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Electrohydrodynamic Encapsulation of Resveratrol Using Food-Grade Nanofibres: Process Optimization, Characterization and Fortification
Food and Bioprocess Technology ( IF 5.6 ) Pub Date : 2019-12-23 , DOI: 10.1007/s11947-019-02399-4
B.G. Seethu , Heartwin A. Pushpadass , F. Magdaline Eljeeva Emerald , B. Surendra Nath , N. Laxmana Naik , K.S. Subramanian

Utilization of resveratrol as a nutraceutical in foods is limited due to its low bioavailability and chemical instability. Therefore, resveratrol was encapsulated into nanofibres by electrospinning at concentrations of 15, 18 and 21% TS, applied voltage of 13, 18 and 23 kV and feed rates of 0.6 and 1 mL/h using WPI-pullulan as wall material. Electrospinning conditions were optimized as 18% TS, 18 kV applied voltage and 0.6 mL/h flow rate. SEM images showed formation of clean and continuous fibres at 18 and 23 kV applied voltage, with a mean fibre diameter of 63 to 208 nm and encapsulation efficiency of 74 and 96.70%. Successful encapsulation of resveratrol was confirmed by FTIR and XRD analyses. The zeta potential of resveratrol-loaded nanofibres was in the range of − 20.5 to − 32.2 mV, suggestive of higher stability. The antioxidant property of resveratrol in nanofibres was retained. No significant physiochemical and sensorial changes were observed in resveratrol fortified milk.

中文翻译:

食品级纳米纤维对白藜芦醇的电流体动力学封装:工艺优化,表征和设防。

由于白藜芦醇的生物利用度低和化学稳定性差,因此在食品中作为营养品的用途受到限制。因此,通过使用WPI-普鲁兰聚糖作为壁材料,以15%,18%和21%TS的浓度,13、18和23 kV的施加电压以及0.6和1 mL / h的进料速度进行电纺丝,将白藜芦醇封装到纳米纤维中。将静电纺丝条件优化为18%TS,18 kV施加电压和0.6 mL / h流速。SEM图像显示在18和23kV施加电压下形成清洁且连续的纤维,平均纤维直径为63至208nm,包封效率为74和96.70%。FTIR和XRD分析证实了白藜芦醇的成功包封。负载白藜芦醇的纳米纤维的ζ电势在− 20.5至− 32.2 mV的范围内,表明具有更高的稳定性。保留了白藜芦醇在纳米纤维中的抗氧化性能。在白藜芦醇强化牛奶中未观察到明显的理化和感官变化。
更新日期:2019-12-23
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