当前位置: X-MOL 学术Org. Lett. › 论文详情
Our official English website, www.x-mol.net, welcomes your feedback! (Note: you will need to create a separate account there.)
Correction to “Radially Oriented [n]Cyclo-meta-phenylenes”
Organic Letters ( IF 5.2 ) Pub Date : 2022-07-29 , DOI: 10.1021/acs.orglett.2c02372
Edison Castro , Saber Mirzaei , Raúl Hernández Sánchez

The sentence “Aside from previous attempts,11” is corrected to “Aside from one previous report,11”. Coupling constants for 1H NMR signals have been added to the revised Supporting Information file with this Correction. The assignment of protons d′ and e′/e*′ in 2 to specific signals in the 1H NMR spectrum is not unequivocally supported by the coupling constants. In addition, the statement “the long-range coupling 4J observed in 2 helped us deduce the resonances coming from a′ to e′” is withdrawn, as there is no direct support from COSY or other experiments. The structural assignment of 2 is in accord with the MALDI data. The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acs.orglett.2c02372. Experimental details; crystallographic data; 1H, 13C, COSY, HSQC, and HMBC NMR spectra; and DFT calculations (PDF) Most electronic Supporting Information files are available without a subscription to ACS Web Editions. Such files may be downloaded by article for research use (if there is a public use license linked to the relevant article, that license may permit other uses). Permission may be obtained from ACS for other uses through requests via the RightsLink permission system: http://pubs.acs.org/page/copyright/permissions.html. This article has not yet been cited by other publications. The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acs.orglett.2c02372. Experimental details; crystallographic data; 1H, 13C, COSY, HSQC, and HMBC NMR spectra; and DFT calculations (PDF) Most electronic Supporting Information files are available without a subscription to ACS Web Editions. Such files may be downloaded by article for research use (if there is a public use license linked to the relevant article, that license may permit other uses). Permission may be obtained from ACS for other uses through requests via the RightsLink permission system: http://pubs.acs.org/page/copyright/permissions.html.

中文翻译:

更正“径向取向的 [n]Cyclo-meta-phenylenes”

句子“除以前的尝试外,11 ”更正为“除以前的报告外,11 ”。1 H NMR 信号的耦合常数已通过此更正添加到修订后的支持信息文件中。耦合常数并未明确支持将 2 中的质子 d' 和 e'/e*' 分配给 1 H NMR 光谱特定信号。此外,“在2中观察到的长程耦合4J帮助我们推断了从 a' 到 e' 的共振”的陈述被撤回,因为没有来自 COZY 或其他实验的直接支持。2的结构分配与 MALDI 数据一致。支持信息可在 https://pubs.acs.org/doi/10.1021/acs.orglett.2c02372 免费获得。实验细节;晶体学数据;1小时,13C、COSY、HSQC 和 HMBC NMR 谱图;和 DFT 计算 (PDF) 大多数电子支持信息文件无需订阅 ACS 网络版即可获得。此类文件可以按文章下载以供研究使用(如果有与相关文章链接的公共使用许可,则该许可可能允许其他用途)。可通过 RightsLink 许可系统请求从 ACS 获得其他用途的许可:http://pubs.acs.org/page/copyright/permissions.html。这篇文章尚未被其他出版物引用。支持信息可在 https://pubs.acs.org/doi/10.1021/acs.orglett.2c02372 免费获得。实验细节;晶体学数据;1小时,13C、COSY、HSQC 和 HMBC NMR 谱图;和 DFT 计算 (PDF) 大多数电子支持信息文件无需订阅 ACS 网络版即可获得。此类文件可以按文章下载以供研究使用(如果有与相关文章链接的公共使用许可,则该许可可能允许其他用途)。可通过 RightsLink 许可系统请求从 ACS 获得其他用途的许可:http://pubs.acs.org/page/copyright/permissions.html。
更新日期:2022-07-29
down
wechat
bug