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MicroRNA Sensors Based on CRISPR/Cas12a Technologies: Evolution From Indirect to Direct Detection Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-03-15 Songcheng Yu, Xueying Lei, Chenling Qu
MicroRNA (miRNA) has emerged as a promising biomarker for disease diagnosis and a potential therapeutic targets for drug development. The detection of miRNA can serve as a noninvasive tool in disea...
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The Role of Catecholamines in the Pathogenesis of Diseases and the Modified Electrodes for Electrochemical Detection of Catecholamines: A Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-03-10 Meng Zhang, Yimeng Wang, Jie Jiang, Yanxiao Jiang, Daqian Song
Catecholamines (CAs), which include adrenaline, noradrenaline, and dopamine, are neurotransmitters and hormones that critically regulate the cardiovascular system, metabolism, and stress response i...
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Advances and Challenges in the Analysis of Boswellic Acids by Separation Methods Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-03-10 Dmytro Kosolapov, Pavel Jáč, Petra Riasová, Jitka Poušková, Miroslav Polášek, Lucie Nováková
Boswellia resin is an exudate from the cut bark of Boswellia trees. The main constituents of pharmacological interest are boswellic acids (pentacyclic triterpenoids), namely α-boswellic acid, β-bos...
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Mechanistic Insight Into the Reactivity of Frustrated Lewis Pairs: Liquid-State NMR Studies Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-03-06 Xinhui Kou
Frustrated Lewis pairs (FLPs) have been widely investigated as promising catalysts due to their metal-free feature and ability to activate small molecules. Over the last few years, the structure, d...
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Chromatographic Methods for the Determination of Organic Pollution in Urban Water: A Current Mini Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-03-07 Paulina Gątarek, Angelina Rosiak, Joanna Kałużna-Czaplińska
The number of pollutants and chemicals with the potential to reach the environment is still largely unknown, which poses great challenges for researchers in various fields of science, environmental...
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Suitability and Applications of Total-Reflection X-Ray Fluorescence Spectrometry for Analytical Characterization of Nuclear Materials Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-02-26 Kaushik Sanyal, Sangita Dhara
The suitability and applications of Total reflection X-ray Fluorescence (TXRF) for characterization of nuclear materials are numerous. TXRF has been successfully applied for trace, minor and major ...
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Accurate Clinical Detection of Vitamin D by Mass Spectrometry: A Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-02-20 Zhilong Xu, Kai Yu, Meng Zhang, Yun Ju, Jing He, Yanxiao Jiang, Yunuo Li, Jie Jiang
Vitamin D deficiency is thought to be associated with a wide range of diseases, including diabetes, cancer, depression, neurodegenerative diseases, and cardiovascular and cerebrovascular diseases. ...
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Advances in Electrochemical Biosensors for the Detection of Common Oral Diseases Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-02-16 Chaoran Liu, Changjun Guan, Yanan Li, Ze Li, Yanchun Wang, Guanghong Han
Limiting and preventing oral diseases remains a major challenge to the health of populations around the world, so finding ways to detect early-stage diseases (e.g., caries, periodontal disease, and...
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Technological Advancement and Trend in Selective Bioanalytical Sample Extraction through State of the Art 3-D Printing Techniques Aiming ‘Sorbent Customization as per need’ Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-02-06 Nasir Khan, Pinaki Sengupta
The inherent complexity of biological matrices and presence of several interfering substances in biological samples make them unsuitable for direct analysis. An effective sample preparation techniq...
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Analytical Strategies to Investigate Molecular Signaling, Proteomics, Extraction and Quantification of Withanolides – A Comprehensive Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-02-01 Sinchana B Gopalaiah, Kavitha Jayaseelan
Withanolides are the class of steroidal molecules getting greater emphasis in recent years. Quality control throughout the manufacturing and storage period is often one of the key problems that hav...
