Petroleum Chemistry ( IF 1.4 ) Pub Date : 2021-07-08 , DOI: 10.1134/s0965544121080089 D. E. Tsaplin 1 , L. A. Kulikov 1 , S. V. Egazar’yants 1 , E. A. Karakhanov 1 , E. R. Naranov 2 , I. S. Levin 2 , A. L. Maximov 2
Abstract
Zeolite-containing materials of various structural types (MFI, MEL, MTW) were prepared by the hydrothermal method using organic templates based on quaternary polymethylenediammonium salts. The materials were characterized by X-ray diffraction analysis, low-temperature nitrogen adsorption–desorption, temperature-programmed ammonia desorption, IR spectroscopy, scanning electron microscopy, X-ray fluorescence analysis, transmission electron microscopy, solid-state 27Al NMR spectroscopy, and IR spectroscopy of adsorbed pyridine. The effect of the template on the structure of the material obtained was revealed.
中文翻译:
在二甲基乙醇胺衍生的二季烷基铵盐存在下结晶沸石
摘要
使用基于季聚亚甲基二铵盐的有机模板,通过水热法制备了各种结构类型(MFI、MEL、MTW)的含沸石材料。通过 X 射线衍射分析、低温氮吸附-解吸、程序升温氨解吸、红外光谱、扫描电子显微镜、X 射线荧光分析、透射电子显微镜、固态27 Al NMR 光谱、和吸附吡啶的红外光谱。揭示了模板对所得材料结构的影响。