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Transition-metal-free [3+3] annulation reaction of sulfoxonium ylides with cyclopropenones for the synthesis of 2-pyrones Green Synth. Catal. Pub Date : 2020-12-1 Maoyao He , Yuncan Chen , Yi Luo , Jianglian Li , Ruizhi Lai , Zengbao Yang , Yuerong Wang and Yong Wu
An efficient and practical synthetic approach was developed for the tandem synthesis of trisubstituted 2-pyrone derivatives from sulfoxonium ylides and cyclopropenones. This [3?3] annulation reaction was carried out under transition-metal-free conditions. A broad range of functional groups were tolerant under mild conditions, and a variety of 2-pyrones were obtained in moderate to good yields.
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Late-stage diversifi cation by rutheniumelectro-catalyzed C¨CH mono- and di-acyloxylation Green Synth. Catal. Pub Date : 2020-12-1 Haiwei Shen , Didi Cheng , Yujin Li , Tao Liu , Xiao Yi , Lei Liu , Fei Ling and Weihui Zhong
A ruthenium-catalyzed electrochemical dehydrogenative C(sp2) H acyloxylation of aniline derivatives with carboxylic acids has been developed. Electric current is used to recycle the active ruthenium-based catalyst and promote H2 evolution. This method significantly expands the scope and enhances the selectivity of metal-electron catalyzed mono- and di-acyloxylations, which remain challenged. Our findings
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Rh(III)-catalyzed direct cross-dehydrogenative coupling of aromatic nitriles with heteroarenes: Rapid access to biheteroaryl-2-carbonitriles Green Synth. Catal. Pub Date : 2020-12-1 Huibei Xu , Yanying Zhu , Xinyue Chai , Jiahui Yang and Lin Dong
Transition-metal-catalyzed direct C¨CH/C¨CH cross-coupling reactions as efficient and atom-economical approaches have been widely used to build up complex heterocyclic compounds. However, the strategy for preparation of biphenyl-2-carbonitriles has not been well established. Herein, we described the first cyanogen directed Rh(III)- catalyzed CDC reaction of aromatic nitriles with heteroarenes. Various
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Ortho-(1-phenylvinyl)benzyl glycosides: Ether-type glycosyl donors for the effi cient synthesis of both O-glycosides and nucleosides Green Synth. Catal. Pub Date : 2020-12-1 Penghua Li , Haiqing He , Lili Xu , Yingying Huang , Zixi Chen , Yunqin Zhang , Rui Yang and Guozhi Xiao
Both O-glycosides and nucleosides are essential biomolecules with important roles in a variety of biological processes. Chemical synthesis of both O-glycosides and nucleosides is a scalable and reliable method to develop new therapeutic agents and decipher their functions. However, the efficient synthesis of both O-glycosides and nucleosides remains one of long-standing challenges in chemical synthesis
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Mechanistic elucidation of the role of metal oxidation states in nickel mediated electrocatalytic coupling of benzyl halides Green Synth. Catal. Pub Date : 2020-12-1 Pradip K. Das , Priyanka Chakraborty , Sandeep Suryabhan Gholap , Th¨¦o P.Gon?alves , Changguang Yao , Huaifeng Li , Zhiping Lai , Abdul-Hamid Emwas and Kuo-Wei Huang
We present the mechanistic understanding of an electrochemically-driven nickel-catalyzed coupling reaction. Computational analysis reveals that the spin density is mostly residing on the nickel (Ni) center when NiII is reduced to NiI. Ni-mediated halogen atom abstraction through outer-sphere electron-transfer pathway to yield coupling products under mild conditions is demonstrated. Importantly, we
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Redesign of a short-chain dehydrogenase/reductase for asymmetric synthesis of ethyl (R)-2-hydroxy-4-phenylbutanoate based on per-residue free energy decomposition and sequence conservatism analysis Green Synth. Catal. Pub Date : 2020-12-1 Bingmei Su , Lian Xu , Xinqi Xu , Lichao Wang , Aipeng Li , Juan Lin , Lidan Ye and Hongwei Yu
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Synthesis of -tertiary allylsilanes by palladium-catalyzed hydrosilylation of 1,1-disubstituted allenes Green Synth. Catal. Pub Date : 2020-12-1 Kaidi Li , Ming Nie and Wenjun Tang