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Quality Consistency Evaluation of Traditional Chinese Medicines: Current Status and Future Perspectives Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-22 Chun-Lu Liu, Yan Jiang, Hui-Jun Li
Quality consistency evaluation of traditional Chinese medicines (TCMs) is a crucial factor that determines the safe and effective application in clinical settings. However, TCMs exhibit diverse, he...
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The Effect of Polymerization Techniques on the Creation of Molecularly Imprinted Polymer Sensors and Their Application on Pharmaceutical Compounds Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-22 Abdullah Al Faysal, S. Irem Kaya, Ahmet Cetinkaya, Sibel A Ozkan, Ayşegül Gölcü
Molecularly imprinted polymers (MIPs) have become more prevalent in fabricating sensor applications, particularly in medicine, pharmaceuticals, food quality monitoring, and the environment. The eas...
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A Recent Advancement in Food Quality Assessment: Using MOF-Based Sensors: Challenges and Future Aspects Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-22 Muhammad Saqaf Jagirani, Weiqiang Zhou, Ahsan Nazir, Muhammad Yasir Akram, Pengwei Huo, Yongsheng Yan
Monitoring food safety is crucial and significantly impacts the ecosystem and human health. To adequately address food safety problems, a collaborative effort needed from government, industry, and ...
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Assessing the Greenness and Environmental Friendliness of Analytical Methods: Modern Approaches and Recent Computational Programs Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-19 Farah Abdulraouf Semysim, Barakat Kareem Hussain, Maha Abbas Hussien, Ebaa Adnan Azooz, Denys Snigur
Environmental measures have drawn more attention recently as a means of identifying cost-effective, safe, and green approaches in analytical methods. As a result, white and green analytical chemist...
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Review of Gas-Chromatographic Measurement Methodologies for Atmospheric Halogenated Greenhouse Gases Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-19 Noh Soo Han, Jeong Sik Lim
Gas chromatography (GC) is crucial for measuring atmospheric halogenated greenhouse gases (hGHGs), usually coupled with electron capture detector (ECD, with higher sensitivity) or mass spectrometry...
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Nanomaterials for Fluorescent Detection of Hemoglobin Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-16 Yongming Guo, Yiting Tang, Yu Tan, Yijin Li, Yubin Xiang
Hemoglobin plays a vital role in a series of biological activities. Abnormal levels of hemoglobin in blood are associated with many clinical diseases. Therefore, development of simple and accurate ...
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The Latest Sensor Detection Methods for per- and Polyfluoroalkyl Substances Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-17 Mingyu Zhang, Yanan Zhao, Brian Bui, Liming Tang, Jiajia Xue, Mingli Chen, Wei Chen
Per- and polyfluoroalkyl substances (PFASs) have emerged as a prominent environmental pollutant in recent years, primarily due to their tendency to accumulate and magnify in both the environment an...
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Nanomaterials Connected to Bioreceptors to Introduce Efficient Biosensing Strategy for Diagnosis of the TORCH Infections: A Critical Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-09 Sofiene Mansouri, Yousef Alharbi, Abdulrahman Alqahtani
TORCH infection is a significant risk factor for severe fetal damage, especially congenital malformations. Screening pregnant women for TORCH pathogens could reduce the incidence of adverse pregnan...
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High-Performance Liquid Chromatography Methods for Determining the Purity of Drugs with Weak UV Chromophores – A Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-05 Elżbieta Sobolewska, Magdalena Biesaga
High-performance liquid chromatography (HPLC) is one of the most useful techniques for the separation and determination of new drugs with a complex nature. The selection of an HPLC detector depends...
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Aptamer-Magnetic Nanoparticle Complexes for Powerful Biosensing: A Comprehensive Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-02 Farag M. A. Altalbawy, Eyhab Ali, Mohammed N. Fenjan, Yasser Fakri Mustafa, Sofiene Mansouri, Bokov D.O., Sharipova Gulnikhol Idiyevna, Neeti Misra, Ahmed Hussien Alawadi, Ali Alsalamy
The selective and sensitive diagnosis of diseases is a significant matter in the early stages of the cure of illnesses. To elaborate, although several types of probes have been broadly applied in c...
