An electrochemical synthesis of diazo compounds from hydrazones in yields as high as 99% was performed. This method was elaborated as a useful synthetic method and demonstrated on various diazo compounds (24 examples). Apart from exhibiting an efficiency that matched that of commonly used harsh and toxic chemical oxidants, this reaction is practically simple to set up, requires mild conditions, and is highly electron efficient (3 F/mol).

中文翻译：

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腙电合成稳定的重氮化合物

以高达 99% 的收率从腙进行了重氮化合物的电化学合成。该方法被阐述为一种有用的合成方法，并在各种重氮化合物（24 个例子）上进行了证明。除了表现出与常用的苛刻和有毒化学氧化剂相匹配的效率外，该反应实际上易于建立，需要温和的条件，并且电子效率高（3 F/mol）。