Journal of Materials Science & Technology ( IF 10.9 ) Pub Date : 2021-08-27 , DOI: 10.1016/j.jmst.2021.06.041 Xu Liu 1 , Lin Song 1 , Andreas Stark 2 , Uwe Lorenz 2 , Zhanbing He 3 , Junpin Lin 3 , Florian Pyczak 2 , Tiebang Zhang 1
In modern β-solidified TiAl alloys, the decomposition of α2 phase is frequently observed during heat treatment or high-temperature deformation of the alloys. In this study, high-temperature deformation and decomposition mechanisms of α2 phase in a Ti-45Al-8.5Nb-0.2B-0.2W-0.02Y alloy are investigated. In a sample deformed at 800 °C, the precipitation of βo(ωo) phase is observed within the equiaxed α2 phase. The nucleation of ωo particles within the βo matrix indicates the α2→βo→ωo transformation. In addition, numerous γ phase precipitates form within the βo(ω) areas. The α2 lamellae decompose into ultrafine (α2+γ) lamellae and coarsened γ lamellae via α2→α2+γ and α2→γ transformation, respectively. Moreover, the ωo phase nucleates within the ultrafine lamellae via α2→ωo transformation. However, in a sample deformed at 1000 °C, the nucleation of βo particles is sluggish, which is caused by the efficient release of the internal stress via dynamic recrystallization (DRX). These results indicate that complex phase transformations can be introduced by the decomposition of α2 phase in TiAl alloys with a high amount of β-stabilizing elements.
中文翻译:
中温压缩高含Nb TiAl合金的变形和相变行为
在现代 β 凝固 TiAl 合金中,在合金的热处理或高温变形过程中经常观察到α 2相的分解。在本研究中,研究了 Ti-45Al-8.5Nb-0.2B-0.2W-0.02Y 合金中α 2相的高温变形和分解机制。在 800 °C 变形的样品中,在等轴 α 2相内观察到β o (ω o ) 相的沉淀。β o矩阵内ω o粒子的成核表明α 2 →β o →ω o转换。此外,β o内会形成大量 γ 相沉淀物。(ω) 区域。α 2薄片分别通过α 2 →α 2 +γ 和α 2 →γ 转变分解为超细(α 2 +γ) 薄片和粗化γ 薄片。此外,ω o相通过α 2 →ω o转变在超细薄片内成核。然而,在 1000 °C 变形的样品中,β o粒子的成核缓慢,这是由于动态再结晶(DRX)有效释放内应力造成的。这些结果表明通过分解 α 2可以引入复杂的相变 TiAl 合金中含有大量 β 稳定元素。