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A transnational perspective on the evolution of the synthetic cannabinoid receptor agonists market: Comparing prison and general populations Drug Test. Anal. (IF 2.903) Pub Date : 2021-01-19 Caitlyn Norman; Sebastian Halter; Belal Haschimi; Dean Acreman; Josie Smith; Alex J. Krotulski; Amanda L.A. Mohr; Barry K. Logan; Niamh NicDaéid; Volker Auwärter; Craig McKenzie
The synthetic cannabinoid receptor agonist (SCRA) market is transnational and the availability of individual SCRAs changes regularly in response to national and international legislative controls. This generates a cyclic pattern and near constant evolution of SCRA compounds. This study reports toxicology‐based and/or seized sample‐based prevalence data relating to SCRA use in prisons from Germany,
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Metabolic studies of HIF stabilizers IOX2, IOX3, and IOX4 (in vitro) for doping control Drug Test. Anal. (IF 2.903) Pub Date : 2021-01-17 Moses Philip; Binoy Mathew; Tajudheen K. Karatt; Zubair Perwad; Michael Benedict Subhahar; Abdul Khader Karakka Kal
The transcriptional activator HIF (hypoxia‐inducible factor) is a vital arbitrator in the performance of cellular responses lacking oxygen supply in aerobic organisms. Since these compounds are capable of enhancing the organism's capacity for molecular oxygen transport, they possess great potential for abuse as a performance‐enhancing agent in sports. A comprehensive study of the metabolic conversion
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Verifying the validity of creatinine measurement in low‐concentrated urine spot samples ‐ photospectrometry vs. liquid chromatography‐tandem mass spectrometry Drug Test. Anal. (IF 2.903) Pub Date : 2021-01-17 Simon Franz; Gisela Skopp; Torsten Dame; Frank Musshoff
One of the major challenges of testing drugs of abuse is the detection of highly diluted urine samples. The ingestion of a large amount of fluid can considerably reduce the concentration of substances, possibly resulting in inaccurate drug testing. For detection, determination of urinary creatinine is a widely established procedure. In this study, results from the most popular methods, including photospectrometry
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The occurrence of non‐ATC‐INN molecules in suspected illegal or illegally traded health products in Europe: A retro‐ and prospective study Drug Test. Anal. (IF 2.903) Pub Date : 2021-01-16 E. Deconinck; C. Vanhee; P.H.J. Keizers; P. Guinot; A. Mihailova; P.V. Syversen; G. Li‐Ship; S. Young; A. Blazewicz; M. Poplawska; J. Loasby Al‐Sayed; L. Stengelshøj Olsen; O. el‐Atma; R. Leist; K.H. Jönsson; M. Afxentiou; M. Mendoza Barrios; I. Dorronsoro Diaz; M. Zemser; A. Kozokin; A. Hackl; M.J. Portela; N. Beerbaum; M. Bertrand
The General European Official Medicines Control Laboratory (OMCL) Network (GEON), co‐ordinated by the European Directorate for the Quality of Medicines & HealthCare (EDQM), regularly organises market surveillance studies on specific categories of suspected illegal or illegally traded products. These studies are generally based on a combination of retrospective and prospective data collection over a
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Issue Information Drug Test. Anal. (IF 2.903) Pub Date : 2021-01-16
No abstract is available for this article.
