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Simultaneous isolation and selective encapsulation of volatile compounds from essential oil during electrospraying of β-Cyclodextrin
Carbohydrate Polymers ( IF 11.2 ) Pub Date : 2021-01-22 , DOI: 10.1016/j.carbpol.2021.117673
Merve Deniz Köse , Buse Nur Tekin , Oguz Bayraktar

This study's primary purpose was to develop a new technique to stabilize high value-added bioactive volatile compounds present in essential oils to ensure their usability as chemical raw materials with enhanced stability. Selective isolation and encapsulation of various volatile compounds by changing the electrospraying process parameter, including voltage, flow rate, and β-Cyclodextrin concentration, were attributed to the formation of inclusion complexes between β-cyclodextrin and volatile compounds. Investigations regarding the effects of independent process variables on simultaneous isolation and selective encapsulation of volatile compounds during electrospraying of β-cyclodextrins were carried out mainly with TLC analyses. The TLC analyses were confirmed with GC, GC–MS, and 1H NMR analyses. It was possible to obtain nanoparticles with an average particle size between 25–160 nm with the designed system. Obtained data revealed that isolation and encapsulation of cumin aldehyde, camphene, isoborneol, and hexadecanoic acid, benzyl benzoate from labdanum essential oil were successfully achieved.



中文翻译:

β-环糊精电喷雾过程中香精油中挥发性化合物的同时分离和选择性包封

这项研究的主要目的是开发一种新技术,以稳定精油中存在的高附加值生物活性挥发性化合物,以确保其用作化学原料的稳定性得到增强。通过改变电喷雾工艺参数(包括电压,流速和β-环糊精浓度)对各种挥发性化合物的选择性分离和包封归因于β-环糊精与挥发性化合物之间的包合物的形成。关于主要过程变量对电喷雾β-环糊精同时挥发物同时分离和选择性包封的影响的研究主要是通过TLC分析进行的。通过GC,GC-MS和1确认了TLC分析1 H NMR分析。使用设计的系统可以获得平均粒径在25-160 nm之间的纳米颗粒。获得的数据表明,成功地从劳丹精油中分离并包封了孜然醛,樟脑,异冰片和十六烷酸,苯甲酸苄酯。

更新日期:2021-01-25
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