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Effect of the PANI content on Curie temperature and microwave absorption properties of SrFe 11 MnO 19 /CoFe 1.9 Bi 0.1 O 4 nanocomposite
Applied Physics A ( IF 2.7 ) Pub Date : 2021-05-05 , DOI: 10.1007/s00339-021-04556-z
S. E. Mousavi Ghahfarokhi , M. Ahmadi , I. Kazeminezhad

The SrFe11MnO19/CoFe1.9Bi0.1O4/PANI nanocomposites were prepared with different mass ratios of SrFe11MnO19/CoFe1.9Bi0.1O4 to PANI by the auto-combustion sol–gel and in-situ polymerization methods. The nanocomposites were analyzed with several techniques such as FTIR, XRD, VSM, and VNA. The Fourier-transform infrared spectroscopy (FT-IR) analysis shows that all pure PANI absorption bonds (exception of the 477 cm−1) have existed in SrFe11MnO19/CoFe1.9Bi0.1O4. X-ray diffraction (XRD) depicts the simultaneous existence of the ferrite composite and PANI phases. Also, VSM analysis reveals that the saturation magnetization (Ms) and the remanence magnetization (Mr) decrease while the magnetic coercivity field (HC) remains almost constant in SrFe11MnO19/CoFe1.9Bi0.1O4/PANI samples. Besides, the Faraday balance technique represents that Curie temperature (TC) of ferrite nanocomposite decreasing with increasing PANI ratio, as well as vector network analysis (VNA) in X and Ku bands, showed that the minimum reflection loss (RL) is − 24.3 dB that belonged to SrFe11MnO19/CoFe1.9Bi0.1O4/PANI with ferrite composite to PANI mass ratio of (C: P = 80:20) %.



中文翻译:

PANI含量对SrFe 11 MnO 19 / CoFe 1.9 Bi 0.1 O 4纳米复合材料居里温度和微波吸收性能的影响

的SRFE 11的MnO 19 /由CoFe 1.9的Bi 0.1 ø 4 / PANI纳米复合材料用SRFE的不同质量比制备11的MnO 19 /由CoFe 1.9的Bi 0.1 Ò 4到PANI由自动燃烧溶胶-凝胶和原位聚合的方法。使用诸如FTIR,XRD,VSM和VNA的多种技术分析了纳米复合材料。傅立叶变换红外光谱(FT-IR)分析表明,SrFe 11 MnO 19 / CoFe 1.9 Bi 0.1中存在所有纯PANI吸收键(477 cm -1除外)。O 4。X射线衍射(XRD)描绘了铁素体复合物相和PANI相的同时存在。此外,VSM分析表明,在SrFe 11 MnO 19 / CoFe 1.9 Bi 0.1 O 4 / PANI样品中,饱和磁化强度(M s)和剩磁强度(M r)降低,而矫顽力场(H C)几乎保持恒定。此外,法拉第平衡技术表明,铁素体纳米复合材料的居里温度(T C)随PANI比的增加而降低,以及X和K u中的矢量网络分析(VNA)。谱带显示最小反射损耗(R L)为− 24.3 dB,属于SrFe 11 MnO 19 / CoFe 1.9 Bi 0.1 O 4 / PANI,铁氧体与PANI的质量比为(CP  = 80:20)% 。

更新日期:2021-05-05
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