Microwave improved porous CoFe₂O₄ and TiO₂ doped CoFe₂O₄ nanostructures were designed using L-threonine as a fuel in our current research work. The synthesized nanomaterials were characterised and investigated to determine the photocatalytic degradation of congo red dye on irradiation of visible light. The powder XRD pattern proved that the obtained crystallite size of CoFe₂O₄ is 44 nm and TiO₂ doped CoFe₂O₄ is 25 nm. It has been observed that the crystalline size is much lower for TiO₂ doped CoFe₂O₄ when compared to the CoFe₂O₄, which is due to the doping of titania. Furthermore, the SEM images of titania doped CoFe₂O₄ indicates that the smaller particles are dispersed with a high agglomeration, due to the interfacial surface tension between the titania and cobalt ferrite particles. DRS spectra proved the measured bandgap of the corresponding CoFe₂O₄ and TiO₂ doped CoFe₂O₄ nanostructures are 3.01 eV and 2.88 eV. The microstructure and the dimension of the synthesized CoFe₂O₄ and TiO₂ doped CoFe₂O₄ spinel ferrites nanostructures were explored by high resolution transmission electron microscope (HR-TEM). The association of photocatalytic properties of CoFe₂O₄ and TiO₂ doped CoFe₂O₄ in a solitary particle is the projected advantage of the current work.

在我们目前的研究工作中，使用 L-苏氨酸作为燃料设计了微波改进的多孔 CoFe ₂ O ₄和 TiO ₂掺杂的 CoFe ₂ O ₄纳米结构。对合成的纳米材料进行表征和研究，以确定刚果红染料在可见光照射下的光催化降解。粉末XRD图证明获得的CoFe ₂ O _{4 的}微晶尺寸为44nm ，TiO ₂掺杂的CoFe ₂ O ₄为25nm。已经观察到，TiO ₂掺杂的 CoFe ₂ O ₄的晶体尺寸小得多与 CoFe ₂ O ₄相比，这是由于二氧化钛的掺杂。此外，二氧化钛掺杂的 CoFe ₂ O ₄的 SEM 图像表明，由于二氧化钛和钴铁氧体颗粒之间的界面表面张力，较小的颗粒以高附聚分散。DRS光谱证明相应的CoFe ₂ O ₄和TiO ₂掺杂的CoFe ₂ O ₄纳米结构的测量带隙为3.01eV和2.88eV。合成的CoFe ₂ O ₄和TiO ₂掺杂的CoFe ₂ O的微观结构和尺寸通过高分辨率透射电子显微镜 (HR-TEM) 探索了_{4 种}尖晶石铁氧体纳米结构。CoFe ₂ O ₄和掺杂TiO _{2 的}CoFe ₂ O ₄在单独粒子中的光催化性能的关联是当前工作的预期优势。