Abstract In present study, nanosized iron oxides particles are synthetised by easy one step precipitation from Mohric salt (NH4)2Fe(SO4)2·6H2O reacting with sodium hydroxide solution in temperature up to 60 °C. When changing the time of reaction, the iron oxide particles of different shape are prepared and when drying wet extracted particles at elevated temperature of 60 °C the change of 2D shaped

Chemical vapor deposition (CVD) is one of the most important methods for the preparation of graphene. Graphene is usually prepared using horizontal tube CVD (HT-CVD) method. However, the preparation of this method is too long, generally more than 2 h. In this article, a method called vertical cold-wall CVD (VCW-CVD) method was introduced for graphene preparation. Due to the vertical angle between direction

This paper investigates interaction processes of the Fe3+, Cu2+, Ni2+, and Co2+ cations with humic acids isolated from brown coals of Ekibastuz basin. It was demonstrated that the sorption of heavy metal ions by humic acids (HA) depends on the concentration and nature of cations and decreases in the order of Fe3+ > Cu2+ > Ni2+ > Co2+; while increase in the concentration of humic acids (HA) results

Abstract Zinc oxide (ZnO) nanoparticles, due to their well-defined physico-chemical and antimicrobial attributes have been presented lately as favourable theranostic nanoplatforms for drug delivery. We hypothesized that surface modification of ZnO nanoparticle with activated polyethylene glycol and folic acid might be of great importance in targeted drug delivery in nasopharyngeal carcinoma since carcinoma

Abstract The objective of this study is to systematically investigate the evolution of silver surface segregation of silver/titanium oxide nanocomposite coatings produced by reactive sputtering process. Different thickness barrier layers were deposited on the surface of Ag-TiOx two-dimensional (2D) and three-dimensional (3D) composite coatings at different deposition rates. In 2D mode, the SEM images

Abstract Nowadays, the expansion of nanoparticles as antimicrobial and anticancer agents is one of the most exciting methods for cancer therapy and microbial diseases that can vanquish the problems of drug resistance. In this research, the biosynthesis of silver nanoparticles (AgNPs) was stated using Summer Savory extract. Moreover, these AgNPs by UV-Vis spectroscopy, FTIR, XRD, FESEM, EDX, PSA, and

Abstract Titanium oxide (TiO2) is one of the most scrutinized material because of its in-built fundamental properties and has been developed as an outstanding photo-catalytic material intended for many different industrial applications. In order to further explore the properties of TiO2, we prepared Copper-loaded TiO2 (Cu-TiO2) nanoparticles (NPs) for inhibiting the growth of bacterial cells and also

Abstract Introduction Microbial resistance is increasing worldwide. Investigations are underway to use nanoparticles as antimicrobial agents to reduce microbial resistance. Materials and methods Seven human pathogenic bacteria were selected according to common hospital infection bacteria: both gram-positive and negative. In this study, imipenem and ciprofloxacin antibiotics were used separately and

Abstract In this work, nano-sized mixed oxides of Mn3O4 and CuO were successfully prepared by a simple hydrothermal method and used as an effective heterogeneous sono-Fenton catalyst for p-nitrophenol (PNP) degradation at the neutral condition. The prepared nanocomposite was characterised by X-ray diffraction (XRD), field-emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy

Abstract A fast and facile method was employed for the synthesis of magnetic graphene oxide (MGO). The synthesized MGO is characterized by different techniques and used as a solid-phase adsorbent for the extraction of β-sitosterol from rapeseed oil deodorizer distillates (RODD) followed by gas chromatography-mass spectrometry analysis. Several parameters affecting the extraction efficiency, including

Abstract Fibroin is a protein that has been extensively studied for biomedical application. In the present study, silk was dissolved in CaCl2-C2H5OH-H2O in order to obtain silk fibroin (SF) solution, and it was then lyophilized in freeze-dryer. The electrospinning of SF sponge was performed at different fibroin concentrations. SF nanofibers were modified by crosslinking PAMAM dendrimers to carboxylic-terminated

