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Effect of thermomechanical treatment on the microstructure and mechanical properties of Si-containing oxide dispersion strengthened reduced activation ferritic steel synthesized via mechanical alloying and spark plasma sintering
Nuclear Materials and Energy ( IF 2.6 ) Pub Date : 2021-07-15 , DOI: 10.1016/j.nme.2021.101041
Wahida R. Ilaham 1 , Lavish Kumar Singh 2 , Anil Kumar 1 , Tapas Laha 1
Affiliation  

The present work describes the effect of thermo-mechanical treatment on the microstructure, and its subsequent effect on the mechanical properties of Si-containing oxide dispersion strengthened (ODS) reduced activation ferritic (RAF) steel. ODS-RAF steel powder mixture with a nominal composition of Fe-14Cr-2W-0.3Ti-1Si-0.3Y2O3 was mechanically alloyed up to 50 h and subsequently consolidated via spark plasma sintering (SPS) at 900 °C followed by thermo-mechanical treatment (TMT) at 850 °C. Microstructural study revealed that the sintered sample consisted of ultrafine grains (0.35 µm) along with nano-size particles (Cr2TiO4, SiO2, and Y2Ti2O7) distributed in the matrix. This sintered sample exhibited excellent mechanical properties such as Vickers hardness (600 VHN), compressive strength (1795 MPa), and total elongation (21%), which is ascribed to the presence of ultrafine grains and nano-size particles. The thermo-mechanically treated sample exhibited an increase in the density by 2.7% and a reduction in the grain size by 23%. Consequently, the Vickers microhardness, compressive strength, and failure elongation of the sintered sample improved by 13%, 37%, and 19%, respectively, upon thermo-mechanical treatment.



中文翻译:

热机械处理对机械合金化和放电等离子烧结合成的含硅氧化物弥散强化还原活化铁素体钢组织和力学性能的影响

目前的工作描述了热机械处理对微观结构的影响,及其对含硅氧化物弥散强化 (ODS) 还原活化铁素体 (RAF) 钢机械性能的后续影响。标称成分为 Fe-14Cr-2W-0.3Ti-1Si-0.3Y 2 O 3 的ODS-RAF 钢粉混合物经机械合金化达 50 小时,随后通过放电等离子烧结 (SPS) 在 900 °C 下固化在 850 °C 下进行热机械处理 (TMT)。微观结构研究表明,烧结样品由超细晶粒 (0.35 µm) 和纳米级颗粒(Cr 2 TiO 4、SiO 2和 Y 2 Ti 2 O 7) 分布在矩阵中。该烧结样品表现出优异的机械性能,如维氏硬度 (600 VHN)、抗压强度 (1795 MPa) 和总伸长率 (21%),这归因于超细晶粒和纳米尺寸颗粒的存在。经过热机械处理的样品密度增加了 2.7%,晶粒尺寸减少了 23%。因此,经热机械处理后,烧结样品的维氏显微硬度、抗压强度和破坏伸长率分别提高了 13%、37% 和 19%。

更新日期:2021-07-20
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