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Annual banned‐substance review: Analytical approaches in human sports drug testing 2019/2020 Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-12 Mario Thevis; Tiia Kuuranne; Hans Geyer
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Effects of theophylline and theobromine on exercise performance and implications for competition sport: A systematic review Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-13 Michael Kennedy
A systematic review was undertaken to evaluate studies on the effects of theophylline and theobromine on exercise performance in normal (healthy) subjects. Theophylline was found to have been studied on eight occasions and theobromine on one, the number of subjects per study ranging from seven to 15. In two exercise investigations, theophylline was superior to placebo at a p < 0.05 level and no different
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Stability of synthetic cathinones in clinical and forensic toxicological analysis—Where are we now? Drug Test. Anal. (IF 2.903) Pub Date : 2020-12-07 Abdulaziz A. Aldubayyan; Erika Castrignanò; Simon Elliott; Vincenzo Abbate
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Dried blood spots for anti‐doping: Why just going volumetric may not be sufficient Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-17 Marc Luginbühl; Stefan Gaugler
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Data from a microdosed rhEPO administration study applying the new biotinylated clone AE7A5 antibody and a further optimized SAR‐PAGE protocol Drug Test. Anal. (IF 2.903) Pub Date : 2021-01-15 Christian Reichel; Damir Erceg; Barbara Lorenc; Veronika Scheiblhofer; Letizia Farmer; Katharina Zanitzer; Thomas Geisendorfer; Günter Gmeiner; Mario Thevis
Erythropoietin (EPO) is a hormone, which stimulates the production of red blood cells. Due to its performance enhancing effect, it is prohibited by the World Anti‐Doping Agency (WADA). In order to reduce the detection window of EPO‐doping, athletes have been applying low doses of recombinant EPO (e.g. < 10 IU/kg body weight, daily or every second day) instead of larger doses twice or more per week
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A review of nicotine‐containing electronic cigarettes – trends in use, effects, contents, labelling accuracy and detection methods Drug Test. Anal. (IF 2.903) Pub Date : 2021-01-15 Amelia Taylor; Keeley Dunn; Sophie Turfus
Electronic cigarettes (ECs) are thought to be less harmful than traditional combustible cigarettes and were originally intended to help smokers quit. Over the past two decades, they have especially gained popularity with the younger generation. To date, there are over 7000 unique e‐liquid flavours available and over 400 different e‐cigarette brands. The accuracy of nicotine strength labelling in e‐liquids
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Single hair analysis: Validation of a screening method for over 150 analytes and application on documented single‐dose cases Drug Test. Anal. (IF 2.903) Pub Date : 2021-01-15 Christopher Wiedfeld; Gisela Skopp; Frank Musshoff
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Forensic application and evaluation of a commercially available pregabalin immunoassay test in serum on an Olympus AU480 Drug Test. Anal. (IF 2.903) Pub Date : 2020-12-29 Cornelius Hess; Sandra Zeidler; Joerg Roehrich
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Doping Detection in Animals – A Review of Analytical Methodologies Published from 1990 to 2019 Drug Test. Anal. (IF 2.903) Pub Date : 2021-01-13 Fernando X. Moreira; Helena Carmo; Maria Paula Guedes de Pinho; Maria de Lourdes Bastos
Despite the impressive innate physical abilities of horses, camels, greyhounds or pigeons, doping agents might be administered to these animals to improve their performance. To control these illegal practices, anti‐doping analytical methodologies have been developed. This review compiles the analytical methods that have been published for the detection of prohibited substances administered to animals
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Stability of phosphatidylethanol 16:0/18:1 in authentic and spiked whole blood Drug Test. Anal. (IF 2.903) Pub Date : 2021-01-04 Catalina Dumitrascu; Maria C.A. van de Lavoir; Hugo Neels; Adrian Covaci; Werner Jacobs; Diona D'Hondt; Alexander L.N. van Nuijs
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β2‐Adrenoceptor agonist activity of higenamine Drug Test. Anal. (IF 2.903) Pub Date : 2020-12-26 Thomas J. Hudzik; Metul Patel; Andrew Brown
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Performance evaluation of handheld Raman spectroscopy for cocaine detection in forensic case samples Drug Test. Anal. (IF 2.903) Pub Date : 2020-12-23 Ruben F. Kranenburg; Joshka Verduin; Renee de Ridder; Yannick Weesepoel; Martin Alewijn; Marcel Heerschop; Peter H.J. Keizers; Annette van Esch; Arian C. van Asten