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Catalytic asymmetric Catellani-type reaction: A powerful tool for axial chirality construction Green Synth. Catal. Pub Date : 2020-12-1 Yue Dong , Renshuai Liu and Wei Wang
This highlight summarizes a recent development of a catalytic enantioselective Catellani-type reaction for the synthesis of axially chiral biaryls. The chirality induction is solely governed by chiral norbornene ligand in the Pd mediated ortho C¨CH functionalization and ipso cross-coupling transformation. The preparative power of the methodology is demonstrated as a powerful manifold for the divergent
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Stereoselective fl uoroarylation of 1,1-difl uoroallenes enabled by palladium catalysis Green Synth. Catal. Pub Date : 2020-12-1 Huanhuan Luo , Yunfei Zhao , Dawei Wang, Minyan Wang and Zhuangzhi Shi
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Radical azidation as a means of constructing C(sp3)-N 3 bonds Green Synth. Catal. Pub Date : 2020-12-1 Liang Ge , Mong-Feng Chiou , Yajun Li and Hongli Bao
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Transition-metal catalyzed asymmetric reactions under continuous flow from 2015 to early 2020 Green Synth. Catal. Pub Date : 2020-7-29 Jingyuan Liao , Shilong Zhang , Zesheng Wang , Xiao Song , Dongliang Zhang , Ravi Kumar , Jian Jin , Peng Ren , Hengzhi You and FenEr Chen
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Perspectives on green synthesis and catalysis Green Synth. Catal. Pub Date : 2020-07-27 Yiram Kim; Chao-Jun Li
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Asymmetric catalysis in synthetic strategies for chiral benzothiazepines Green Synth. Catal. Pub Date : 2020-07-27 Haifeng Wang; Shuangxi Gu; Qiongjiao Yan; Li Ding; Fen-Er Chen
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Asymmetric catalytic hydrogenation of imines and enamines in natural product synthesis Green Synth. Catal. Pub Date : 2020-07-27 Pei Tang; Huijing Wang; Wen Zhang; Fen-Er Chen
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Recent advances in visible-light photoredox-catalyzed nitrogen radical cyclization Green Synth. Catal. Pub Date : 2020-07-27 Pengzi Wang; Quanqing Zhao; Wenjing Xiao; Jiarong Chen
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Biosynthesis of organic molecules via artificial cascade reactions based on cytochrome P450 monooxygenases Green Synth. Catal. Pub Date : 2020-07-27 Ren-Jie Li; Zhongwei Zhang; Carlos G. Acevedo-Rocha; Jing Zhao; Aitao Li
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Structure-guided protein design of fluoroacetate dehalogenase for kinetic resolution of rac-2-bromobutyric acid Green Synth. Catal. Pub Date : 2020-07-27 Shu Wang; Zhanbing Cheng; Yanbing Xu; Lu Yang; Jian-Bo Wang; Zhenhua Tian; Xudong Qu
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One-pot synthesis of salicylaldehyde containing biaryl frameworks via an aminocatalytic Diels-Alder-retro-Diels-Alder cascade reaction of ynals with 2-pyrones Green Synth. Catal. Pub Date : 2020-07-27 Xixi Song; Yueteng Zhang; Peng Ji; Fanxun Zeng; Fangchao Bi; Wei Wang
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Radical coupling of β-ketoesters and amides promoted by Brønsted/Lewis acids Green Synth. Catal. Pub Date : 2020-07-27 Joshua L. Zhu; Stephen W. Laws; Michael J. Rourke; Karl A. Scheidt
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Robust NHC-palladacycles-catalyzed Suzuki−Miyaura cross-coupling of amides via C-N activation Green Synth. Catal. Pub Date : 2020-07-27 Qinyue Deng; Qingshu Zheng; Bin Zuo; Tao Tu
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Primary amine-functionalized mesoporous phenolic resin as an effective and stable solid base catalyst for Knoevenagel reactions in water Green Synth. Catal. Pub Date : 2020-07-27 Kaixuan Wang; Huating Jiang; Min Tong; Yao Xiao; Hexing Li; Fang Zhang
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Catalytic asymmetric Catellani-type reaction: A powerful tool for axial chirality construction Green Synth. Catal. Pub Date : 2020-09-26 Yue Dong; Renshuai Liu; Wei Wang