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Emerging Investigators in Flow Chemistry 2023 J. Flow Chem. (IF 2.7) Pub Date : 2024-03-18 Cecilia Bottecchia, Wu Jie, Luca Capaldo
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Determination of micromixing times in commercially available continuous-flow mixers: evaluation of the incorporation and interaction by exchange with the mean model J. Flow Chem. (IF 2.7) Pub Date : 2024-03-06 Jasper H. A. Schuurmans, Micha Peeters, Matthieu Dorbec, Koen P. L. Kuijpers
To understand and predict the effect of mixing in a mixer or reactor, characterization is essential. The Villermaux-Dushman system of competitive parallel reactions is one of the most frequently used methods to obtain details on the micromixing behavior in mixers and reactors. For quantitative information, a model can convert experimental data into a universal micromixing time, which can be used to
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Access semi-stabilized and unstabilized diazo compounds using iodosylbenzene J. Flow Chem. (IF 2.7) Pub Date : 2024-02-29 Laurent Vinet, Emmanuelle M. D. Allouche, Vanessa Kairouz, André B. Charette
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3D-printed open-source sensor flow cells for microfluidic temperature, electrical conductivity, and pH value determination J. Flow Chem. (IF 2.7) Pub Date : 2024-02-28 Robin Dinter, Lennart Helwes, Stijn de Vries, Kausik Jegatheeswaran, Henning Jibben, Norbert Kockmann
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Design and structural parameter optimization of Venturi-type microbubble reactor for wastewater treatment by CFD simulation J. Flow Chem. (IF 2.7) Pub Date : 2024-02-27 Hanfei Liu, Chao Li, Shuangfei Zhao, Hao Zhu, Yiping Huang, Wei He, Yue Zhao, Yuguang Li, Kai Guo
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Lab-scale flow chemistry? Just do it yourself! J. Flow Chem. (IF 2.7) Pub Date : 2024-02-23 Laura Y. Vázquez-Amaya, Guglielmo A. Coppola, Erik V. Van der Eycken, Upendra K. Sharma
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Practical synthesis of tetrahydrofolate by highly efficient catalytic hydrogenation in continuous flow J. Flow Chem. (IF 2.7) Pub Date : 2024-02-16 Heng Pang, Junrong Huang, Juntao Wang, Gang Wang, Ana Xu, Lei Luo, Qunhui Yuan, Hengzhi You, Fen-Er Chen
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A perspective on the past, the present, and the future of computational fluid dynamics (CFD) in flow chemistry J. Flow Chem. (IF 2.7) Pub Date : 2024-02-16 Natan Padoin, Tatiana Matiazzo, Humberto Gracher Riella, Cíntia Soares
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Advances in cofactor immobilization for enhanced continuous-flow biocatalysis J. Flow Chem. (IF 2.7) Pub Date : 2024-02-14 Bente Reus, Matteo Damian, Francesco G. Mutti
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Continuous and size-control synthesis of lipopolyplex nanoparticles enabled by controlled micromixing performance for mRNA delivery J. Flow Chem. (IF 2.7) Pub Date : 2024-02-12 Shirong Song, Zhikai Liu, Letao Guo, Wang Yao, Hongchen Liu, Mei Yang, Guangwen Chen
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Design and implementation of an automated DT-PhotoFluor radiosynthesis module for 18F-fluorination of aliphatic, branched chain amino acids J. Flow Chem. (IF 2.7) Pub Date : 2024-02-07 Gokce Engudar, Zheliang Yuan, Matthew B. Nodwell, Hua Yang, Chelsey Currie, Stuart McDiarmid, Robert Britton, Paul Schaffer
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A fully continuous-flow process for the synthesis of 4-nitropyrazole J. Flow Chem. (IF 2.7) Pub Date : 2024-01-31 Jiadi Zhou, Zhaoyang Mu, Lishan Geng, Xuyang Zhao, Chenwei Gao, Zhiqun Yu
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Investigation into a high-p,T,c continuous flow synthesis of myristyl-γ-picolinium chloride (MGPC) – a preservative in pharmaceutical formulations J. Flow Chem. (IF 2.7) Pub Date : 2024-01-26 Karuna Veeramani, Manish Shinde, Vishnuvardhana Vema Reddy Eda, Swamy Peraka, Saranya Mohan, Rakeshwar Bandichhor, Srinivas Oruganti
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The continuous flow synthesis of azos J. Flow Chem. (IF 2.7) Pub Date : 2024-01-26 Adam T. McCormack, John C. Stephens