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Recent Advances in Dispersive Liquid-Liquid Microextraction for Pharmaceutical Analysis Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2024-01-02 Karen Sze Jie Tay, Hong Heng See
Sample clean-up and pre-concentration are critical components of pharmaceutical analysis. The dispersive liquid-liquid microextraction (DLLME) technique is widely recognized as the most effective a...
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Molecularly Imprinted Polymer-Based Sensors Integrated with Transition Metal Dichalcogenides (TMDs) and MXenes: A Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-12-28 Vandana Thotathil, Naheed Sidiq, Jawaher S. Al Marri, Shabi Abbas Zaidi
Molecularly imprinted polymer (MIP)-based electrochemical sensors have been extensively researched due to their higher sensitivity, quick response, and operational ease. To develop more advanced se...
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Malondialdehyde Analysis in Biological Samples by Capillary Electrophoresis: The State of Art Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-12-26 Maria Patrícia do Nascimento, Bruna Marchiori Berlande, Marina Guedes Fraga Lopes, Mário Flávio Cardoso de Lima, Claudio Teodoro de Souza, Marcone Augusto Leal de Oliveira
Lipid peroxidation occurs when substances, such as reactive oxygen species, attack lipids. Polyunsaturated fatty acids are the main targets. Several products are formed, including primary products ...
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A Comprehensive Review on Shilajit: What We Know about Its Chemical Composition Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-12-22 Elham Kamgar, Massoud Kaykhaii, Joanna Zembrzuska
Shilajit, a natural material known for thousands of years, is primarily famous because it was the main constituent used for the mummification of bodies by dynastic Egyptians. However, for millennia...
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Mycotoxins in Vegetable Oils: A Review of Recent Developments, Current Challenges and Future Perspectives in Sample Preparation, Chromatographic Determination, and Analysis of Real Samples Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-12-22 Basil K. Munjanja, Philiswa N. Nomngongo, Nomvano Mketo
Mycotoxins are toxic compounds that are formed as secondary metabolites by some fungal species that contaminate crops during pre- and postharvest stages. Exposure to mycotoxins can lead to adverse ...
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Hair and Nail-On-Chip for Bioinspired Microfluidic Device Fabrication and Biomarker Detection Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-12-22 Rohitraj Ray, Amith Rakesh, Sheetal Singh, Harishkumar Madhyastha, Naresh Kumar Mani
The advent of biosensors has tremendously increased our potential of identifying and solving important problems in various domains, ranging from food safety and environmental analysis, to healthcar...
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Spectrum-Effect Relationship in Chinese Herbal Medicine: Current Status and Future Perspectives Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-12-21 Si Li, Xi Huang, Yuan Li, Rong Ding, Xuemei Wu, Ling Li, Canlin Li, Rui Gu
The quality of Chinese herbal medicine (CHM) directly impacts clinical efficacy and safety. Fingerprint technology is an internationally recognized method for evaluating the quality of CHM. However...
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Nanoparticles Based Sensors for Cyanide Ion Sensing, Basic Principle, Mechanism and Applications Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-12-20 Zarif Gul, Aqsa Iqbal, Javeria Shoukat, Anila Anila, Rafia Rahman, Shaheed Ullah, Muhammad Zeeshan, Muhammad Saleem Ashiq, Ataf Ali Altaf
Rapidly detecting potentially toxic ions such as cyanide is paramount to maintaining a sustainable and environmentally friendly ecosystem for living organisms. In recent years, molecular sensors ha...
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Headspace Microextraction. A Comprehensive Review on Method Application to the Analysis of Real Samples (from 2018 till Present) Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-12-11 Arina Skok, Yaroslav Bazel
This work describes current trends in the development of headspace microextraction methods. The main trends in the selection of detection techniques used in combination with microextraction and pre...
