The purpose of this study was to evaluate the mechanical strength and biodegradation of a ZK60 plate coated with poly(l-lactic)-acid polymer (PLLA) in a LeFort I osteotomy canine model for maxillofacial applications. The PLLA-coated ZK60 plate and screw were evaluated using a LeFort I osteotomy canine model based on five beagles. The presence of wound dehiscence, plate exposure, gas formation, inflammation

The effect of doping the ferrite alloy Fe-16Cr by the oversized impurities Sb and Au on the mechanism of the short-range ordering induced by “warm” severe plastic deformation was studied using the method of Mössbauer spectroscopy. A comparison between the results obtained and the positron annihilation data on the evolution of the defects of vacancy type stabilized by the impurities Sb and Au was performed

Despite the dominance of the blast furnace ironmaking process, more attention is being paid to the new technologies with lower energy consumption and carbon dioxide emissions. A novel flash ironmaking technology using pulverized coals and iron concentrates as raw materials, which is different from flash ironmaking with the reductive gas as the reducing agent, is studied. In order to obtain the flow

In pyrometallurgical processes refining copper, the main source of loss in the conversion stage is from slag. This paper reports on research work treating converter slag containing high percentages of copper (36 wt%) using ammonium hydroxide at room temperature. Variables analyzed are solution pH, agitation, temperature, NH4OH concentration and particle size. Results showed that the hydronium ion resulting

The present study is devoted to extending Barlat’s famous yield criteria to tension–compression asymmetry by a novel method originally introduced by Khan, which can decouple the anisotropy and tension–compression asymmetry characteristics. First, Barlat (1987) isotropic yield criterion, which leads to a good approximation of yield loci calculated by the Taylor–Bishop–Hill crystal plasticity model,

Welding is a widely used process that requires continuous developments to meet new application demands of mechanical projects under severe conditions. The homogeneity of metallurgical and mechanical properties in welded joints is the key factor for any welding process. The applications of external magnetic fields, mechanical vibration, and ultrasound are the fundamental steps to achieve success in

In this work, the effect of drawing pass on the surface layer softening or plasticizing of Q235 steel bar during electrochemical cold drawing (ECD) was studied, as well as cold drawing in air (DIA) for comparison. The results indicate that the softening or plasticizing degree gradually decreases with increasing drawing pass. The reason for this should be that dislocations generated in surface layer

Nowadays, composite materials are playing an increasingly important role in material forming processes because they can combine remarkable physical and mechanical properties with relatively low weight. The main objective of this work is to study the forming behaviour of multi-layer sheets by finite element analysis. The possibility of replacing the composite by a single equivalent material, with a

Optimization of the schedule is an effective way to reduce energy consumption in hot strip manufacturing. The heating energy and the rolling energy contribute the vast majority of the energy consumption. In order to reduce the energy consumption for the whole process, an optimization method based on the multi-objective function was applied, and the heating energy and rolling energy were both taken

Active brazing of zirconia with metallic alloys is a promising method for enhancing the mechanical property of zirconia. However, the brazing process of zirconia and metallic alloys has not been studied in detail because of a limitation in selection of materials and processing conditions. Here, we successfully brazed zirconia with Ti-3Al-2.5V alloy using amorphous Zr54Ti22Ni16Cu8 active filler alloy

This paper presents thermochemical synthesis of copper/alumina nanocomposites in a Cu-Al2O3 system with 1–2.5 wt.% of alumina and their characterization, which included: transmission electron microscopy: focused ion beam (FIB), analytical electron microscopy (AEM) and high resolution transmission electron microscopy (HRTEM). Thermodynamic analysis was used to study the formation mechanism of desirable

A novel semi-dieless bellows forming process with a local heating technique and axial compression has been initiated for the past years. However, this technique requires a high difficulty in maintaining the output quality due to its sensitivity to the processing conditions. The product quality mainly depends on not only the temperature distribution in the radial and axial direction but also the compression

