L . ) and adhesives such as EPI, MUF, PRF and PUR. The experiments were assisted with FE analyses employing

Waterborne polyurethane resins (WPUs) were prepared from polytetramethylene ether glycol (PTMG) and PTMG/polyhydric alcohol liquefied lignin (LL) with isophorone diisocyanate (IPDI), and ethylenediamine (EDA) and 1,4-butanediol (1,4-BD) were used as chain extenders. The effects of LL and the kind of chain extender on the properties of the WPU suspensions and dried films were studied. WPU suspensions

This study aimed to investigate the antioxidant ability and the chemical composition of apolar and polar extractives from Douglas-fir bark, cork and phloem, establishing a possible correlation with the structural variation along the tree stem and geographic location. Douglas-fir bark extractives’ composition were analyzed at three stem heights in trees from two locations. Cork and phloem extracts’

Article Frontmatter was published on June 1, 2021 in the journal Holzforschung (volume 75, issue 6).

This study applied synchrotron radiation XRD to analyze the mechanical behavior of cellulose microfibrils in wood containing annual rings (thickness: 5 mm), for different layers of the secondary cell wall, under uniaxial load. Cellulose in S 2 and in S 1 and S 3 layers were analyzed respectively, and the data were used to investigate for deformation behavior in the lattice spacing ( d 004 ). As a result

Basic density is a fundamental wood property of pulp and sawn wood. An IML Resi PD 400 drilling resistance tool (IML System GmbH, Wiesloch, Germany) was used to evaluate the basic density of Eucalyptus nitens discs and the impact of needle friction on basic density prediction. To determine the accuracy of that prediction with the commonly used linear drill bit shaft friction correction and determine

This paper examines how the moisture conditioning method affects the electrical conductance of wood. A widely used dataset was acquired by Stamm in 1929 who used a method of conditioning where water-saturated wood specimens were partially dried, sealed and left for a period of time for moisture to be redistributed before the electrical conductance was measured. However, more recent measurements combined

A 3D combined elastic-plastic damage constitutive model for wood is proposed within the theoretical framework of classical plasticity and continuum damage mechanics (CDM). The model is able to describe the various behavior of wood under loading, including the orthotropic elasticity, strengths inequality under tension and compression in each orthotropic direction, ductile softening under longitudinal

In this work, a novel waterborne hyperbranched polyacrylate (HBPA) dispersed organo-montmorillonite (OMMT) emulsion was synthesized and used for the treatment of wood in a vacuum environment in order to enhance the physical and mechanical properties of the wood. The sapwood of Cathay poplar ( Populus cathayana Rehd.) and Radiata pine ( Pinus radiata D.Don) were used as the samples for experimentation

The moisture-induced recovery of compressed wood is one of the major problems of wood densification technology. Achieving a cost-efficient surface densification process without the need for additional resins to eliminate the set-recovery may lead to an increase in value of low-density wood species. A previous study has shown that a pre-treatment with ionic liquids (ILs) can nearly eliminate the set-recovery

The effectiveness of pressurized hot-water extraction conditions for obtaining galactoglucomannans (GGMs) from Pinus halepensis suitable for applications like coatings and films packaging was investigated. For this purpose, high molar masses with high yields are required, presenting a serious challenge for hot-water extraction processes. The extraction of GGMs was carried out in an accelerated solvent

Treating wood with water-soluble resins is a well-known and effective method to improve the durability of wood. However, there has been no systematic work to date related to the influence of average molecular size of phenol-formaldehyde (PF) resin on the decay resistance of wood, especially of hardwoods. Therefore, the goal of this study was to investigate the effect of average molecular size of PF

Polyolefins used in building materials and furniture require the use of flame-retardant (FR) additives to improve their fire safety. Such additives should be safe to humans and the environment, and preferably bio-based. In the present work, the FR performance of unmodified and chemically modified technical lignins was compared to that of the ammonium polyphosphate/pentaerythritol (APP/PER) intumescent

Article Frontmatter was published on May 1, 2021 in the journal Holzforschung (volume 75, issue 5).