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Saliva Analysis Based on Microfluidics: Focusing the Wide Spectrum of Target Analyte Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-12-01 Xin Liu, Xinyue Zhou, Xiaojia Li, Yixuan Wei, Tianlin Wang, Shuo Liu, Huazhe Yang, Xiaoting Sun
Saliva is one of the most critical human body fluids that can reflect the state of the human body. The detection of saliva is of great significance for disease diagnosis and health monitoring. Micr...
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Resolving D-Amino Acid Containing Peptides Using Ion Mobility-Mass Spectrometry: Challenges and Recent Developments Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-11-17 Mohamed Abdulbagi, Bin Di, Bo Li
Peptides and proteins having D-amino acids in their sequences are now believed to be widespread among different living organisms. Their significance is attributed to the diverse functions of these ...
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Analytical Tools and Methods for Explosive Analysis in Forensics: A Critical Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-11-07 Bhumika Sharma, Ranu Gadi
This review summarizes (i) compositions and types of improvised explosive devices; (ii) the process of collection, extraction and analysis of explosive evidence encountered in explosive and related...
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Recent Trends of Vibrational Spectroscopy in Examination of Sequence of Strokes: Application in Forensic Documents Examination Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-11-07 Arya Suresh Babu, Anjali Tomar, Shweta Sharma
Chronological sequencing of ink strokes has been a challenge for the Forensic Document Examiners (FDE). Document forgery is a common practice and the ability to determine the order in which the pri...
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Mass Spectrometry Analysis for Clinical Applications: A Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-11-01 Hong Zhang, Yali Yang, Yanxiao Jiang, Meng Zhang, Zhilong Xu, Xiaofei Wang, Jie Jiang
Mass spectrometry (MS) has become an attractive analytical method in clinical analysis due to its comprehensive advantages of high sensitivity, high specificity and high throughput. Separation tech...
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Fluorescence Resonance Energy Transfer (FRET)-Based Sensor for Detection of Foodborne Pathogenic Bacteria: A Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-11-02 Priyadharshini Bhupathi, Thoraya Mohamed Elhassan A-Elgadir, Riyadh Hasan Mohammed Ali, Hijran Sanaan Jabbar, Djakhangirova Gulnoza, S. K. Joshi, Mohammed Kadhem Abid, Esraa Ahmed Said, Ahmed Alawadi, Ali Alsaalamy
Sensitive and rapid determination of foodborne pathogenic bacteria is of practical importance for the control and prevention of foodborne illnesses. Nowadays, with the prosperous development of flu...
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Green Assessment of Analytical Procedures for the Determination of Pharmaceuticals in Sewage Sludge and Soil Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-11-03 Carmen Mejías, Marina Arenas, Julia Martín, Juan Luis Santos, Irene Aparicio, Esteban Alonso
The main difficulties when analyzing pharmaceutically active compounds (PhACs) in solid environmental samples is the complexity of the samples and the low concentration levels of such pollutants. M...
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Analytical Methods for the Determination of Quercetin and Quercetin Glycosides in Pharmaceuticals and Biological Samples Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-10-29 Fotouh R. Mansour, Inas A. Abdallah, Alaa Bedair, Mahmoud Hamed
Flavonoids are plant-derived compounds that have several health benefits, including antioxidative, anti-inflammatory, anti-mutagenic, and anti-carcinogenic effects. Quercetin is a flavonoid that is...
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A Review of Electrochemical Techniques for Corrosion Monitoring – Fundamentals and Research Updates Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-10-25 Sheetal, Sheetal Kundu, Sanjeeve Thakur, Ashish Kumar Singh, Manjeet Singh, Balaram Pani, Viswanathan S. Saji
Interculturally, corrosion has been counted as one of the most expensive factors toward the retrogression of concrete and metallic structures resulting in huge monetary losses and unanticipated los...