A new concept for copper (Cu) metal leaching by the simultaneous use of cupric ions (Cu2+) and oxygen (O2) was proposed to improve Cu metal leaching in sulfuric acid. According to this concept, Cu2+ oxidizes Cu metal into cuprous ion (Cu+), and O2 oxidizes Cu+ into Cu2+. The improvement in Cu leaching efficiency from Cu metal was investigated experimentally in the sulfuric acid solution using Cu2+

This study investigated the critical high-temperature deformation of the low-lead (Pb) Cu38Zn3Pb alloy. Moreover, the dezincification mechanism of this alloy for high-temperature applications was evaluated. The results reveal that tensile temperatures influence the phase structures of the brass alloy matrix. Many voids and holes formed at the phase boundaries above 400 °C due to the hard-brittle b’

There are multiple references to sample cleaning methods prior to hydrogen content determination, or hydrogen spectroscopy analysis, but there is still no unified criteria; different authors use their own “know-how” to perform this task. The aim of this paper is to solve, or at least clarify, this issue. In this work, the most commonly used sample cleaning methods are compared. Then, five different

In this study, a new method is proposed for the plasticization of inclusions by taking advantage of the behavior of alkali metals in lowering the inclusion melting point. A series of experiments with NaF additions to molten steel were carried out using a carbon tube furnace followed by simulated rolling tests using the solidified ingots and characterization of inclusions with the help of automated

The metal titanium (Ti) and its alloys have many attributes which are attractive as structural materials, but they also have one major disadvantage, high initial cost. Nevertheless, Ti and Ti alloys are used extensively in airframes, gas turbine engines (GTE), and rocket engines (RE). The high cost is a deterrent, particularly in airframe applications, in that the other alloys it competes with are

In this study, a new-generation high-strength and high-ductility medium Mn steel (0.1C-5Mn-Fe) for the automotive industry was joined by the fiber laser and gas tungsten arc welding (GTAW) methods. Formability testing of the welded joints was done by the Erichsen cupping test and finite element (FE) analysis. The results showed that the formability of medium Mn steel welded joints was sensitive to

The effect of temperature, time and rotation speed of FT-GTL process water on the corrosion rate of API X-120 carbon steel was investigated. Electrochemical impedance spectroscopy and potentiodynamic polarization techniques were used to determine the carbon steel corrosion rate under temperatures ranging from 293 to 323 K and rotation speed of 0, 500, 1000, 2000 rpm when the immersion time was 0.5

The gas metal arc welding (GMAW) process was used to weld 3003-H14 plates under restricted and unrestricted thermal expansion. Experimental and numerical analysis were conducted to determine the relation between weld thermal cycles and residual stresses. A customized data acquisition system with K-type thermocouples was used to measure the weld thermal cycles, while residual stresses were determined

This article is focused on an analysis of factors negatively affecting the tube production process of tubes made from austenitic stainless steel with a very small diameter of 0.34 mm. The analysis was concentrated on factors that affect the drawing process stability of the seam tubes where the desired final dimensions—a diameter of 0.34 mm and a wall thickness of 0.057 mm—are limiting factors. Seam

Imperfections due to the manufacturing process can significantly affect the local fatigue strength of the bulk material in cast aluminium alloys. Most components possess several sections of varying microstructure, whereat each of them may inherit a different highly-stressed volume (HSV). Even in cases of homogeneous local casting conditions, the statistical distribution parameters of failure causing

Ever since humans engaged in directed manufacturing activities to make tools and utensils[…]

Wire Arc Additive Manufacturing (WAAM) features high deposition rates and, thus, allows production of large components that are relevant for aerospace applications. However, a lot of aerospace parts are currently produced by forging or machining alone to ensure fast production and to obtain good mechanical properties; the use of these conventional process routes causes high tooling and material costs