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Continuous flow ozonolysis of cardanol for greener synthesis of bio-based monomers J. Flow Chem. (IF 2.7) Pub Date : 2024-01-18 Sphurti P. Kulkarni, Amol A. Kulkarni
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An affordable, programmable and interactive continuous flow Photoreactor setup for undergraduate organic synthetic teaching labs J. Flow Chem. (IF 2.7) Pub Date : 2024-01-18 Michał Domański, Gilles Marcou, Joshua P. Barham
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Continuous flow synthesis of meso-substituted porphyrins with inline UV–Vis analysis J. Flow Chem. (IF 2.7) Pub Date : 2024-01-15 Firdaus Parveen, Henry J. Morris, Harvey West, Anna G. Slater
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Solid dosing in High-Throughput Experimentation: generalization of mass enhancer technologies for submilligram scale J. Flow Chem. (IF 2.7) Pub Date : 2024-01-09
Abstract The emergence of High-Throughput Experimentation (HTE) as a powerful tool for reaction discovery and optimization is changing the way organic chemists are designing their experiments. It is a fantastic way to largely investigate a reaction, in a minimum of time and reagent consumption. However, HTE needs to be accessible to a wide audience for a full implementation in academic and industrial
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Application of stop-flow micro-tubing reactor system in organic reaction development J. Flow Chem. (IF 2.7) Pub Date : 2023-12-28 Qian Wang, Ruize Yin, Zihan Wang, Yanbin Zhang, Jie Wu
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Flow chemical laboratory practice for undergraduate students: synthesis of paracetamol J. Flow Chem. (IF 2.7) Pub Date : 2023-12-27 Bettina Rávai, Máté János Orosz, Orsolya Péterfi, Dorián László Galata, Erika Bálint
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Continuous synthesis of ε-caprolactone in a microreactor and kinetics insights into its side reactions J. Flow Chem. (IF 2.7) Pub Date : 2023-12-27 Bin Wu, Xindi Feng, Wei Du, Zhixiang Li, Gang Qian, Xuezhi Duan, Xinggui Zhou, Zhen Liu, Jing Zhang
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Continuous synthesis of boron-doped carbon nitride supported silver nanoparticles in an ultrasound-assisted coiled flow inverter microreactor J. Flow Chem. (IF 2.7) Pub Date : 2023-12-22 Yu-tian Tao, Ke-Jun Wu, Chao-Hong He
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Continuous-flow Synthesis of Anisotropic Plasmonic Nanostructures J. Flow Chem. (IF 2.7) Pub Date : 2023-12-18 Vini Singh, Perali Ramu Sridhar, R. Singh
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Two photons are better than one: continuous flow synthesis of ꞵ-lactones through a doubly photochemically-activated Paternò-Büchi reaction J. Flow Chem. (IF 2.7) Pub Date : 2023-12-15 Federica Minuto, Emanuele Farinini, Serena De Negri, Riccardo Leardi, Davide Ravelli, Pavlo Solokha, Andrea Basso
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Continuous Flow Generation of Highly Reactive Organometallic Intermediates: A Recent Update J. Flow Chem. (IF 2.7) Pub Date : 2023-11-28 Mauro Spennacchio, Philipp Natho, Michael Andresini, Marco Colella
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Investigations on the continuous flow generation of 2,6-dichloro-N-fluoropyridinium tetrafluoroborate using F2 gas J. Flow Chem. (IF 2.7) Pub Date : 2023-11-28 Kevin Simon, Desiree Znidar, Gabriel Glotz, Doris Dallinger, C. Oliver Kappe
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Methyl acetate production by reactive distillation using a vertical plate microdistillator J. Flow Chem. (IF 2.7) Pub Date : 2023-12-01 Yosuke Muranaka, Taisuke Maki, Soma Matsumoto, Kazuhiro Mae
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Telescoped synthesis of vicinal diamines via ring-opening of electrochemically generated aziridines in flow J. Flow Chem. (IF 2.7) Pub Date : 2023-11-29 Marharyta Laktsevich-Iskryk, Anastasiya Krech, Mihhail Fokin, Mariliis Kimm, Tatsiana Jarg, Timothy Noël, Maksim Ošeka
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Enhancing N-arylation productivity: the amplified potential of electrophotocatalysis in flow J. Flow Chem. (IF 2.7) Pub Date : 2023-11-28 Jolien De Ketelaere, Thomas S. A. Heugebaert
