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One-pot synthesis of pyrido[2,3-d:5,6-d′]dipyrimidines using CoFe2O4@SiO2-PA-CC-guanidine-SA magnetic nanoparticles in water
Applied Organometallic Chemistry ( IF 3.9 ) Pub Date : 2021-08-19 , DOI: 10.1002/aoc.6293
Hedieh Rostami 1 , Lotfi Shiri 1
Affiliation  

In this study, the synthesis of pyrido[2,3-d:5,6-d′]dipyrimidines using CoFe2O4@SiO2-PA-CC-guanidine-SA magnetic nanoparticles with excellent yields has been reported. Pyrido[2,3-d:5,6-d′]dipyrimidines were synthesized from the four-component reaction of barbituric acid derivatives, benzaldehyde derivatives and ammonium acetate in water at room temperature. The synthesized catalyst was identified using Fourier-transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), X-ray powder diffraction (XRD), thermogravimetric analysis (TGA) and vibrating sample magnetometer (VSM) techniques.

中文翻译:

使用CoFe2O4@SiO2-PA-CC-胍-SA磁性纳米粒子在水中一锅法合成吡啶并[2,3-d:5,6-d']双嘧啶

在这项研究中,报道了使用 CoFe 2 O 4 @SiO 2 -PA-CC-胍-SA 磁性纳米粒子以优异的产率合成吡啶并[2,3-d:5,6-d']双嘧啶。由巴比妥酸衍生物、苯甲醛衍生物和乙酸铵在室温下在水中的四组分反应合成了吡啶并[2,3-d:5,6-d']双嘧啶。采用傅里叶变换红外光谱(FT-IR)、扫描电子显微镜(SEM)、能量色散X射线光谱(EDX)、X射线粉末衍射(XRD)、热重分析(TGA)和振动样品磁强计 (VSM) 技术。
更新日期:2021-09-28
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