Abstract Lateral flow immunoassay (LFIA) is the most widely used platform of the point-of-care (POC) detection. Since the most important factor in deciding the results of this technique is the visual quality of the test, it should be at its optimum. To address this issue, the present study examines optimising critical parameters to improve the quality of LFIA performance. In this regard the penicillin-binding

Abstract Recently, scientists have used the metallic nanoparticles especially copper nanoparticles for formulating many new neuroprotective supplements in the field of neurology. Also, we know the role of Nigella sativa L. in increasing the physiological activities of the central nervous system in traditional medicine. In the present study, we decided to prepare and formulate a new neuroprotective

Abstract This study investigated the removal of phosphorus (PO4−3-P) from water samples by SnO2 and WO3 nanoparticles (NPs). The effects of adsorbent dosage, pH, contact time and temperature with an initial concentration of 50 mg L−1 of P were investigated. SEM-EDX, FTIR, XRD, and BET analyses were performed to characterize these nanoparticles. The results indicated that the maximum adsorption capacity

Abstract In this article, we report a simple, effective, sensitive, non-toxic and environmentally friendly method for the detection of dopamine (DA). This method utilises the property of the self-polymerization of dopamine under alkaline conditions, and gets the concentration of dopamine by measuring the fluorescence intensity of polydopamine (PDA) nanoparticles. And this method only uses NaHCO3 to

Abstract The objective of this work is to develop cost-effective, reliable, and large-scale production of metallic nanoparticles (NPs) by adopting green chemistry principles for industrial applications. In that view, we have studied the phytochemical reducibility of silver nitrate by making use of Calotropis Procera (Ait.) R. Br root extract, and based on its medicinal properties, an attempt was made

Abstract Polydiacetylene (PDA)-based liposome have been attractive as sensory platforms owing to their applicability in simultaneous detection of colorimetric and fluorogenic signals. As PDA show low quantum yield, gold nanoparticles (GNPs) were used to amplify the fluorescence of the PDA by localized surface plasmon resonance. In this study, positively and negatively surface charged GNPs at different

Abstract Herein, BNPs@Cur-Pd as a versatile and reusable nanocatalyst was successfully synthesized and used for C–C coupling reactions. The Suzuki, Heck and Stille coupling reactions with good to excellent yields were conducted with Pd. Also, the catalyst could be recycled and reused for several sequential runs without considerable Pd leaching or diminishing of reaction yields. This simple methodology

Abstract Every year, many people die due to cancer in all of the world. So, the preparation and formulation of new chemotherapeutic supplements and drugs with remarkable effects for the treatment of cancer are in the priority of both developing and developed countries. Recently, gold nanoparticles have been used as modern chemotherapeutic drugs for the treatment of several cancers such as leukemia

Abstract The present study deals with Plectranthus amboinicus (Lour.), multiple potential herbs perceived as a medicinal and culinary adjunct has been used to fabricate gold (Au) nanoparticles (NPs) in an eco-benign fashion. We have primly reported the antioxidant and anticarcinogenic effects of phytofabricated Au NPs towards lung adenocarcinoma (LAC) cells (A549 cell line) in vitro. The herbal concentrate

Abstract The design of highly active photocatalysts for degradation of phenol can be particularly challenging for solar energy utilisation. Herein, a series of mesoporousLaCo1−xCexO3catalysts have been synthesised and studied for degradation of phenol under UV irradiation. Compared with LaCoO3-SG catalyst which is formed through sol-gel method, optimised LaCo1−xCexO3-NC prepared by nanocasting method

Abstract In this article, the dynamic behaviour of a rectangular atomic force microscope immersed in different liquids has been investigated. To account the rotatory inertia and shear deformation effects, Timoshenko beam theory has been applied. Here carbon tetrachloride (CCl4), methanol, acetone, water and air have been considered as the environments. Euler–Bernoulli and Timoshenko beam theories has

Abstract Lung cancer is one of the most widely recognised types of cancer and the acquisition of resistance towards chemotherapeutic drugs worsens the situation. Therefore, a site-directed, multi-targeting drug delivery system that is compliant with patients is the need of the hour. 5-Fluorouracil (5-FU), an anti-cancer chemotherapy drug, was delivered to the lung cancer cells using papain-inspired

Abstract In this work, worm-like SnS2 nanoparticles were prepared by a hydrothermal process. And then their photocatalytic activity was explored for the restoration of effluent containing Cr (VI). The results indicate that the product obtained is hexagonal SnS2 nanoparticles and adopts a worm-like morphology with length of approximate 6 nm and diameter of 3 nm. Moreover, the as-prepared SnS2 nanoparticles

(2020). Statement of Retraction. Journal of Experimental Nanoscience: Vol. 15, No. 1, pp. 99-99.