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Label‐free proteomics for discovering biomarker candidates of RAD140 administration to castrated horses Drug Test. Anal. (IF 2.903) Pub Date : 2020-12-04 Hiu Wing Cheung; Kin‐Sing Wong; Ning Sum To; Amanda J. Bond; Adrian F. Farrington; Anil Prabhu; Peter Curl; Terence S.M. Wan; Emmie N.M. Ho
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Estimation of alcohol and nicotine consumption in 11 cities of Turkey using wastewater‐based epidemiology Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-17 Evsen Yavuz Guzel; Aslı Atasoy; İsmail Ethem Gören; Nebile Daglioglu
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Doping in the Ultimate Fighting Championship (UFC): A 4‐year epidemiological analysis Drug Test. Anal. (IF 2.903) Pub Date : 2020-12-03 Mohamad Y. Fares; Hasan Baydoun; Hamza A. Salhab; Hussein H. Khachfe; Youssef Fares; Jawad Fares; Joseph A. Abboud
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Two‐dimensional high performance liquid chromatography purification of underivatized urinary testosterone and metabolites for compound‐specific stable carbon isotope analysis Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-05 Karine Lalonde; Andrew Barber; Christiane Ayotte
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LC‐HRMS characterization of the skin pigmentation and sexual enhancers melanotan II and bremelanotide sold on the black market of performance and image enhancing drugs Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-27 Serena Mestria; Sara Odoardi; Giampietro Frison; Sabina Strano Rossi
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An in vitro assay approach to investigate the potential impact of different doping agents on the steroid profile Drug Test. Anal. (IF 2.903) Pub Date : 2020-12-07 Thomas Piper; Sonja Heimbach; Martin Adamczewski; Mario Thevis
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Preliminary data on the potential for unintentional antidoping rule violations by permitted cannabidiol (CBD) use Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-30 Ute Mareck; Gregor Fusshöller; Hans Geyer; Marilyn A. Huestis; Anja B. Scheiff; Mario Thevis
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Investigations into the stable isotope ratios of 1‐phenyl‐2‐propanone Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-12 Kate Lansdown; Katrina A. Jolliffe; Helen Salouros
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Issue Information Drug Test. Anal. (IF 2.903) Pub Date : 2020-12-15
No abstract is available for this article.
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The 38th Manfred Donike workshop on doping analysis Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-21 Mario Thevis
Since 1983, the Manfred‐Donike‐Workshop on Doping Analysis has been annually held in Cologne, Germany, and sadly, this year, the community was to mourn for one of its early and most respected colleagues.1 The meeting's 38th edition was organized February 9–14, 2020, shortly before the COVID‐19 pandemic struck the world with full fury, in anticipation of the Games of the XXXII Olympiad in Tokyo, Japan
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Detection of clostebol in sports: Accidental doping? Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-29 Xavier de la Torre; Cristiana Colamonici; Michele Iannone; Daniel Jardines; Francesco Molaioni; Francesco Botrè
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Excretion of 19‐norandrosterone after consumption of boar meat Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-30 Frank Hülsemann; Gregor Fußhöller; Christine Lehn; Mario Thevis
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The analytical approach for detection of carbamylated erythropoietin for doping control purposes Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-29 Paweł Kaliszewski; Paulina Siek; Zofia Zalewska; Dorota Michalak; Dorota Kwiatkowska
Erythropoietin (EPO) has protective effects in several tissues and could be used for therapeutic purposes, but the doses of EPO that can be beneficial in case of hypoxic–ischemic conditions due to overinduced erythropoiesis could be detrimental in treated patients. Carbamylation of erythropoietin maintains the tissue‐protective effects of EPO but without erythropoietic effects. Carbamylated EPO (CEPO)
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The intra‐individual stability of GH biomarkers IGF‐I and P‐III‐NP in relation to GHRH administration, menstrual cycle, and hematological parameters Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-30 Magnus Ericsson; Hasanuzzaman Bhuiyan; Basam Yousif; Mikael Lehtihet; Lena Ekström
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Analysis of cobalt for human sports drug testing purposes using ICP‐ and LC‐ICP‐MS Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-03 Andre Knoop; Peter Planitz; Bernhard Wüst; Mario Thevis
