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Microstructure and Superconducting Properties of Rapid Heating, Quenching, and Transformation (RHQT) Powder-in-Tube Nb3Al Wires Doped with Sn Element
Physica Status Solidi (A) - Applications and Materials Science ( IF 2 ) Pub Date : 2021-05-20 , DOI: 10.1002/pssa.202100081
Yuanbin Hu 1 , Mingming Ran 1 , Ming Chen 1 , Xuan Yu 1 , Lian Liu 1 , Yongliang Chen 1 , Yong Zhang 1 , Zhou Yu 1 , Yong Zhao 1, 2, 3
Affiliation  

Properties of rapid heating, quenching, and transformation (RHQT)-treated powder-in-tube (PIT) Nb3Al1−xSnx wires are studied herein. After the RHQ process, the body-centered cubic (bcc) phase is formed in the Sn-doped Nb3Al wires. The transformed superconducting A15 phase shows a uniform microstructure and homogenous component distribution feature. With the increase of the Sn doping level, the critical transition temperature (Tc), critical current density (Jc), and irreversibility field (Birr) of the superconducting wires increase first and then reduce, achieving the highest Tc value of 17.6 K and the smallest ΔTc of 0.6 K in the 4% Sn doped Nb3Al wire. The 4% Sn addition helps to improve the layer Jc of the sample to 2.1 × 105 A cm−2 at 8 K and 5 T, which is about 2.5 times that of the pure Nb3Al sample. Furthermore, the Nb3Al1−xSnx (x = 0.04) wire gives the highest Birr value of 17.22, 13.23, and 9.11 T at 8, 10, and 12 K, respectively. The addition of Sn helps to achieve stoichiometric Nb3Al A15 phase and formation of precipitations with the size of 10 nm, which might act as the flux-pinning center.

中文翻译:

快速加热淬火相变 (RHQT) 管内粉末掺锡 Nb3Al 线材的显微组织和超导性能

本文研究了快速加热、淬火和相变 (RHQT) 处理的管内粉末 (PIT) Nb 3 Al 1- x Sn x线材的特性。在RHQ工艺之后,体心立方(bcc)相在Sn掺杂的Nb 3 Al线中形成。转变后的超导 A15 相显示出均匀的微观结构和均匀的成分分布特征。与Sn的掺杂水平的增加,临界转变温度(Ť Ç),临界电流密度(Ĵ Ç)和不可逆场(IRR超导线材先增加后降低的),达到最高Ť Ç在 4% Sn 掺杂的 Nb 3 Al 线中,17.6 K 的值和0.6 K的最小 Δ T c。添加 4% Sn 有助于将样品的层J c在 8 K 和 5 T下提高到 2.1 × 10 5  A cm -2,大约是纯 Nb 3 Al 样品的2.5 倍。此外,Nb 3 Al 1- x Sn x ( x  = 0.04) 焊丝在 8、10 和 12 K 下分别提供了17.22、13.23和 9.11 T的最高B irr值。添加 Sn 有助于实现化学计量的 Nb 3Al A15 相和尺寸为 10 nm 的析出物的形成,可能作为磁通钉扎中心。
更新日期:2021-05-20
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