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Mesoporous SBA-15@ n -Pr-THAM-ZrO organic–inorganic hybrid: as a highly efficient reusable nanocatalyst for the synthesis of polyhydroquinolines and 2,3-dihydroquinazolin-4 (1h)-ones
Journal of Porous Materials ( IF 2.6 ) Pub Date : 2021-04-01 , DOI: 10.1007/s10934-021-01063-7
Arash Ghorbani-Choghamarani , Hamid Aghavandi , Masoud Mohammadi

In this work, tris(hydroxymethyl)aminomethane-Zirconium complex supported on modified SBA-15 (SBA-15@n-Pr-THMAM-ZrO) prepared as a novel mesoporous catalyst. The structure of this porous compound was characterized by XRD, nitroge adsorption–desorption, TEM, TGA, EDS, ICP, X-ray mapping, and SEM techniques. The catalytic activity of SBA-15@n-Pr-THMAM-Zr has been investigated for the multicomponent synthesis of polyhydroquinoline and 2,3-dihydroquinazolin-4(1H)-one derivaives.



中文翻译:

介孔SBA-15 @ n -Pr-THAM-ZrO有机-无机杂化物:作为高效可重复使用的纳米催化剂,用于合成聚氢喹啉和2,3-二氢喹唑啉-4(1h)-ones

在这项工作中,负载在改性SBA-15(SBA-15n-Pr-THMAM-ZrO)上的三(羟甲基)氨基甲烷-锆络合物被制备为新型介孔催化剂。该多孔化合物的结构通过XRD,亚硝基吸附解吸,TEM,TGA,EDS,ICP,X射线绘图和SEM技术表征。研究了SBA-15n-Pr-THMAM-Zr对多氢喹啉和2,3-二氢喹唑啉-4(1H)-一种衍生物的多组分合成的催化活性。

更新日期:2021-04-02
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