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The comparison of bulk and in-situ irradiation damage on cubic-Lu2TiO5 and orthorhombic-La2TiO5
Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms ( IF 1.3 ) Pub Date : 2021-05-04 , DOI: 10.1016/j.nimb.2021.04.017
Huanhuan He , Qiurong Xie , Zhiwei Lin , Shengming Jiang , Xiaotian Hu , Ming Tang , Jian Zhang

Polycrystalline cubic-Lu2TiO5 and orthorhombic-La2TiO5 compounds were prepared by traditional ceramic processing. In-situ and ex-situ ion beam irradiations were performed on these samples at room temperature. Bulk samples were irradiated with 800 keV Kr2+ ions and characterised ex-situ, whilst powder samples were in-situ irradiated with 1 MeV Kr2+ ions. For Lu2TiO5, a completely amorphization was observed at the fluences of 2 × 1014 ions/cm2 (~0.37 dpa) in the bulk sample and 5 × 1014 ions/cm2 (~0.99 dpa) in the TEM sample. For La2TiO5, complete amorphization was observed at the fluences of 5 × 1013 ions/cm2 (~0.08 dpa) in the bulk sample and 1.25 × 1014 ions/cm2 (~0.21 dpa) in the TEM sample. It seems that a higher irradiation fluence to amorphization was needed for in-situ TEM samples than that for bulk samples.



中文翻译:

立方Lu 2 TiO 5和正交晶La 2 TiO 5的整体和原位辐照损伤的比较

通过传统的陶瓷工艺制备了多晶立方Lu 2 TiO 5和正交晶La 2 TiO 5化合物。在室温下对这些样品进行原位和异位离子束辐照。用800 keV Kr 2+离子辐照大块样品并进行原位表征,而用1 MeV Kr 2+离子原位辐照粉末样品。对于Lu 2 TiO 5,在批量样品中以2×10 14离子/ cm 2(〜0.37 dpa)和5×10 14离子/ cm 2的通量观察到完全非晶化。(〜0.99 dpa)在TEM样品中。对于La 2 TiO 5,整体样品的注量为5×10 13离子/ cm 2(〜0.08 dpa),而TEM样品的注量为1.25×10 14离子/ cm 2(〜0.21 dpa),则完全非晶化。似乎原位TEM样品比散装样品需要更高的辐照通量以实现非晶化​​。

更新日期:2021-05-05
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