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Lignin-containing fibers extraction and hydrogel preparation for fiber-optic relative humidity sensor fabrication
Industrial Crops and Products ( IF 5.9 ) Pub Date : 2021-10-01 , DOI: 10.1016/j.indcrop.2021.114112
Xiaotong Fu 1 , Hairui Ji 1 , Xiaohui Liu 2 , Wenyuan Zhu 3
Affiliation  

Herein, a physicochemical pretreatment method, namely, a combination of recyclable acid hydrotrope (p-toluenesulfonic acid, p-TsOH) treatment and ultrasonic treatment (10 s), was employed to extract lignin-containing fibers (LFs) from wood material (poplar). The LFs were used to produce reinforced polyvinyl alcohol (PVA) hydrogels via a dissolution-regeneration process in LiBr⋅3H2O solution. After coating the produced hydrogel on the end face of a single-mode fiber (SMF), a fiber-optic relative humidity sensor (FORHS) was fabricated to monitor environmental humidity. A high sensitivity (4.7 dB) and good repeatability (R 2 = 0.98, the confidence factor) were found within a humidity range from 45 % to 80 %. Therefore, this study provides a sustainable approach for valorization of lignocellulosic biomass.



中文翻译:

用于光纤相对湿度传感器制造的含木质素纤维提取和水凝胶制备

在此,采用物理化学预处理方法,即可回收酸性水溶助长剂(甲苯磺酸,p- TsOH)处理和超声处理(10 s)相结合,从木材(杨树)中提取含木质素纤维(LFs)。)。LFs 用于通过在 LiBr·3H 2 O 溶液中的溶解-再生过程生产增强型聚乙烯醇 (PVA) 水凝胶。在单模光纤 (SMF) 的端面上涂覆产生的水凝胶后,制造了光纤相对湿度传感器 (FORHS) 以监测环境湿度。高灵敏度 (4.7 dB) 和良好的可重复性 ( R 2= 0.98,置信因子)是在 45 % 到 80 % 的湿度范围内发现的。因此,本研究为木质纤维素生物质的增值提供了一种可持续的方法。

更新日期:2021-10-02
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