The establishment of agroforestry systems (AFS) is a consistent strategy to integrate sustainable supply of wood, food and environmental services in a single land plot. Teak ( Tectona grandis Linn. F.) is an interesting option for the tree component in AFS, though there is a lack of information on its potential. This study aimed to characterize the quality of teak wood produced in an AFS regarding

Although visible and near-infrared (Vis-NIR) spectroscopy can rapidly and nondestructively identify wood species, the conventional spectrometer approach relies on the aggregate light absorption due to the chemical composition of wood and light scattering originating from the physical structure of wood. Hence, much of the work in this area is still limited to further spectral pretreatments, such as

Young’s modulus in the longitudinal direction was measured by a longitudinal vibration (LV) test on western hemlock specimens with various length/width ratios. The effects of the configuration and orthotropy of the specimen on the measurement of Young’s modulus was investigated through subsequent finite element (FE) calculations. The experimental results suggested that Young’s modulus could not be

Anisotropic shrinkage is a typically feature in wood, which is of critical importance in wood drying. In this study, the shrinkage strains over each growth ring were determined by a full-field strain measurement system during moisture content (MC) loss. Color maps were used to visualize the full-field distribution of displacement and shrinkage strain under different MC conditions. The variation of

The purpose of this study was to determine the applicability of methyl methacrylate (MMA) and MMA–styrene in treating batai ( Paraserianthes falcataria ) wood. The effectiveness of the treatment was evaluated based on Fourier transform infrared spectroscopy (FTIR) analysis, physico-mechanical properties of the treated wood, and moisture sorption isotherm using dynamic vapour sorption (DVS) apparatus

Esterified phenolics occur as γ -linked lignin acylations in many plant taxa but little is known about the distribution or function of such groups. In the family Salicaceae, p -hydroxybenzoate groups are present in the lignin of poplars ( Populus spp.) and willows ( Salix spp.). In this study, the distribution of cell wall-bound p -hydroxybenzoate was examined in different tissue and cell types of

Lignin nanoparticles (LNPs) from lignocellulosic biomass are expected to become promising basic building blocks for various applications in the development of multifunctional nanocomposites. Facile green preparation of LNPs and their application in polyvinyl alcohol (PVA) composite films were studied in this paper. LNPs were produced by performing fractionation of wheat straws at less than 80 °C with

Mass loss (ML) of wood caused by thermal degradation is one of the most important features of the thermal treatments and referred to as an indicator of intensity and quality of the process. The ML is proportional to the quantity of the effective heat power exchanged during the treatment process, represented by the area of the temperature profile versus time during the process. In this paper a model

The dimensional instability and inferior mechanical strength of radiata pine ( Pinus radiata D. Don) limit its use in musical instruments. To improve its properties, a two-step treatment by furfuryl alcohol (FA) and tung oil (TO) were used involving impregnation of FA precursor solution into the wood matrix, forming a highly cross-linked resin, followed by a modification with TO. Examination using

With the growing popularity in digital systems and electronic communication equipment, there is an urgent need to develop lightweight, green, and efficient electromagnetic interference (EMI) shielding materials to handle the increasingly serious problem of radiation pollution. Herein, Ti 3 C 2 T x (MXene)/natural wood (NW) composites were prepared using a vacuum-pulse impregnation method and characterized

Article Frontmatter was published on April 1, 2021 in the journal Holzforschung (volume 75, issue 4).

“Non-Fickian” diffusion of wood moisture refers to the unexplained anomalous behaviour of water vapour sorption in wood. The depression of moisture diffusion rates in thin sections of wood tissue during moisture content change at high relative humidity is one of the least-understood aspects of “non-Fickian” diffusion. In a previous work, a rate-limiting effect by two cooperative couplings of moisture

The objective of this work was to provide a rapid and nondestructive imaging method for evaluating the hygroscopic behavior of thermally modified lignocellulosic materials (softwood and hardwood). The difference in the hygroscopic behavior was explained by moisture content (MC) mapping results and molecular association characteristics of absorbed water (i.e. weakly, moderately, and strongly hydrogen-bonded