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Impact of gas-solid direct contact on gas-liquid-solid reaction performance in a flow reactor J. Flow Chem. (IF 2.7) Pub Date : 2023-11-28 Shusaku Asano, Hiroyuki Miyamura, Mizuki Matsushita, Shinji Kudo, Shū Kobayashi, Jun-ichiro Hayashi
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Nitration process of 2-(2,4-dichlorophenyl)-4-(difluoromethyl)-5-methyl-1,2,4-triazol-3-one in a microreactor J. Flow Chem. (IF 2.7) Pub Date : 2023-11-09 Jian-yang Cao, Jing Hou, Le-wu Zhan, Bin-dong Li
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Leveraging flow chemistry for the synthesis of trisubstituted isoxazoles J. Flow Chem. (IF 2.7) Pub Date : 2023-11-08 Michael Prieschl, Niklas Sulzer, Joerg Sedelmeier, Dainis Kaldre, René Lebl, Kurt Püntener, Stefan Hildbrand, Jason D. Williams, C. Oliver Kappe
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The joint effort of enzyme technology and flow chemistry to bring biocatalytic processes to the next level of sustainability, efficiency and productivity J. Flow Chem. (IF 2.7) Pub Date : 2023-11-07 Silvia Donzella, Martina Letizia Contente
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Recent developments of automated flow chemistry in pharmaceutical compounds synthesis J. Flow Chem. (IF 2.7) Pub Date : 2023-11-06 Jiashu Wu, Xingxing Yang, Yourong Pan, Tao Zuo, Zuozhou Ning, Chengxi Li, Zhiguo Zhang
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Investigating the photochemical reaction of an oxazolone derivative under continuous-flow conditions: from analytical monitoring to implementation in an advanced UVC-LED-driven microreactor J. Flow Chem. (IF 2.7) Pub Date : 2023-11-07 Gaëlle Lebrun, Marie Schmitt, Michael Oelgemöller, Marc Vedrenne, Jean-François Blanco, Karine Loubière
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Synthesis of BuNENA in a continuous flow microreactor J. Flow Chem. (IF 2.7) Pub Date : 2023-11-07 Zhi-Yuan Jiang, Jing Hou, Le-Wu Zhan, Bin-Dong Li
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Perspectives on flow biocatalysis: the engine propelling enzymatic reactions J. Flow Chem. (IF 2.7) Pub Date : 2023-10-23 Ana I. Benítez-Mateos, Francesca Paradisi
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Development of an automated flow chemistry affinity-based purification process for DNA-encoded chemistry J. Flow Chem. (IF 2.7) Pub Date : 2023-09-26 Robin Dinter, Katharina Götte, Franziska Gronke, Leon Justen, Andreas Brunschweiger, Norbert Kockmann
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Droplet generation at T-junctions in parallelized microchannels J. Flow Chem. (IF 2.7) Pub Date : 2023-08-16 Zhongdong Wang, Xingyu Xiang, Sajawal Raza, Asad Ullah, Chunying Zhu, Tianyang Feng, Youguang Ma, Taotao Fu
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Continuous-flow synthesis of 7-methoxy-1-tetralone: an important intermediate of (-)-Dezocine J. Flow Chem. (IF 2.7) Pub Date : 2023-07-27 Liangchuan Lai, Liang Gao, Minjie Liu, Yongxing Guo, Dang Cheng, Meifen Jiang, Fener Chen
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Safe and on-demand protocol for the continuous generation of SO2 and Cl2 for subsequent utilization in organic synthesis J. Flow Chem. (IF 2.7) Pub Date : 2023-07-24 Gulice Yiu Chung Leung, Shannon Thoi Rui Ying, Edwin Chia, Anqi Chen, Gabriel Loh, Balamurugan Ramalingam
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Enantioselective catalytic Strecker reaction on cyclic (Z)-aldimines in flow: reaction optimization and sustainability aspects J. Flow Chem. (IF 2.7) Pub Date : 2023-07-19 Antonella Ilenia Alfano, Andrea Sorato, Alessia Ciogli, Heiko Lange, Margherita Brindisi
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Continuous flow process development for the synthesis of an industrial raw material via solvent-free aromatic Claisen rearrangement J. Flow Chem. (IF 2.7) Pub Date : 2023-07-14 Nikola Petrovic, Sándor B. Ötvös, C. Oliver Kappe
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3D printed reactors and Kessil lamp holders for flow photochemistry: design and system standardization J. Flow Chem. (IF 2.7) Pub Date : 2023-07-05 Matthew R. Penny, Stephen T. Hilton