(2020). Statement of Retraction. Journal of Experimental Nanoscience: Vol. 15, No. 1, pp. 98-98.

(2020). Statement of Retraction. Journal of Experimental Nanoscience: Vol. 15, No. 1, pp. 97-97.

Abstract In this work, by appealing to a heterometallic cluster approach, a new highly porous metal-organic framework (MOF) formulated as {(Me2NH2)[Ni3K2(TZIA)3(H2O)3]·(DMF)4}n (1) has been fabricated by a solvothermal reaction of a bifunctional organic ligand 5-(1 H-tetrazol-5-yl)isophthalic acid (H3TZIA) with the Ni(II) and K(I) salts in water and DMF mixed solvents. The resulting activated 1a has

Abstract Mitotic spindle orientation is postulated to be regulated by two mechanisms: (1) Hertwig’s rule in which cells divide perpendicular to their major axis and (2) cortical cues arising from the spatial distribution of extracellular matrix. It was shown that cortical cues override cell geometry in dictating mitotic spindle orientation for cells cultured on 2D surfaces. In this study, we seek to

Abstract Mesoporous titania–ceria mixed oxide (MTCMO) was synthesised in a sol–gel method using cerium chloride and titanium isopropoxide (TTIP) as CeO2 as well as TiO2 precursors and sodium dodecyl sulphate (SDS) as a structure-directing agent and its application was evaluated in the synthesis of aromatic β-phosphonomalonate derivatives via cascade Knoevenagel–phospha-Michael addition reaction. The

Abstract In this study, adsorption treatment of phenol pollutant using electrospun poly(3-hydroxybutyrate) [P(3HB)] and poly(3-hydroxybutyrate-co-3-hydroxyhexanoate) [P(3HB-co-3HHx)] is highlighted for the first time. Both P(3HB) and P(3HB-co-3HHx) were extracted from bacterial cells and nanofibres were fabricated through electrospinning technique for the adsorption of phenol. The electrospun nanofibres

Abstract A systematic read on evaluating the machining characteristics of wire cut electrical discharge machining (WEDM) using analysis of variance (ANOVA) and multilinear regression model based multi objective optimization is provided during this analysis article. The current work explores, the surface roughness of copper metal matrix composite (MMCs) is minimized by optimizing the process parameters

Abstract With the goal of developing a new type of boron neutron capture therapy (BNCT) agent, selective internalisation of submicrometer boron carbide spherical particles into cancer cells via surface transferrin conjugation is demonstrated and confirmed in vitro and in vivo. Herein, negatively charged, spherical, submicrometer boron carbide (B4C) particles were coated with positively charged poly-L-lysine

Microporous foamed polymers are widely used in numerous fields hence, research on these materials has great practical significance. In this work, the effects of nano-SiO2 on the micromorphology of polystyrene (PS) microporous foamed materials were systematically studied by varying nano-SiO2 content and foaming temperature. Relative to PS, the results show that addition of nano-SiO2 significantly affects

This study aimed to report a one-pot, eco-friendly and room temperature procedure to prepare highly stable (at least 15 months) silver nanoparticles (AgNPs) using the aqueous leaf extract of Cordia myxa. The effects of different parameters, such as applied pH in the reaction mixture, amount of the leaf extract, silver ion concentrations, time of reaction and synthesis temperature, on the formation

A new 2 D Cu(II)-based coordination polymer (CP) {[Cu5(Hcia)4(dpp)2(H2O)2(μ-OH)2]·2H2O}n (1) was designed and synthesized via using the mixed-ligand strategy, using 1,3-di(4-pyridyl)propane (dpp) colinker with a flexible spacer H3cia (H3cia: 5-(2-carboxybenzyloxy)isophthalic acid). Furthermore, we use the grinding method to downsize the complex 1 to nano-region (denoted as nano 1 hereafter). Furthermore

