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Development of hybrid materials based on carbon black reinforced poly(2-methoxyaniline): preparation, characterization and tailoring optical, thermal and electrochemical properties
Colloid and Polymer Science ( IF 2.4 ) Pub Date : 2021-04-18 , DOI: 10.1007/s00396-021-04837-2
F. Z. Kouidri , I. Moulefera , S. Bahoussi , A. Belmokhtar , A. Benyoucef

A novel type of poly(2-methoxyaniline)@carbon black (P2MA@CB) was formulated by incorporating laboratory synthesized CB nanoparticles into pure P2MA. The resulting materials were characterized using X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), ultraviolet-visible spectroscopy (UV-vis), Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), thermogravimetric analysis (TGA) and electrochemically by cyclic voltammetry (CV). The optical study shows the P2MA@CB samples to be of nanosize. Besides, the CV results show that this nanomaterials exhibited high electroactivity. All the results demonstrated that the P2MA@CB (0.5g) hybrid material is very promising for application in electrochemical sensing.

Graphical abstract



中文翻译:

基于炭黑增强的聚(2-甲氧基苯胺)的杂化材料的开发:制备,表征和定制光学,热和电化学性能

通过将实验室合成的CB纳米粒子掺入纯P2MA中,配制出一种新型的聚(2-甲氧基苯胺)@炭黑(P2MA @ CB)。使用X射线光电子能谱(XPS),X射线衍射(XRD),紫外可见光谱(UV-vis),傅立叶变换红外光谱(FTIR),透射电子显微镜(TEM),热重分析法对所得材料进行表征(TGA)和电化学的循环伏安法(CV)。光学研究表明,P2MA @ CB样品具有纳米尺寸。此外,CV结果表明该纳米材料表现出高电活性。所有结果表明,P2MA @ CB(0.5g)杂化材料在电化学传感中具有广阔的应用前景。

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更新日期:2021-04-18
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