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Continuous morphology-controllable precipitation strategy for europium oxalate hydrates via microchannel reactor J. Flow Chem. (IF 2.7) Pub Date : 2023-06-30 Keyu Tao, Hao Li, Junjie Cheng, Zhi Cao, Yefan Li
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Continuous heterogeneous synthesis of hexafluoroacetone and its machine learning-assisted optimization J. Flow Chem. (IF 2.7) Pub Date : 2023-06-13 Tingting Qi, Guihua Luo, Haotian Xue, Feng Su, Jianli Chen, Weike Su, Ke-Jun Wu, An Su
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Continuous catalytic aerobic oxidation of o‑chlorotoluene to o-chlorobenzoic acid under slug flow conditions J. Flow Chem. (IF 2.7) Pub Date : 2023-06-09 Jiming Liu, Linchang Liu, Wei Zhang, Peng Li, Xin Li, Zhiqun Yu, Weike Su
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Accurate determination of the kinetics of toluene nitration in a liquid–liquid microflow system J. Flow Chem. (IF 2.7) Pub Date : 2023-05-22 Jing Song, Yongjin Cui, Yujun Wang, Kai Wang, Jian Deng, Guangsheng Luo
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Continuous flow Friedel–Crafts acetylation of phenols and electron-rich arenes and heteroarenes J. Flow Chem. (IF 2.7) Pub Date : 2023-05-09 Kévin Saint-Jacques, André B. Charette
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Micro-Batch flow reactor for the photoproduction of H2O2 from water/real seawater J. Flow Chem. (IF 2.7) Pub Date : 2023-04-19 Aswin Gopakumar, Tong Zhang, Shoubhik Das
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Advances in continuous polymer analysis in flow with application towards biopolymers J. Flow Chem. (IF 2.7) Pub Date : 2023-03-30 Samuel B. H. Patterson, Raymond Wong, Graeme Barker, Filipe Vilela
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FOMSy: 3D-printed flexible open-source microfluidic system and flow synthesis of PET-tracer J. Flow Chem. (IF 2.7) Pub Date : 2023-03-22 Florian Menzel, Jonathan Cotton, Thomas Klein, Andreas Maurer, Thomas Ziegler, Jochen M. Neumaier
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Leveraging first-principles and empirical models for disturbance detection in continuous pharmaceutical syntheses J. Flow Chem. (IF 2.7) Pub Date : 2023-03-16 Cameron Armstrong, Yuma Miyai, Anna Formosa, Pratiik Kaushik, Luke Rogers, Thomas D. Roper
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Rapid plugged flow synthesis of nucleoside analogues via Suzuki-Miyaura coupling and heck Alkenylation of 5-Iodo-2’-deoxyuridine (or cytidine) J. Flow Chem. (IF 2.7) Pub Date : 2023-03-16 Sujeet Gaware, Santosh Kori, Jose Luis Serrano, Rambabu Dandela, Stephen Hilton, Yogesh S. Sanghvi, Anant R. Kapdi
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Aerobic oxidation of hydroxymethylfurfural using a homogeneous TEMPO/TBN catalytic system in 3D-printed milli-scale porous reactors J. Flow Chem. (IF 2.7) Pub Date : 2023-03-06 Dionysia Koufou, Jorid Smets, Rob Ameloot, Simon Kuhn
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An eco-friendly and very low catalyst loading continuous condensation of primary amines and 1,3 Di carbonyl compounds: Synthesis of enaminones and enaminoesters by microreactor technology J. Flow Chem. (IF 2.7) Pub Date : 2023-03-01 Zahra Goodarzi, M. Sadegh Ramezani
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Continuous one-pot synthesis of new spiro-fused indoles from biobased building blocks using carbamoylation and imidation reactions under ultrasonic irradiation J. Flow Chem. (IF 2.7) Pub Date : 2023-02-15 Milene M. Hornink, Beatriz G. Rodrigues, Caroline S. Santos, Leandro H. Andrade
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5-Hydroxymethylfurfural synthesis from fructose over deep eutectic solvents in batch reactors and continuous flow microreactors J. Flow Chem. (IF 2.7) Pub Date : 2023-02-15 Chencong Ruan, Hero Jan Heeres, Jun Yue
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Effects of two-phase periodic velocity on droplet coalescence inside microchannels J. Flow Chem. (IF 2.7) Pub Date : 2023-02-07 Wen-qing Li, Xiao-juan Li, An-qi Guan, Zhi-jiang Jin, Jin-yuan Qian
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Continuous dehydration of glycerol to Acrolein based on HPW/TS-COOH catalyzation J. Flow Chem. (IF 2.7) Pub Date : 2023-02-06 Chen-Xin Su, Jing-Jing Chen, Shao-Yun Wu, Shao-Heng Li, Shou-Quan Zhou, Hui-Dong Zheng, Fu-Weng Zhang