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Factors Affecting the Extraction of (Poly)Phenols from Natural Resources Using Deep Eutectic Solvents Combined with Ultrasound-Assisted Extraction Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-10-18 Shahida Anusha Siddiqui, Ali Ali Redha, Molla Salauddin, Iskandar Azmy Harahap, H. P. Vasantha Rupasinghe
Replacing conventional solvents with deep eutectic solvents (DES) has shown promising effects on the extraction yield of (poly)phenols. DES can be combined with ultrasound-assisted extraction (UAE)...
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Unlocking the Hidden Depths: Multi-Modal Integration of Imaging Mass Spectrometry-Based and Molecular Imaging Techniques Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-10-17 Behnaz Akbari, Bertrand Russell Huber, Janet Hope Sherman
Multimodal imaging (MMI) has emerged as a powerful tool in clinical research, combining different imaging modes to acquire comprehensive information and enabling scientists and surgeons to study ti...
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Advances in Optical Probes for the Detection of Hydrazine in Environmental and Biological Systems Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-10-10 Lun Zhang, Lijuan Cheng
Hydrazine, as a crucial raw material in the fine chemical industry, plays an indispensable role in fuel, catalyst, pesticide and drug synthesis. Due to its good water solubility and high toxicity, ...
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Recent Approaches for Analytical Characterization of Phospholipids in Food Matrices. Is the Phospholipid Fraction Exploited in the Authentication of Food Lipids? Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-10-08 Rosalía López-Ruiz, Ana M Jimenez-Carvelo, Luis Cuadros-Rodríguez
Phospholipids (PhLs) are essential components of cell membranes, characterized by a hydrophobic tail and a hydrophilic headgroup. They play several roles in biological systems, including energy sto...
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Recent Advances in Organic Sensors for the Detection of Ag+ Ions: A Comprehensive Review (2019–2023) Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-10-04 Mubark Alshareef
Recently, organic sensors for the detection of Ag+ and other metal ions have experienced significant advancements. This is because there is a growing demand for reliable and sensitive tools to moni...
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Mass Spectrometry Based on Chemical Derivatization Has Brought Novel Discoveries to Lipidomics: A Comprehensive Review Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-10-02 Dan Wang, Huaming Xiao, Xin Lv, Hong Chen, Fang Wei
Lipids, as one of the most important organic compounds in organisms, are important components of cells and participate in energy storage and signal transduction of living organisms. As a rapidly ri...
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Recent Advances in Catecholamines Analytical Detection Methods and Their Pretreatment Technologies Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-09-21 Jie Jiang, Meng Zhang, Zhilong Xu, Yali Yang, Yimeng Wang, Hong Zhang, Kai Yu, Guangfeng Kan, Yanxiao Jiang
Catecholamines (CAs), including adrenaline, noradrenaline, and dopamine, are neurotransmitters and hormones that play a critical role in regulating the cardiovascular system, metabolism, and stress...
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Emerging Insights into the Use of Advanced Nanomaterials for the Electrochemiluminescence Biosensor of Pesticide Residues in Plant-Derived Foodstuff Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-09-20 Sulieman Ibraheem Shelash Al-Hawary, Jitendra Malviya, Raed H. Althomali, Sami G. Almalki, Kibum Kim, Rosario Mireya Romero-Parra, Ahmad Fahad Ahmad, Hijran Sanaan Jabbar, Shaik Vaseem Akram, Ahmed Hussien Radie
Pesticides have an important role in rising the overall productivity and yield of agricultural foods by eliminating and controlling insects, pests, fungi, and various plant-related illnesses. Howev...