In this study, the effect of thermo-mechanical densification on the density, hardness, compression strength, bending strength (MOR), and modulus of elasticity (MOE) of fir and aspen wood pretreated with water repellents was analyzed. Wood specimens were impregnated with paraffin, linseed oil and styrene after pre-vacuum treatment. Then, the impregnated wood specimens were densified with compression

The conformation of lignin in solvents is major key factors governing the physicochemical properties of aromatic polymers. However, the conformational changes of lignin in good and poor solvents is not clearly understood at the molecular level. In this study, short- (DP 2.77) and long-chain (DP 4.49) lignin oligomer model compounds composed solely of interunit β– O –4 bonds with a narrow polydispersity

To improve the reactivity of lignin for incorporation into high value polymers, the introduction of amines via Mannich reaction is a commonly used strategy. During this functionalization reaction, intra- as well as intermolecular lignin–lignin crosslinking occurs, which can vastly change the elastic properties of the lignin, and therefore, the properties of the resulting polymer. Therefore, the molecular

An efficient separation technology for hydrolysates towards a full valorization of bamboo is still a tough challenge, especially regarding the lignin and lignin-carbohydrate complexes (LCCs). The present study aimed to develop a facile approach using organic solvent extraction for efficiently fractionating the main components of bamboo hydrolysates. The high-purity lignin with only a trace of carbohydrates

Article Frontmatter was published on March 1, 2021 in the journal Holzforschung (volume 75, issue 3).

This review compiles various literature studies on the environmental impacts associated with the processes of thermal modification of wood. In wood preservation field, the wood modification by heat is considered as an ecofriendly process due to the absence of any additional chemicals. However, it is challenging to find proper scientific and industrial data that support this aspect. There are still

This study aims at identifying the mechanisms of oil and water imbibition in heartwood and sapwood of Douglas-fir through a combination of original experiments with magnetic resonance imaging (MRI) and nuclear magnetic resonance (NMR) relaxation measurements for oil and free water, and deformation measurements for bound water. Experiments by weighing are performed to verify whether the imbibition process

The aim of this research was to explore the potential of acoustic impact test to evaluate the condition of hardwood logs in regard to internal decay, void, crack and defect ratio using an acoustic signal separation and enhancement algorithm. Longitudinal acoustic signals were obtained from 15 logs of four hardwood species through acoustic impact testing. The defect components were separated from the

A combination of alkaline thermal pretreatment followed by thermomechanical extrusion was studied as a novel sequential pretreatment process for an effective breakdown of the lignocellulosic structure of Eucalyptus grandis wood (EW). The first step was studied by analysing the influence of two factors: the NaOH-to-dry biomass ratio or NaOH loading (NaOH/DM) and the liquid-to-solid ratio (L/S). Optimization

Numerous investigations on the antioxidant properties of different plant tissue extracts are available in literature, but few studies on the effect of thermally modified wood on secondary metabolites were carried out up to now. This study highlights the influence of the thermal modification of Castanea sativa Mill. wood on total content of antioxidant compounds and consequently on its antioxidant activity

It is frequently observed that bamboo particle composites (BPCs) do not show higher mechanical performances than the corresponding wood particles composites (WPCs), although bulk bamboo is much stronger than wood in mechanical performances. Herein this phenomenon was demonstrated from the cell compositions in the applied bamboo particles. To address that, a simple method to physically separate bamboo

Samples of Scots pine sapwood were treated with epoxidized linseed and soybean oils to improve decay, insect and termite resistance of wood. Non-epoxidized (raw) linseed and soybean oils were included as reference treatment in the study. In the epoxidation process, hydrogen peroxide was used to open double bounds, and acetic acid was added as a catalyst. Two retention levels, Ret A (80–140 kg m −3

In this study, a simple and effective method for preparing bamboo with high fungal resistance was first proposed. Flattened moso bamboo ( Phyllostachys pubescens ), which is a perishable species, was connected to a silver plate and exposed to a high-voltage electrostatic field (HEVF). The method was based on HEVF excitation of a silver plate to produce silver ions and facilitate in situ impregnation