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Towards compound identification of synthetic opioids in nontargeted screening using machine learning techniques Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-18 Joshua Klingberg; Adam Cawley; Ronald Shimmon; Shanlin Fu
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Shape matters: The application of activity‐based in vitro bioassays and chiral profiling to the pharmacological evaluation of synthetic cannabinoid receptor agonists in drug‐infused papers seized in prisons Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-08 Lysbeth H. Antonides; Annelies Cannaert; Caitlyn Norman; Niamh NicDáeid; Oliver B. Sutcliffe; Christophe P. Stove; Craig McKenzie
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Detecting the abuse of 19‐norsteroids in doping controls: A new gas chromatography coupled to isotope ratio mass spectrometry method for the analysis of 19‐norandrosterone and 19‐noretiocholanolone Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-26 Loredana Iannella; Cristiana Colamonici; Davide Curcio; Francesco Botrè; Xavier de la Torre
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Increase in drugs‐of‐abuse findings in post‐mortem toxicology due to COVID‐19 restrictions—First observations in Finland Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-20 Claudia Mariottini; Ilkka Ojanperä; Pirkko Kriikku
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An optimized SDS‐PAGE protocol with a new blotting system for the initial testing procedure of ESAs in doping control Drug Test. Anal. (IF 2.903) Pub Date : 2020-12-02 Laurent Martin; Jean‐Antoine Martin; Michel Audran; Alexandre Marchand
Recombinant erythropoietins (rEPOs) are still among the substances endurance athletes use for doping. Detection methods are based on an electrophoretic separation of the proteins followed by a western blot and immunodetection with specific anti‐EPO antibodies. In addition to IEF‐PAGE, the SDS‐PAGE method has been used to differentiate endogenous EPO from rEPOs by their molecular weight (MW). However
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Detection of ethinyl estradiol and resorcylic acid lactones in poultry meat according to the national residue plan Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-25 Loredana Annunziata; Pierina Visciano; Maria Rosaria De Massis; Maria Schirone; Maria Novella Colagrande; Guido Campana; Giacomo Migliorati
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A validated method for the simultaneous quantification of cannabidiol, Δ9‐tetrahydrocannabinol, and their metabolites in human plasma and application to plasma samples from an oral cannabidiol open‐label trial Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-23 Richard C. Kevin; Rebecca Vogel; Peter Doohan; Maximus Berger; G. Paul Amminger; Iain S. McGregor
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Detection of intact insulin analogues in post‐mortem vitreous humour—Application to forensic toxicology casework Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-16 Nicola Beckett; Rebecca Tidy; Bianca Douglas; Colin Priddis
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Horseradish‐peroxidase‐conjugated anti‐erythropoietin antibodies for direct recombinant human erythropoietin detection: Proof of concept Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-29 Sven C. Voss; Nelson N. Orie; Wesal El‐Saftawy; Stephanie Saghbazarian; Alanoud Al‐Kaabi; Costas Georgakopoulos; Ioanna Athanasiadou; Vidya Mohamed‐Ali; Mohammed Al‐Maadheed
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On the road of dried blood spot sampling for antidoping tests: Detection of GHRP‐2 abuse Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-16 Gemma Reverter‐Branchat; Jordi Segura; Oscar J. Pozo
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The colloidal gold nanoparticle‐based lateral flow immunoassay for fast and simple detection of plant‐derived doping agent, higenamine Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-20 Poomraphie Nuntawong; Akihiro Ochi; Jiranan Chaingam; Hiroyuki Tanaka; Seiichi Sakamoto; Satoshi Morimoto
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An infrared spectroscopic approach to characterise white powders, easily applicable in the context of drug checking, drug prevention and on‐site analysis Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-16 Eric Deconinck; Camille Aït‐Kaci; Andries Raes; Michaël Canfyn; Jean‐Luc Bothy; Céline Duchateau; Corenthin Mees; Kris De Braekeleer; Lies Gremaux; Peter Blanckaert
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Pharmacokinetics of salmeterol and its main metabolite α‐hydroxysalmeterol after acute and chronic dry powder inhalation in exercising endurance‐trained men: Implications for doping control Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-17 Søren Jessen; Victoria Becker; Sebastian Rzeppa; Vibeke Backer; Kasper Høtoft Bengtsen; Ingunn Hullstein; Yvette Dehnes; Morten Hostrup