This study aimed to synthesise TiO2 nanoparticles (NPs) in pure rutile structure at moderate temperature without calcination and use them as the catalyst for alachlor removal under UV-C radiation. The crystal structure, composition, and particle size of the synthesised TiO2 NPs were analysed using an X-ray diffractometer (XRD) and a scanning electron microscope (SEM). The XRD spectra revealed the production

Azo dyes are not efficiently removed in water treatment. So the development of excellent absorbent is significant important for environmental protection. In this study, ceria is successfully immobilized on 40-60 mesh sand by using a simple method of sol–gel. And then research the effect of absorption on azo dyes in waster using immobilized CeO2 (ICe). The ICe absorbent displays high removal efficiency

Toxic effects of nanoparticles on human health are considerably increasing their worldwide recognition. Currently silver nanoparticles are being widely used in consumer medical products, due to its uniqueness in biomedical applications. Uptake of these particles via various administration routes can also lead to different toxic effects. In this study, we assessed the toxic effect of 11–75 nm ranged

Nano- and micro-scale engineered surface structures are often used to control cell morphology and mimic the extracellular matrix in tissue engineering. However, there is little understanding of how toxins produced by common bacteria might affect cell adhesion to these structures. In this study, human dermal fibroblast (GM5565) cells were incubated on patterned tungsten/silicon oxide nanocomposite in

In this work, a new ternary Ag/AgI/Ag3BiO3 photocatalyst was fabricated by an in-situ precipitation method, where Ag0 nanoparticles, serving as a mediator, implanted on the surface of glossy AgI, quantum efficiency being improved attributed to the surface plasmon resonance (SPR) effect. The composites showed superior photocatalytic performance to methylene blue (MB) degradation under visible illumination

The study focuses on the fabrication and properties evaluation of dual functional electrospun polycaprolactone scaffolds incorporating antibiotic drug cefuroxime and having custom tailored topography for the support of human cells to be used in tissue regeneration. The scaffolds were evaluated in regard to their morphology, total porosity, thermal properties, tensile properties and cells adhesion/growth

There are a relatively large number of studies on surfactants facilitates the dispersion of multi-walled carbon nanotubes (MWCNTs), however reports for both orientation and size aggregation of surfactants on MWCNTs are scarcely described. In this study, we demonstrate the visualization of the surfactants aggregates onto MWCNTs using atomic force microscopic (AFM) and field emission electron scanning

Samarium oxychloride (SmOCl) is a promising photocatalyst for environment remediation. It is difficult to form SmOCl nanoplate by sophisticated wet chemical techniques used to prepare other layer-structured rare earth oxychloride nanoplates. Here, we report the synthesis of SmOCl nanoplates by chemical vapour deposition (CVD). Transmission electron microscopy characterization reveals that the nanoplates

We presented a simple and efficient strategy for deposition of gold nanoparticles (AuNPs) upon transparent bare and indium tin oxide (ITO) film coated glass substrate using gold colloids as Au sources. The method involved two steps: embedding in polyvinyl alcohol (PVA) film and annealing at high temperature. The AuNPs deposited on solid substrate because of migration and coalescence of gold at high

(2019). Correction. Journal of Experimental Nanoscience: Vol. 14, No. 1, pp. 171-171.

Mutated COX-2 has become the new molecular marker of aspirin resistance. However, there is still a technical ‘bottleneck’ for direct and sensitive detection of circulating COX-2 mutant gene. In this work, we reported a simple and ultrasensitive electrochemical method for COX-2–765G/C (rs20417) detection for the first time. Polyallylamine (PAA) functionalised Pt nanostructures with long-spined sea urchin-like

Currently, nanoparticles have been widely used as lubricant additives, few researches have investigated their applications as additives for lubricating grease. In this paper, mixtures of ZnO and Si3N4 nanoparticles were added into grease as additives. XRD and TEM were utilized to the investigate phase composition, microstructure and morphology of the nanomaterials. The composite grease was prepared