Abstract The paper presents a novel approach to determine charring of wood exposed to standard and natural fire that is based on a new numerical model named PyCiF. The new model couples an advanced 2D heat-mass model with a pyrolysis model. A new charring criterion based on a physical phenomenon is implemented in the PyCiF model to determine charring of wood. This presents the main advantage of the

Abstract Density of wood can be increased by filling its porous structure with polymers. Such densification processes aim to increase hardness of wood and are particularly interesting for flooring applications. This study aims to evaluate efficiency of different polymers for chemical densification based on the polymer properties. Yellow birch (Betula alleghaniensis Britt.) was chemically densified

Abstract This study reports a new cellulosic material that maintains the original three-dimensional structure of bamboo and is produced by optimization of chemical treatments. Bamboo blocks were prepared from the current year culms of moso bamboo (Phyllostachys edulis) and subjected to three chemical treatments alone or in combination. Based on the color changes and Fourier transform infrared spectra

Abstract It is well known the properties of resin impregnation wood is significantly influenced by the specific distribution pattern of resin in the modified wood. In this work, bamboo was furfurylated with an improved process. In addition to testing and evaluating its main physical, mechanical and durable properties, it was explored how the furfuryl alcohol (FA) resin is distributed in the furfurylated

Abstract Inorganic impregnation strengthening of Chinese fir wood was carried out to improve the strength, dimensional stability, flame retardancy, and smoke suppression of Chinese fir wood. Sodium silicate was used as reinforcement, a sulfate and phosphate mixtures were used as a curing agent, and Chinese fir wood was reinforced by the respiratory impregnation method (RIM) that imitating human respiration

Abstract The effect of wollastonite on the wetting properties of welded Scots pine-joints was studied using the multicycle Wilhelmy plate method and by observation of the chemical composition of the welded joints. Welding pine with wollastonite for 5 s resulted in a decrease in the water uptake and the swelling, and an increase in the contact angle of the welded joint compared to welded wood without

Abstract Whether water sorption hysteresis exists above 75 °C and the representation of its relationship with wood softening remains unclear. In this study, sorption hysteresis at three temperature levels, namely, 75, 90 and 99.5 °C, was investigated using accurately controlled conditioning chambers using powder samples from seven wood species. The dry mass loss percentage of the samples and proper

Abstract Natural constituents of wood cell-wall layers are affected in various ways by thermal treatment. This study investigated the effect of high-temperature treatment on the properties of cell-wall layers. The properties were studied using PeakForce quantitative nanomechanical mapping and Fourier-transform infrared spectroscopy (FTIR). European beech wood was thermally treated at 200 °C for 1,

Abstract The aim of this study was to evaluate the characteristics of radio-frequency/vacuum combined with mechanical press (RF/VP) drying on three softwood timbers (Douglas fir, Hemlock, and Radiata pine) with longitudinal kerfs. The results were as follows: Due to the dielectric permittivity of wood, RF/VP drying at a fixed frequency of 13.56 MHz significantly influenced the moisture content (MC)

Abstract In this study, oriented bamboo scrimber board (OBSB) was manufactured with a synthesized formaldehyde-free tannin adhesive. The chemical properties of the tannin adhesive were analyzed with 13C nuclear magnetic resonance spectroscopy (13C-NMR) and diffuse reflectance infrared Fourier transform spectroscopy (DRIFT). Results revealed that 70% aqueous acetone extractives of Acacia confusa bark

Journal Name: Holzforschung Volume: 75 Issue: 2 Pages: i-iii

In this paper, voxel-based finite element modelling based on spatial geometry and density data is applied to simulate the detailed stress and strain distribution in a large wood element. As example, a moulded wooden tube with a length of 3 m and a diameter of 0.3 m is examined. Gamma-ray computed tomography is used to obtain both, its actual geometric shape and spatial density distribution. Correlation

Microfibril angle (MFA) is a key biological trait contributing to wood stiffness, which is a common breeding objective for solid wood products in many tree species. To explore its genetic architecture, area-weighted MFA was measured in two Eucalyptus nitens progeny trials in Tasmania, Australia, with common open-pollinated families. Radial strips were extracted from 823 trees in 131 families and MFA