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Continuous alumina fiber-reinforced yttria-stabilized zirconia composites with high density and toughness
Journal of the European Ceramic Society ( IF 5.7 ) Pub Date : 2019-12-20 , DOI: 10.1016/j.jeurceramsoc.2019.12.041
Xuewu Li , Xiaohui Fan , Na Ni , Xiaofeng Zhao , Chuanwei Li , Ping Xiao

Continuous alumina fiber-reinforced yttria-stabilized zirconia (YSZ) composites with a LaPO4 fiber coating were fabricated by slurry infiltration and spark plasma sintering (SPS). The LaPO4 coating was deposited on the reinforcement alumina fabrics by a modified sol-gel method. The YSZ slurry with good dispersion and stability was prepared by optimizing the pH value, dispersant addition and ball milling time. The fabricated composite with a high density of ∼ 92 % has a good flexural strength of 277 ± 43 MPa, and a superior fracture toughness of 15.93 ± 0.75 MPa·m1/2 exhibiting a non-brittle failure behavior. It was found that the LaPO4 coating reduced the residual stress near the fiber/matrix interface to 131 ± 41 MPa, which was 369 ± 63 MPa in the composite without the fiber coating. The LaPO4 coating renders a weak interphase to improve the composite toughness by activating several toughening mechanisms including crack deflection, fiber debonding and pullout, and delamination behavior.



中文翻译:

具有高密度和韧性的连续氧化铝纤维增强的氧化钇稳定的氧化锆复合材料

通过浆料浸渗和电浆等离子体烧结(SPS),制备了具有LaPO 4纤维涂层的连续氧化铝纤维增强的氧化钇稳定的氧化锆(YSZ)复合材料。通过改进的溶胶-凝胶法将LaPO 4涂层沉积在增强氧化铝织物上。通过优化pH值,添加分散剂和球磨时间,制备了具有良好分散性和稳定性的YSZ浆料。所制成的高密度〜92%的复合材料具有277±43 MPa的良好抗弯强度,以及15.93±0.75 MPa·m 1/2的优异断裂韧性,表现出非脆性破坏行为。发现LaPO 4涂层将纤维/基体界面附近的残余应力降低到131±41 MPa,在没有纤维涂层的复合材料中为369±63 MPa。LaPO 4涂层通过激活几种增韧机制(包括裂纹偏转,纤维脱粘和拉拔以及脱层行为),提供了弱的中间相,从而提高了复合材料的韧性。

更新日期:2019-12-20
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