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Recent Advances in Aptasensors for Rapid Pesticide Residues Detection Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-09-14 Na Qin, Jinfeng Liu, Fengyun Li, Jingbo Liu
Abstract Pesticides are applied widely to increase agricultural output and quality, however, this practice results in residual issues that not only harm the environment but also put people and animals’ lives and health at risk. As a result, it is critical to find pesticide residues in a variety of sources, including crops, water supplies, and soil. Aptamers are more flexible in their synthesis and
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Research Progress of SERS Sensors Based on Hydrogen Peroxide and Related Substances Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-09-11 Shuyan Ruan, Wenting Liu, Wenxi Wang, Yudong Lu
Abstract Hydrogen peroxide (H2O2) has an important role in living organisms, and its detection is of great importance in medical, chemical, and food safety applications. This review provides a comparison of different types of Surface-enhanced Raman scattering (SERS) sensors for H2O2 and related substances with respect to their detection limits, which are of interest due to high sensitivity compared
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Advances in AI-Driven Retention Prediction for Different Chromatographic Techniques: Unraveling the Complexity Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-09-06 Yash Raj Singh, Darshil B. Shah, Dilip G. Maheshwari, Jignesh S. Shah, Shreeraj Shah
Abstract Retention prediction through Artificial intelligence (AI)-based techniques has gained exponential growth due to their abilities to process complex sets of data and ease the crucial task of identification and separation of compounds in most employed chromatographic techniques. Numerous approaches were reported for retention prediction in different chromatographic techniques, and consistent
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A Critical Review of Soil Sampling and Data Analysis Strategies for Source Tracing of Soil in Forensic Investigations Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-09-06 Nur Ain Najihah Binti Mohd Rosdi, Nadirah Abd Hamid, Saiful Fazamil Mohd Ali, Hukil Sino, Loong Chuen Lee
Abstract Soil is one type of Earth material demonstrating a wide range of physical, chemical, and biological properties. As the compositional profile of soil is a product of interaction between numerous abiotic and biotic components, it tends to be unique by its geographic origin. Hence, soil is paramount for predicting source or origin in forensic provenance and intelligence, food provenance, biosecurity
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Drilling into “Quality by Design” Approach for Analytical Methods Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-09-04 Lucas Chiarentin, Carla Gonçalves, Cátia Augusto, Margarida Miranda, Catarina Cardoso, Carla Vitorino
Abstract The need for consistency in analytical method development reinforces the dependence of pharmaceutical product development and manufacturing on robust analytical data. The Analytical Quality by Design (AQbD), akin to the product Quality by Design (QbD) endows a high degree of confidence to the method quality developed. AQbD involves the definition of the analytical target profile as starting
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A Review of the Analysis of Phthalates by Gas Chromatography in Aqueous and Food Matrices Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-08-30 Shikha Bhogal, Aman Grover, Irshad Mohiuddin
Abstract As a commonly well-known industrial chemical, phthalates are produced in high volumes to be used in various consumer products (e.g., plasticizers, medical devices, construction materials, and toys) to enhance softness, durability, transparency, and flexibility. Phthalates are generally not chemically bonded to the polymer chain of the plastic in which they are mixed. Thus, they may leach,
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A Review on Pretreatment and Analysis Methods of Polyether Antibiotics in Complex Samples Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-08-30 Xin-Wei Wei, Yuan Zhang, Yu Zhou, Ming Li, Zhi-Fei Liu, Xue-Song Feng, Yue Tan
Abstract Polyether antibiotics (PAs) are the anti-coccidiosis drugs used for treating and preventing coccidiosis. Studies show the residues of these antibiotics in food cause adversities and threaten human health. PAs thus need robust, rugged, and accurate methods for their analysis. This review encompasses pretreatment and detection methods of PAs in diverse matrices since 2010. Both conventional