The commercialisation of polymer electrolyte fuel cells (PEFCs) has been hampered by the high cost of platinum metal. Due to its high durability and catalytic activity, platinum is widely used to catalyse the oxygen reduction and hydrogen oxidation reactions essential to the operation of these cells. Core@shell nanoparticles with thin layers of platinum deposited on cores composed of cheaper materials

ZnO@SiO2-TTIP was synthesised as a novel heterogeneous catalyst and characterised by FT-IR, XRD, TEM, SEM and N2 adsorption-desorption. In this catalytic system, TTIP acts as a dopant agent for ZnO@SiO2 to decreases the recombination of photogenerated electron/hole pairs and improves the catalyst activity. The catalyst was successfully utilised for the synthesis of 2-substituted benzimidazoles and

In this research, a one step, facile route has been undertaken to synthesise copper oxide/reduced graphene oxide (CuO/rGO) nanocomposites. X-ray powder diffraction analysis (XRD) was carried out to identity the crystalline structure and phase of the synthesised sample. Elemental analysis and surface morphological features were analysed using EDX and FESEM Images. Particle size as well as the shape

This article presents an experimental investigation of domestic refrigerator using R134a as working fluid with different concentration of Al2O3, TiO2 nano particles and nano composite particles dispersed in polyolester (POE) oil lubricant. All the nano particles were added to the POE oil with 0.1gL−1 volume concentration. The experiments are conducted for different compositions such as R134a with POE

A nano enhanced phase change material, NEPCM, was prepared by the addition of carbon nanotubes, CNTs, to butyl stearate. This study utilised single walled nano tube, multi-walled nanotube and modified multi-walled nanotube. Several kinds of surfactants were used to stabilise nano-particles in butyl stearate. Tetramethyl ethylene diamine (TEMED) was the best surfactant for enhancing the stability time

Tribochemical silica coating is a common practice to achieve suitable adhesion with intended synthetic substrates or natural tissues, and the key to this technology is the preparation of alumina abrasive coated by nano-silica (AACNS). In this paper, a novel physical method of producing silicon nanoparticles (SiNPs) that is the base to AACNS is put forward in this paper. The source of the silica coating

In this work, different microfluidic colour-changing devices are implemented by using dry film photoresist-based moulds instead of standard photolithography moulds. EtertecHT-115T negative dry film photoresist is employed to realise the rapid fabrication of the moulds for colour-changing layers. The major factors that may affect the fidelity of the dry film moulds during fabrication are summarised

A number of strontium-based iron oxides are available for the industrial use. Among them, strontium hexaferrite cobalt iron oxide (Sr2Co2Fe12O22) is preferred over others due to its better magnetic and electrical properties than others. This material is also extensively used for the absorption of microwave radiations. This study was conducted to account for the synthesis and characterization of Sr2Co2Fe12O22

Microsize Powders of Ni and Cu were prepared by water atomization technique to fabricate metal matrix composites containing various percentages of nanosized boron nitride particles (1, 2, 3, 4, 5 wt. % of BN in a matrix containing (20 wt. %Ni and 80 wt. %Cu). The prepared mixtures were cold compacted under 400 MPa, and sintered for 2 h at 1000 °C in a controlled atmosphere of 3:2 N2/H2 gas mixtures

As the transistor size approaches nano dimension, short channel effects become dominant in micro devices, leading to an incessant struggle to keep pace with Moore's law. This paved way to development of newer technologies like molecular electronics. The self-assembled bottom-up approach makes molecular switches more prone to defects than micro devices. The widely studied molecular switches are mechanically

In this study ZSM-5 Nano particles with high crystallinity were synthesized using a dry gel conversion technique. An L9 orthogonal array of the Taguchi method was applied to investigate the effect of synthesis parameters, such as crystallization time, gel drying temperature, molar composition of template (TPAOH) and water content in the crystallization stage on crystallinity and particle size of the

Little information is available on Titanium dioxide nanoparticles (nTiO2) behavior in different culture media for aquatic organisms. This study aimed to accurately evaluate nTiO2 dispersion and sedimentation in common freshwater algae (BG-11) and daphnia aquatic (SM7) culture media. We additionally investigated potential mechanisms of nTiO2 stability under arsenate influence. Results showed that high