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Antibacterial activity of ZnO nanoflowers deposited on biodegradable acrylic acid hydrogel by chemical bath deposition
Bulletin of Materials Science ( IF 1.8 ) Pub Date : 2019-12-18 , DOI: 10.1007/s12034-019-1967-1
Sinan Temel , Fatma Ozge Gokmen , Elif Yaman

In the first part of this study, acrylic acid (AA) hydrogels were produced by a free radical reaction. Chemical and morphological structures of AA-hydrogels were specified by using Fourier transform infrared (FT-IR) spectroscopy and scanning electron microscopy (SEM) techniques. In the second part of the study, ZnO nanoflowers were synthesized on the AA-hydrogel by using a chemical bath deposition (CBD) technique for the first time in the literature. The AA-hydrogel acted as the substrate in the CBD process. The deposition time effect on the morphological properties of ZnO nanoflowers was determined by applying SEM. According to the SEM results, the deposition time in the production of ZnO nanoflowers has played a vital role in the surface morphology. Chemical, morphological and thermal properties of the ZnO nanoflowers were determined by applying FT-IR, scanning electron microscopy-energy dispersive X-ray spectroscopy and thermogravimetric analysis techniques. Elemental mapping of ZnO nanostructures was carried out using SEM. The antibacterial activity of the ZnO nanoflower-deposited AA-hydrogel was determined against Gram-negative and Gram-positive bacteria. Escherichia coli (E. coli) and Staphylococcus aureus (S. aureus) were used as test microorganisms. Gram-negative bacteria were more resistant to hydrogels and ZnO nanoflowers compared to Gram-positive bacteria.

中文翻译:

通过化学浴沉积沉积在可生物降解丙烯酸水凝胶上的 ZnO 纳米花的抗菌活性

在本研究的第一部分,丙烯酸 (AA) 水凝胶是通过自由基反应生产的。通过使用傅里叶变换红外 (FT-IR) 光谱和扫描电子显微镜 (SEM) 技术指定 AA-水凝胶的化学和形态结构。在研究的第二部分,文献中首次使用化学浴沉积 (CBD) 技术在 AA-水凝胶上合成了 ZnO 纳米花。AA-水凝胶作为 CBD 过程中的底物。通过应用扫描电镜确定沉积时间对 ZnO 纳米花形态特性的影响。根据SEM结果,ZnO纳米花生产中的沉积时间对表面形貌起着至关重要的作用。化工,通过应用 FT-IR、扫描电子显微镜-能量色散 X 射线光谱和热重分析技术确定了 ZnO 纳米花的形态和热性能。使用 SEM 进行 ZnO 纳米结构的元素映射。ZnO 纳米花沉积的 AA-水凝胶对革兰氏阴性和革兰氏阳性细菌的抗菌活性被确定。大肠杆菌(E.coli)和金黄色葡萄球菌(S.aureus)用作测试微生物。与革兰氏阳性菌相比,革兰氏阴性菌对水凝胶和 ZnO 纳米花的抵抗力更强。ZnO 纳米花沉积的 AA-水凝胶对革兰氏阴性和革兰氏阳性细菌的抗菌活性被确定。大肠杆菌(E.coli)和金黄色葡萄球菌(S.aureus)用作测试微生物。与革兰氏阳性菌相比,革兰氏阴性菌对水凝胶和 ZnO 纳米花的抵抗力更强。ZnO 纳米花沉积的 AA-水凝胶对革兰氏阴性和革兰氏阳性细菌的抗菌活性被确定。大肠杆菌(E.coli)和金黄色葡萄球菌(S.aureus)用作测试微生物。与革兰氏阳性菌相比,革兰氏阴性菌对水凝胶和 ZnO 纳米花的抵抗力更强。
更新日期:2019-12-18
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