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Wear Performance of TiCN Coating on Medium-Carbon Steel by Composite Thermo-Reactive Deposition
Transactions of the Indian Institute of Metals ( IF 1.6 ) Pub Date : 2022-06-22 , DOI: 10.1007/s12666-022-02649-8
Wei Wang , Yepeng Tu , Caiyuan Sun , Jin Zhang , Songxia Li

Duplex surface treatment of AISI 1045 steel involves nitriding followed by titanium thermo-reactive deposition (TRD) techniques at 900 ℃ for 3 h. The treatment forms a titanium carbonitride coating with a maximum thickness of 8.5 μm. Characterization using a scanning electron microscope equipped with an energy-dispersive X-ray spectrometer (SEM–EDS) and X-ray diffraction (XRD) indicated that the compact and dense coatings mainly consisted of Ti(C0.51N0.21) and Fe0.975Ti0.025 phases. Furthermore, the microhardness and tribological properties of the coating treated at 900 ℃ for 3 h were investigated using microhardness test and wear test. The average hardness value of the pre-nitride coating is 1136 HV0.05 and that of the composite treatment coating is 2166 HV0.05, which are 4.6 and 8.8 times that of the substrate, respectively. Compared with the substrate, the pre-nitriding layer presented a moderate friction coefficient, whereas the samples with pre-nitriding and titanizing duplex-treated layers showed the best wear resistance.



中文翻译:

复合热反应沉积对中碳钢TiCN涂层的磨损性能

AISI 1045 钢的双相表面处理包括渗氮,然后是钛热反应沉积 (TRD) 技术,在 900 ℃ 下持续 3 小时。该处理形成最大厚度为 8.5 μm 的碳氮化钛涂层。使用配备能量色散 X 射线光谱仪 (SEM-EDS) 和 X 射线衍射 (XRD) 的扫描电子显微镜进行表征表明,致密的涂层主要由 Ti(C 0.51 N 0.21 ) 和 Fe 0.975 Ti组成0.025相。此外,采用显微硬度试验和磨损试验研究了涂层在 900 ℃ 处理 3 h 的显微硬度和摩擦学性能。预氮化涂层的平均硬度值为 1136 HV 0.05复合处理涂层为2166 HV 0.05,分别是基材的4.6倍和8.8倍。与基体相比,预渗氮层具有中等的摩擦系数,而预渗氮和钛化双相处理层的样品表现出最好的耐磨性。

更新日期:2022-06-22
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