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Comprehensive Two-Dimensional Gas Chromatography in Petroleum Derived Samples: A Review on Advances in Source and Weathering Studies of Spilled Oil Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-08-26 Antônia M. Corrêa, Juliana M. Sousa, Kátia Z. Leal, Marcelo C. Bernardes
Abstract Since its introduction comprehensive two-dimensional gas chromatography (GC × GC) has been widely applied to analyze complex samples due to its enhanced peak capacity and selectivity, thereby increasing the number of identifiable peaks and improving coelution issues. Even though it is still undergoing development, GC × GC provides many advantages in the analysis of petroleum-derived samples
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Determination of Total Sulfur Content in Fuels: A Comprehensive and Metrological Review Focusing on Compliance Assessment Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-08-23 Khrissy Aracélly Reis Medeiros, Livio Garcia da Costa, Gabriela Knippelberg Bifano Manea, Roberta de Moraes Maciel, Ednéia Caliman, Mônica Teixeira da Silva, Rodrigo Caciano de Sena, Elcio Cruz de Oliveira
Abstract Sulfur-containing compounds are naturally found in crude oil, and they can be partially removed during the refining process. The wide use of fossil fuels has a significant contribution to sulfur emissions into the atmosphere, and Governments are striving to reduce the amount of the fuels by environmental regulations. The reduction of sulfur levels in diesel and other transportation fuels is
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Volatile Methylsiloxanes in Complex Samples: Recent Updates on Pretreatment and Analysis Methods Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-08-21 Wei-lai Wang, Yuan Zhang, De-mei Sun, Zu-yi Chen, Min Qian, Yu Zhou, Xue-song Feng, Xin-yuan Zhang
Abstract Volatile methylsiloxanes (VMSs) are massively produced chemicals having applications in industry and home because of their physical and chemical characteristics. They are used in personal care products such as cosmetics, household coatings, cleaners, skin care products, and others. Resultantly, large number of VMSs are discharged into air where they can be subjected to atmospheric migrations
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Insights into Genus Codonopsis: From past Achievements to Future Perspectives Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-08-16 Jiaqi Yue, Ying Xiao, Wansheng Chen
Abstract Codonopsis plants, as a kind of medicinal and edible herb, have a long history of application and have been widely concerned by pharmacists and biologists. In this article, the species diversity, taxonomy and distribution, ethnic medicinal records, chemical composition, pharmacological activity, and quality evaluation methods of Codonopsis species were systematically reviewed. In addition
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Recent Development in Fluorescent Probes for the Detection of Hg2+ Ions Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-07-30 Ajay Kumar
Abstract Mercury, a highly toxic heavy metal, poses significant environmental and health risks, necessitating the development of effective and responsive techniques for its detection. Organic chromophores, particularly small molecules, have emerged as promising materials for sensing Hg2+ ions due to their high selectivity, sensitivity, and ease of synthesis. In this review article, we provide a systematic
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Recent Advances in Fluorescent Probes for Zinc Ions Based on Various Response Mechanisms Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-07-24 Jinrong Wen, Qianying Hua, Sha Ding, Aokui Sun, Yong Xia
Abstract Zinc is a vital metal element with extensive applications in various fields such as industry, metallurgy, agriculture, food, and healthcare. For living organisms, zinc ions are indispensable, and their deficiency can lead to physiological and metabolic abnormalities that cause multiple diseases. Hence, there is a significant need for selective recognition and effective detection of free zinc
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Multi-Attribute Method (MAM): An Emerging Analytical Workflow for Biopharmaceutical Characterization, Batch Release and cGMP Purity Testing at the Peptide and Intact Protein Level Crit. Rev. Anal. Chem. (IF 5.0) Pub Date : 2023-07-25 Silvia Millán-Martín, Craig Jakes, Sara Carillo, Lizzie Gallagher, Kai Scheffler, Kelly Broster, Jonathan Bones
Abstract The rapid growth of biotherapeutic industry, with more and more complex molecules entering the market, forces the need for advanced analytical platforms that can quickly and accurately identify and quantify product quality attributes. Mass spectrometry has the potential to provide more detailed information about the quality attributes of complex products, and MS methods are more sensitive