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Low‐volume LC–MS/MS method for the pharmacokinetic investigation of carvedilol, enalapril and their metabolites in whole blood and plasma: Application to a paediatric clinical trial Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-30 Tanja Gangnus; Bjoern B. Burckhardt;
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Elimination profiles of prednisone and prednisolone after different administration routes: Evaluation of the reporting level and washout periods to ensure safe therapeutic administrations Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-08 Sergi Coll; Núria Monfort; Élida Alechaga; Xavier Matabosch; Oscar J. Pozo; Clara Pérez‐Mañá; Rosa Ventura
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Urinary steroid profile in relation to the menstrual cycle Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-03 Jenny Schulze; Tina Suominen; Helena Bergström; Magnus Ericsson; Linda Björkhem Bergman; Lena Ekström
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New application of the CRISPR‐Cas9 system for site‐specific exogenous gene doping analysis Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-17 Joon‐Yeop Yi; Minyoung Kim; Hophil Min; Byung‐Gee Kim; Junghyun Son; Oh‐Seung Kwon; Changmin Sung
The increased potential for gene doping since the introduction of gene therapy presents the need to develop anti‐doping assays. We therefore aimed to develop a quick and simple method for the detection of specifically targeted exogenous doping genes utilizing an in vitro clustered regularly interspaced short palindromic repeats‐CRISPR associated protein 9 (CRISPR‐Cas9) system. A human erythropoietin
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Metabolism and excretion of the benzodiazepine analogue etizolam in the horse Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-09 Erin Johnson; Jasper van Heemst; Jeshurun Benavides; Bobby Gray
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Quantification of direct-acting oral anticoagulants: Application of a clinically validated liquid chromatography tandem-mass spectrometry method to forensic cases. Drug Test. Anal. (IF 2.903) Pub Date : 2020-09-22 Martin H J Wiesen,Cornelia Fietz,Martin Jübner,Stefanie Iwersen-Bergmann,Hilke Andresen-Streichert,Carsten Müller,Thomas Streichert
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Biosafety Level 2 cabinet UV‐C light exposure of sports antidoping human urine samples does not affect the stability of selected prohibited substances Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-29 Sven Voss; Wadha Abushreeda; Ariadni Vonaparti; Aisha Al‐Wahaibi; Noora Al‐Sowaidi; Ibrahim Al‐Mohannadi; Souhila Mahieddine; Safa Khelifi; Sofia Salama; Amal Saleh; Maryam Al‐Mohannadi; Wesal El‐Saftawy; Khalifa Al‐Hamad; Ahmad Nofal; Najib Dbes; Rodrigo Aguilera; Mohammed Al Maadheed; Costas Georgakopoulos
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Linking long noncoding RNAs (lncRNAs) and doping detection Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-29 Bernardo Bonilauri; Bruno Dallagiovanna
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New qualitative analysis strategy for illicit drugs using Raman spectroscopy and characteristic peaks method Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-03 Cui‐Mei Liu; Hong‐Yuan He; Lin Xu; Zhen‐Dong Hua
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The effect of serial administration of bicarbonate on plasma total CO2 concentrations in horses Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-08 Simon R. Bailey; Grace Forbes; Naomi Selvadurai; Katelin McLarney; Susan Jones; Catherine M. Steel
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Stability of psilocybin and its four analogs in the biomass of the psychotropic mushroom Psilocybe cubensis Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-29 Klára Gotvaldová; Kateřina Hájková; Jan Borovička; Radek Jurok; Petra Cihlářová; Martin Kuchař
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Kinetic profile of N,N‐dimethyltryptamine and β‐carbolines in saliva and serum after oral administration of ayahuasca in a religious context Drug Test. Anal. (IF 2.903) Pub Date : 2020-10-29 Rafael Lanaro; Sueli Moreira Mello; Kelly Francisco da Cunha; Gabriela Silveira; Nelson Francisco Corrêa‐Neto; Stephen Hyslop; Oscar G. Cabrices; Jose Luiz Costa; Alessandra Linardi
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Hair analysis can support the follow‐up addiction care after acute New Psychoactive Substances intoxication: Illustration by two cases Drug Test. Anal. (IF 2.903) Pub Date : 2020-11-02 Jennifer Lagoutte‐Renosi; Camille Richeval; Mélodie Phanithavong; Jean‐François Wiart; Eugénie Castex; Xavier Vanhoy; Florian Hakim; Sylvie Deheul; Juliana Tournebize; Delphine Allorge; Jean‐Michel Gaulier