A potential new bactericide treatment for NiTi orthodontic archwires based in the electrodeposition of silver nanoparticles on the surface was studied. Twenty-five archwires were treated by electrodeposition, obtaining nanoparticles of silver embedded on the archwire surface. These were evaluated in order to investigate the possible changes on the superelastic characteristics (critical temperatures

Currently, high-speed steel (HSS) powders are deposited locally on a metal surface through direct energy deposition (DED) onto hardface tool steel. Although the HSS powder enhances the hardness and the abrasion resistance of a metal surface, it makes the tool steel brittle because of its high carbon content. In addition, the steel is likely to break when subjected to a high load over time. This study

In continuous casting, the nozzle position may deviate from the center under actual operating conditions, which may cause periodic fluctuation of the steel-slag interface and easily lead to slag entrapment and gas absorption. Swirling nozzles can reduce these negative effects. A mathematical simulation method based on a round mold of steel components with a 600 mm diameter is applied to study the flow

The 440C martensitic stainless steel is considered to be among the hardest steels, owing to its high carbon content. Careful heat treatment of this material introduces multiple carbide particles, which can alter microstructure and mechanical properties. This study focused on the effect of austenitisation temperature on the microstructure and tensile properties of 440C steel. Austenitisation was performed

The effects of interstitials on the mechanical properties of single-phase f.c.c. high entropy alloys (HEAs) have been assessed based on a review of the literature. It is found that in nearly all studies, carbon increases the yield strength, in some cases by more than in traditional alloys. This suggests that carbon can be an excellent way to strengthen HEAs. This strength increase is related to the

A compositional and crystallographic study was carried out on the Smy(FexNi1−x)4Sb11.5Sn0.5 filled skutterudite system (0.40 ≤ x ≤ 0.80) with the aim to determine the equilibrium Sm filling fraction (y) within the considered x range. The relevance of the material lies in its potential thermoelectric properties: in analogy with similar skutterudites systems, these features should in fact result as being

In this work, the carbothermic reduction of iron- and zinc-bearing products is studied through in situ microwave heating, dielectric properties monitoring, and mass spectrometry up to high temperatures (1000 °C). The results are correlated to the information provided by conventional analysis techniques such as differential scanning calorimetry (DSC) and thermogravimetry (TG). This combination allows

A great variety of powder metallurgy techniques can produce biomimetic porous titanium structures with similar mechanical properties to host bone tissue. In this work, loose sintering and space holder techniques, two frequently used metallurgical techniques, are compared to evaluate the influences of porosity (content, size, morphology and wall roughness), mechanical properties (stiffness and yield

An improved shielding structure of a bumper that constructed from Ti/Al/Mg density-graded materials was presented. Two types of Ti/Al/Mg density-graded materials with the same areal density were prepared by diffusion bonding and powder metallurgy, respectively. The characteristics of hypervelocity impact including penetration holes in the bumper, damage patterns on the rear wall and micrographs of

Boron is a unique and popular grain refiner element in cast titanium aluminide (TiAl) alloys, as it helps to improve mechanical properties if properly alloyed. However, the formation mechanism of different types of borides in cast TiAl alloys is not yet clearly understood. This study seeks to correlate the chemical composition and cooling rate during solidification of cast TiAl alloys, with the type

Adhesive joints between dissimilar layers of metals and composites are increasingly used by different industries, as they promise significant weight savings and, consequently, a reduction in energy consumption and pollutant emissions. In the present work, the interfacial fracture behavior of a new titanium–carbon fiber reinforced plastic (CFRP) adhesive joint is experimentally investigated using the

The use of bolted joints to connect the transition piece and monopile is nowadays widely applied in the offshore wind industry. Traditionally, grouted connections were used in the early generation of offshore wind turbines, but the experienced failures in such connections led to an increased tendency towards bolted flange connections to join the transition piece and monopile in the new generation of

