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Condensation of Diamantan-3-one with Malononitrile and Methyl and Ethyl Cyanoacetates in the Presence of Binder-Free FeHY and NiHy Zeolites
Russian Journal of Organic Chemistry ( IF 0.8 ) Pub Date : 2021-07-18 , DOI: 10.1134/s1070428021060105 R. I. Khusnutdinov 1 , N. A. Shchadneva 1 , Yu. Yu. Mayakova 1 , R. I. Aminov 1
中文翻译：
Diamantan-3-one 与丙二腈、甲基和乙基氰基乙酸酯在无粘合剂 FeHY 和 NiHy 沸石存在下的缩合
更新日期：2021-07-19
Russian Journal of Organic Chemistry ( IF 0.8 ) Pub Date : 2021-07-18 , DOI: 10.1134/s1070428021060105 R. I. Khusnutdinov 1 , N. A. Shchadneva 1 , Yu. Yu. Mayakova 1 , R. I. Aminov 1
Affiliation
Abstract
Binder-free iron- and nickel-containing micro-, meso-, and macroporous zeolites FeHY and NiHY were found to effectively catalyze Knoevenagel condensation of diamantan-3-one with malononitrile, methyl cyanoacetate, and ethyl cyanoacetate at 40°C (5 h) with 94–98% yield.
中文翻译：
Diamantan-3-one 与丙二腈、甲基和乙基氰基乙酸酯在无粘合剂 FeHY 和 NiHy 沸石存在下的缩合
摘要
发现不含粘合剂的含铁和镍的微孔、中孔和大孔沸石 FeHY 和 NiHY 可有效催化 diamantan-3-one 与丙二腈、氰基乙酸甲酯和氰基乙酸乙酯在 40°C（5 小时）的 Knoevenagel 缩合反应。 ) 的产率为 94–98%。
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