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Microstructure and high-temperature mechanical properties of co-continuous (Ti3AlC2+ Al3Ti)/2024Al composite fabricated by pressureless infiltration
Ceramics International ( IF 5.2 ) Pub Date : 2021-09-22 , DOI: 10.1016/j.ceramint.2021.09.208
Hongjie Wang 1, 2 , Zhenying Huang 1, 2 , Jiacheng Yi 1, 2 , Xue Li 1, 2 , Ji Zhang 1, 2 , Yuangbo Wang 1, 2 , Weici Zhuang 1, 2 , Qun Yu 1, 2
Affiliation  

Ti3AlC2/2024Al composites with a co-continuous structure were successfully fabricated from 2024Al powders and Ti3AlC2 porous preforms (with porosity of 48%, 41% and 35%, respectively) by pressureless infiltration at 930 °C. Long-rod like Al3Ti was in situ formed due to reaction of Ti atoms de-intercalated from Ti3AlC2 and liquid 2024Al, which interpenetrated with Ti3AlC2 to form a new continuous framework. The mechanical properties in relationship with the initially different volume fractions of Ti3AlC2 and 2024Al at room temperature and high temperature were investigated. At room temperature, 59 vol%Ti3AlC2/2024Al has the best comprehensive mechanical properties, with the flexural strength of 510 MPa, compressive strength of 729 MPa, and compressive strain of 5.49%. Due to the co-continuous structure and the excellent high temperature of Al3Ti, all samples exhibit well mechanical properties at 300 °C. Among them, 52 vol%Ti3AlC2/2024Al has the best performance with the ultimate compressive strength of 532 MPa, which is only 18.7% lower than room temperature. And even at 400 °C,it still has an objective compression strength of 394 MPa due to the highest content of Al3Ti. In addition, after quenching from 400 °C to room temperature, the residual flexural strength of 52 vol%Ti3AlC2/2024Al can be reached to 450 MPa with the mere reduction rate of 7.4%. And no cracks are observed at the boundary of each phase, which means the good thermal shock resistance of the composites.



中文翻译:

无压渗透制备共连续(Ti3AlC2+Al3Ti)/2024Al复合材料的显微组织和高温力学性能

以 2024Al 粉末和 Ti 3 AlC 2多孔预制件(孔隙率分别为 48%、41% 和 35%)在 930 °C 下通过无压渗透成功制备了具有共连续结构的Ti 3 AlC 2 /2024Al 复合材料。由于从Ti 3 AlC 2脱嵌的Ti原子与液态2024Al反应,原位形成像Al 3 Ti这样的长棒,与Ti 3 AlC 2相互渗透形成新的连续骨架。力学性能与初始不同体积分数 Ti 3 AlC 2 的关系和 2024Al 在室温和高温下进行了研究。室温下,59 vol%Ti 3 AlC 2 /2024Al的综合力学性能最好,抗弯强度为510 MPa,抗压强度为729 MPa,压缩应变为5.49%。由于 Al 3 Ti的共连续结构和优异的耐高温性,所有样品在 300 °C 下都表现出良好的机械性能。其中,52 vol%Ti 3 AlC 2 /2024Al性能最佳,极限抗压强度为532 MPa,仅比室温低18.7%。并且即使在 400 °C 下,由于 Al 3含量最高,它仍具有 394 MPa 的客观抗压强度蒂。此外,从400℃淬火至室温后,52vol %Ti 3 AlC 2 /2024Al的残余抗弯强度可达到450 MPa,仅降低7.4%。且各相边界处均未观察到裂纹,表明复合材料具有良好的抗热震性。

更新日期:2021-09-22
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