This work is aimed at the analysis of the dynamic resistance, electrical energy and behavior of the force between electrodes (including thermal expansion) during welding at optimized parameters, referring to the process of spot welding using additive manufacturing (AMSW). For comparative purposes, this analysis also includes the conventional resistance spot welding process (RSW). The experiments were

Additive manufacturing (AM) processes have undergone significant progress in recent years, having been implemented in sectors as diverse as automotive, aerospace, electrical component manufacturing, etc. In the medical sector, different devices are printed, such as implants, surgical guides, scaffolds, tissue engineering, etc. Although nowadays some implants are made of plastics or ceramics, metals

The kinetic features of solvent and solid-phase extraction of yttrium and iron (III) from simulated and industrial phosphoric acid solutions are revealed. Di-2-ethylhexylphosphoric acid (D2EHPA) was used as a liquid extractant, and D2EHPA-containing Levextrel resin—a co-polymerization product of styrene and divinylbenzene in the presence of D2EHPA—was used as a solid-phase extraction agent. Significant

The one-dimensional analytical model was promoted to help select the creep constitutive equation and predict heat treatment temperature in a ferritic welded structure, along with neglecting the impact of structural constraint and deformation compatibility. The analytical solutions were compared with simulation results, which were validated with experimental measurements in a ferritic welded rotor.

An AZ91 magnesium alloy (Mg-9%, Al-1% Zn) was processed by high-pressure torsion (HPT) after solution-heat treatment. Tensile tests were carried out at 423, 523, and 623 K in the strain rate range of 10−5−10−1 s−1 to evaluate the occurrence of superplasticity. Results showed that HPT processing refined the grain structure in the alloy, and grain sizes smaller than 10 µm were retained up to 623 K. Superplastic

Metal additive manufacturing (AM) works on the principle of consolidating feedstock material in layers towards the fabrication of complex objects through localized melting and resolidification using high-power energy sources. Powder bed fusion and directed energy deposition are two widespread metal AM processes that are currently in use. During layer-by-layer fabrication, as the components continue

The use of titanium hydride as a raw material has been an attractive alternative for the production of titanium components produced by powder metallurgy, due to increased densification of Ti compacts, greater control of contamination and cost reduction of the raw materials. However, a significant amount of hydrogen that often remains on the samples could generate degradation of the mechanical properties

Step rolling can be used to mass-produce ultrafine-grained (UFG) Ti-6Al-4V sheets. This study clarified the effect of subsequent annealing on the tensile properties of step-rolled Ti-6Al-4V at room temperature (RT) and elevated temperature. The step-rolled alloy retained its UFG structure after subsequent annealing at 500–600 °C. The RT ductility of the step-rolled alloy increased regardless of annealing

In the hot strip rolling (HSR) process, accurate prediction of bending force can improve the control accuracy of the strip crown and flatness, and further improve the strip shape quality. In this paper, six machine learning models, including Artificial Neural Network (ANN), Support Vector Machine (SVR), Classification and Regression Tree (CART), Bagging Regression Tree (BRT), Least Absolute Shrinkage

When grinding hard-to-machining materials such as titanium alloys, a massive grinding heat is generated and gathers in the grinding zone due to the low thermal conduction of the materials. The accumulated grinding heat easily leads to severe thermal damages to both the workpiece and the grinding wheel. A novel oscillating heat pipe (OHP) grinding wheel is one of the solutions to this phenomenon. The

The present work is aimed at refining the grain size in the Co–28Cr–5Mo–0.3C (wt%) cast alloy using particle-stimulated nucleation (PSN) of recrystallization. It is pointed out that PSN resulted in considerable grain refinement (≈80%) of the as-cast structure, leading to an increased yield and tensile strength (around 30%). Partial solutionizing is associated with the formation of γfcc and athermal

A novel high C high Si carbide free bainitic steel was developed for the production of cold work tools, knives, and rolls, requiring high hardness, toughness, as well as abrasive/adhesive wear resistance and resistance to galling at low costs. The steel was tribologically tested in dry sliding conditions under abrasive and adhesive wear mode, facilitated by using alumina and bearing steel ball as a

The super-duplex stainless steel UNS S32750 consists of two main phases, austenite and ferrite, which differ not only by their morphology, physical, and mechanical properties, but also by their deformation behaviour. A heterogenous deformation can be obtained during thermomechanical processing, generating internal stresses and sometimes fissures or cracks on sample lateral surfaces, due to ferrite’s

In this study, the influence of internal pressure and axial compressive displacement on the formability of small-diameter ZM21 magnesium alloy tubes in warm tube hydroforming (THF) was examined experimentally and numerically. The deformation behavior of ZM21 tubes, with a 2.0 mm outer diameter and 0.2 mm wall thickness, was evaluated in taper-cavity and cylinder-cavity dies. The simulation code used

The current study focuses on the melting behavior of a scrap bar with low carbon content in hot metal which contains high carbon concentration by applying experiments and mathematical modelings. The experiments suggest that higher temperature is favorable for the melting of the bar and the melting rate of the bar is initially high while decreased to a relative stable level after 90 s in the current

Mg-Zn-Y alloys with long-period stacking ordered structures (LPSO) have attracted attention due to their excellent mechanical properties. In addition to the LPSO structure, Mg alloys can also be strengthened by oxide particles. In the present study, oxide dispersion strengthened Mg97Zn1Y2 (at%) alloys were prepared by equal channel angular pressing (ECAP) of mechanical alloyed (MA) powder under an

Currently, the available evaluation methods for determining the chip breakability in the industry are mainly based on subjective visual assessment of the chip formation by an operator during machining or on chips that were collected after the tests. However, in many cases, these methods cannot give us accurate quantitative differences for evaluation of the chip breakability of similar steel grades

The use of microwave heating in primary metallurgy is gaining an increasing interest due to the possibility to selectively process ores and to volumetrically heat large amounts of low-thermal conductivity minerals. In this paper the study, development and testing of a new applicator combining the use of microwave and induction heating for rapid reduction of metal containing oxides is described. Numerical

In order to improve the cold rolled steel strip flatness, the load distribution of the tandem cold rolling process is subject to investigation and optimization. The strip deformation resistance model is corrected by an artificial neural network that is trained with the actual measured data of 4500 strip coils. Based on the model, a flatness prediction model of strip steel is established in a five-stand

Since the current volumes of collected end-of-life lithium ion batteries (LIBs) are low, one option to increase the feasibility of their recycling is to feed them to existing metals production processes. This work presents a novel approach to integrate froth flotation as a mechanical treatment to optimize the recovery of valuable metals from LIB scrap and minimize their loss in the nickel slag cleaning

A TA1 (Ti alloy)/low alloy steel (LAS) composite plate was manufactured by explosive welding. The effects of the bonding interface microstructure on the mechanical properties and fracture behavior of the composite plate were investigated. The results show that the interface has a wavy structure with intermetallic compounds (IMCs) enclosed by a steel matrix. The metallurgical bonding interface was achieved

Cleanliness control is an eternal theme to improve the properties of steel products. With the increasing recycling rates of scrap steel, the removal and stabilization of residual elements have become a vital issue for improving the performance of steel products. Thermodynamic and mismatch calculations plus laboratory experiments were carried out to study the heterogeneous nucleation phenomena of inclusions

Wire and arc additive manufacturing of stiffened ribs for fabricating large integral panel components holds promise for lightweight construction, but stress and warpage remain intractable problems. This work take stress in central lines as a research focus, theoretically analyzes stress evolution along central lines without a stress distribution hypothesis, then further develops prediction models of

The characteristics of weld bead formation and droplet transfer in pulsed gas metal arc weld (GMAW) with different arc lengths were studied by changing the base current time in this work. The results showed that it was easier to cause short circuits and spatters with a short arc. However, the deviation between the deepest point of penetration and the center of bead will be aggravated with the increase